C08.03 - Physical Properties

SIGNIFICANCE AND USE
3.1 Insulating firebrick (IFB) are classified by their bulk density and reheat change (see Classification C155). This test method defines thermal stability by measurement of IFB's reheat change following 24 h at a test temperature.  
3.2 Since this test exposes the entire sample to an isothermal temperature condition, the user should be aware that most applications for IFB involve a thermal gradient which may cause the IFB's dimensions to change differentially.
SCOPE
1.1 This test method covers the determination of the permanent linear (and volume) change of insulating firebrick upon reheating under prescribed conditions.  
1.2 The values stated in inch-pound units are to be regarded as the standard. The values given in parentheses are for information only.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 Apparent porosity, water absorption, apparent specific gravity, and bulk density are primary properties of refractory shapes. These properties are widely used in the evaluation and comparison of product quality and as part of the criteria for selection and use of refractory products in a variety of industrial applications. These test methods are used for determining any or all of these properties and are particularly useful for testing hydratable products.  
3.2 These test methods are primary standard methods that are suitable for use in quality control, research and development, establishing criteria for and evaluating compliance with specifications, and providing data for design purposes.  
3.3 Fundamental assumptions inherent in these test methods are:  
3.3.1 The test specimens conform to the requirements for size, configuration, and original faces,  
3.3.2 The open pores of the test specimens are fully impregnated with liquid during the vacuum-pressure treatment, and  
3.3.3 The blotting of the saturated test specimens is performed as specified in a consistent and uniform manner to avoid withdrawing liquid from the pores.  
3.3.4 Deviation from any of these assumptions adversely affects the test results.  
3.4 In laboratory studies involving castable specimen, a bias was noted between formed 2 in. by 2 in. by 2 in. (50 mm by 50 mm by 50 mm) and specimens quartered from larger 9 in. by 4.5 in. by 2.5 in. (228 mm by 114 mm by 64 mm) cast specimens. Additionally, an error in the apparent porosity determination was found on castables whenever the specimens were heated to 1500 °F (816 °C) and then exposed to water as a saturation media. The error was attributed to reactivity of cement with water and subsequent re-hydration of cement phases. The higher the cement level of the castable, the greater the error noted. It was concluded that an error in porosity values could occur for refractory materials having a potential to form hydrated species with water. T...
SCOPE
1.1 These test methods cover the determination of the following properties of refractory shapes:  
1.1.1 Apparent porosity,  
1.1.2 Liquid absorption,  
1.1.3 Apparent specific gravity, and  
1.1.4 Bulk density.  
1.2 These test methods are applicable to all refractory shapes except those that chemically react with both water and mineral spirits. When testing a material capable of hydration or other chemical reaction with water but which does not chemically react with mineral spirits, mineral spirits is substituted for water and appropriate corrections for the density differences are applied when making calculations.  
1.3 Units—The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.3.1 Exception—The apparatus used in this standard is only available in SI units.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
Note 1: Test Methods C20 cover procedures for testing properties of refractories that are not attacked by water.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 Refractory brick are used as modular units in furnace construction and should not deviate significantly from the intended configuration with respect to size, bulk density, flat surfaces, and right angles. These test methods are particularly suited for use under field conditions and provide a means to determine whether the brick meets the requirements considered necessary to assure a satisfactory refractory construction.
SCOPE
1.1 These test methods cover procedures for measuring size, dimensional measurement, bulk density, warpage, and squareness of rectangular dense refractory brick and rectangular insulating firebrick. More precise determination of bulk density of refractory brick can be made by Test Methods C20. Stack height is generally determined only for dense refractories.  
Note 1: Test Methods C830 and Test Method C914 are also used to determine bulk density of refractory brick, by different procedures.  
1.2 The test methods appear in the following order:    
Sections    
Size and Bulk Density  
4 through 7    
Warpage of Refractory Brick  
8 through 10    
Squareness of Refractory Brick  
11 through 14  
1.3 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
4.1 The true specific gravity of a material is the ratio of its true density, determined at a specific temperature, to the true density of water, determined at a specific temperature. Thus, the true specific gravity of a material is a primary property which is related to chemical and mineralogical composition.  
4.2 This test method is particularly useful for hydratable materials that are not suitable for test with Test Method C135.  
4.3 For refractory raw materials and products, the true specific gravity is a useful value for: classification, detecting differences in chemical composition between supposedly like samples, indicating mineralogical phases or phase changes, calculating total porosity when the bulk density is known, and for any other test method that requires this value for the calculation of results.  
4.4 This test method is a primary standard method which is suitable for use in specifications, quality control, and research and development. It can also serve as a referee test method in purchasing contracts or agreements.  
4.5 Fundamental assumptions inherent in this test method are the following:  
4.5.1 The sample is representative of the material in general,  
4.5.2 The total sample has been reduced to the particle size specified,  
4.5.3 No contamination has been introduced during processing of the sample,  
4.5.4 The ignition of the sample has eliminated all free or combined water without inducing sintering or alteration,  
4.5.5 An inert gas (helium) has been used in the test, and  
4.5.6 The test method has been conducted in a meticulous manner.  
4.5.7 Deviation from any of these assumptions negates the usefulness of the results.  
4.6 In interpreting the results of this test method, it must be recognized that the specified sample particle size is significantly finer than specified for Test Method C135. Even this finer particle size for the sample does not preclude the presence of some closed pores, and the amount of residual close...
SCOPE
1.1 This test method covers the determination of the true specific gravity of solid materials, and is particularly useful for materials that easily hydrate which are not suitable for test with Test Method C135. This test method may be used as an alternate for Test Methods C135, C128, and C188 for determining true specific gravity.  
1.2 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.2.1 Exception—In 7.3, the equivalent SI unit is expressed in parentheses.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 Fireclay steel-teeming nozzles and sleeves are classified by volume reheat change. Bloating of some refractories results in irregular reheat dimensions, which are difficult to measure. This practice determines the volume without depending upon physical linear measurements.  
3.2 Blast furnace checkers that have irregular cross-sections are classified by “creep properties.” This practice determines the average cross-sectional area.
SCOPE
1.1 This practice covers the methods of calculating areas, volumes, and linear changes of irregularly shaped refractory specimens.  
1.2 The specimens must have a constant cross-sectional area over a length (L).  
1.3 The values stated in SI units are to be regarded as the standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 Apparent porosity, water absorption, apparent specific gravity, and bulk density are primary properties of burned refractory brick and shapes. These properties are widely used in the evaluation and comparison of product quality and as part of the criteria for selection and use of refractory products in a variety of industrial applications. These test methods are used for determining any or all of these properties.  
3.2 These test methods are primary standard methods which are suitable for use in quality control, research and development, establishing criteria for and evaluating compliance with specifications, and providing data for design purposes.  
3.3 Fundamental assumptions inherent in these test methods are that the test specimens are not attacked by water, the test specimens conform to the requirements for size, configuration, and original faces, the open pores of the test specimens are fully impregnated with water during the boiling treatment, and the blotting of the saturated test specimens is performed as specified in a consistent and uniform manner to avoid withdrawing water from the pores. Deviation from any of these assumptions adversely affects the test results.  
3.4 In laboratory studies involving castable specimens, a bias was noted between formed 2 by 2 by 2 in. (50 by 50 by 50 mm) and specimens that were quartered from larger 9 by 4.5 by 2.5 (228 by 114 by 64 mm) cast specimens. Additionally, an error in the apparent porosity determination on castables was found whenever the specimens were heated to 1500 °F (816 °C) and then exposed to water as a saturation media (Test Methods C830). The error was attributed to reactivity of cement with water and subsequent re-hydration of cement phases. The higher the cement level of the castable, the greater the error noted. It was concluded that an error in porosity values could occur for refractory materials having a potential to form hydrated species with water.3  
3.5 Certain precautions must be exe...
SCOPE
1.1 These test methods cover the determination of the following properties of burned refractory brick:  
1.1.1 Apparent porosity,  
1.1.2 Water absorption,  
1.1.3 Apparent specific gravity, and  
1.1.4 Bulk density.  
1.2 These test methods are not applicable to refractories attacked by water.  
1.3 The values stated in inch-pound units are to be regarded as the standard. The values given in parentheses are for information only.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 The true specific gravity of a material is the ratio of its true density, determined at a specific temperature, to the true density of water, determined at a specific temperature. Thus, the true specific gravity of a material is a primary property which is related to chemical and mineralogical composition.  
3.2 For refractory raw materials and products the true specific gravity is a useful value for: classification, detecting differences in chemical composition between supposedly like samples, indicating mineralogical phases or phase changes, calculating total porosity when the bulk density is known, and for any other test method which requires this value for the calculation of results.  
3.3 This test method is a primary standard method which is suitable for use in specifications, quality control, and research and development. It can also serve as a referee test method in purchasing contracts or agreements.  
3.4 Fundamental assumptions inherent in this test method are the following:  
3.4.1 The sample is representative of the material in general,  
3.4.2 The total sample has been reduced to the particle size specified,  
3.4.3 No impurity has been introduced during processing of the sample,  
3.4.4 The sample itself is not magnetic and all magnetic material introduced during processing of the sample has been removed,  
3.4.5 The material is not hydratable or reactive with water, and  
3.4.6 The test method has been conducted in a meticulous manner.  
3.4.7 Deviation from any of these assumptions negates the usefulness of the results.  
3.5 In interpreting the results of this test method it must be recognized that the specified sample particle size does not guarantee that all closed pores have been eliminated. The amount of residual closed pores may vary between materials or even between samples of the same or like materials, and the specified sample particle size is not the same as that specified for Test Method C604. The values generated by this ...
SCOPE
1.1 This test method covers the determination of true specific gravity of refractory materials under prescribed conditions. It is not applicable to materials attacked by water.  
1.2 Units—The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.2.1 Exception—The equipment used in this standard for weights and volumes is only available in SI units.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
2.1 This test method may be used to quickly determine volume and bulk density of a refractory of any shape, provided it has sufficient structural integrity to permit handling. Thus it may be used on unfired or fired, strong or friable shapes.  
2.2 Since the test may be performed quickly, it has found application as manufacturing in-process control as well as in characterizing finished refractory products. Also it may be used to examine specimens after other test or service exposure.
SCOPE
1.1 This test method covers the basic procedure for determining bulk density and volume of refractory shapes. This test is applicable to all refractory shapes or monoliths, burned or unburned, independent of composition or forming method, including materials that slake and hydrate. It is particularly suitable for determining bulk density and volume of complex shapes after forming, since results may be obtained in a matter of minutes.  
1.2 Units—The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.2.1 Exception—The balance used in this standard is only available in SI units (Sections 3 – 6).  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For a specific hazard statement, see 3.2.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 Granular refractory materials may be either refractory grain raw materials that are used in the manufacture of finished refractory products, or bulk granular refractory materials that are sold, with or without some degree of processing, to refractory consumers for various uses. In either case, characterizing the properties of a granular refractory material is essential in evaluating its quality or consistency of quality and in determining suitability for end use. One of the important properties is bulk density because of its relationship to end product quality, usage, and performance.  
3.2 The refractories producer can use this test method as one of the quality control tests for his manufactured or mined refractory grain raw materials or for evaluating potential refractory grain raw materials.  
3.3 For the refractories consumer, the principal use of this test method is in the evaluation of the quality or the consistency of quality of the granular material in purchased refractory mixes or in bulk granular refractory materials used by the consumer.  
3.4 This is a primary test method, and thus is suitable for use in specifications, quality control, and research and development. It can also serve as a referee test method in purchasing contracts or agreements and as a base for development of more rapid, secondary test methods for use in quality control on manufactured refractory raw materials.  
3.5 Fundamental assumptions inherent in this test method are that the sample is representative of the material in general, the particle size of the sample is within the range specified by the test method, the material is not readily hydratable, and the size and quantity of pores in the material permits removal of surface water without drainage from the pores themselves. Deviation from any of these assumptions negates the usefulness of the test results.  
3.6 In interpreting the results of this test method, it must be recognized that the specific gravity of the materia...
SCOPE
1.1 This test method covers a procedure for determining the bulk density of granular refractory materials, commercial products which usually have particles that are retained on a 0.265 in. (6.7 mm) or coarser sieve.  
Note 1: This test method is not suitable for materials that hydrate in boiling water.  
1.2 Units—The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.2.1 Exceptions—In Sections 4, 7, and 8, the apparatus used is only available in SI units.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
4.1 This test method measures the relative abrasion resistance of various refractory samples under standard conditions at room temperature.  
4.2 The abrasion resistance of a refractory material provides an indication of its suitability for service in abrasive environments.  
4.3 The results obtained by this test method could be different than those obtained in service because of the different conditions encountered.
SCOPE
1.1 This test method covers the determination of relative abrasion resistance of refractory brick at room temperature. This test method can also be applied to castable refractories (see Metric Dimensions, Practice C861 and Practice C865) and plastic refractories (see Practice C1054).  
1.2 Units—When values are stated in both SI and inch-pound units, the units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, use each system independently of the other. Combining values from the two systems may result in nonconformance with the standard. Several values are stated only in SI units as a matter of convention and to permit comparison of results. Included are the abrading media weight (grams), specimen weight (grams), specimen weight loss due to abrasion (grams), and the resultant volume loss (cubic centimeters).  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 Particle size distribution has a major effect upon most of the refractory properties. These test methods provide a means of measuring the distribution for the purpose of comparison to the desired distribution.  
3.2 These test methods also cover determination of the water content of refractory materials in the wet condition and of air-dried samples received, so that the sieve analysis can be calculated on the dry basis.  
3.3 These methods can produce data for specification acceptance, design purposes, manufacturing control, and research and development.  
3.4 A reference set of standard matched or calibrated sieves4 shall be provided for use in checking the set of sieves used in the actual sieve analysis of samples. The sieves for use in sieve analysis may also be standard matched sieves or may be unmatched sieves conforming to the Specification Table in Specification E11, provided that such sieves will give results that differ by no more than 5 % from those obtained with the reference set when the two sets are compared in accordance with the section of Test Method C429 on testing of sieves and sample splitters.
SCOPE
1.1 These test methods cover a wet and a dry method for sieve analysis of refractory materials.  
1.1.1 Wet Sieve Analysis—Water promotes the slaking of clays and helps to separate fine particles, washing them from the larger grains. This method is recommended for use with materials that require water addition, and that slake in normal industrial use.  
1.1.2 Dry Sieve Analysis—The dry method is not as effective as the wet method in determining the amount of material present in the smaller particle sizes. It is recommended (1) for clays, when the slaking action of water is undesirable, (2) when the material is in the form of coarsely ground grog and calcine, and (3) when the clay is to be used in such a way that the ultimate particle size is of secondary importance.  
1.2 These test methods also cover determination of the water content of refractory materials in the wet condition and of air-dried samples as received, so that the sieve analysis can be calculated on the dry basis. Included is a method for obtaining the water content of other refractory materials, such as plastic refractories and wet mixes.  
1.3 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 This test method is used to measure the rate of flow of air or nitrogen through refractory brick and monoliths and to thus determine the permeability of tested products.  
3.2 This test method is useful in research and development for establishing the relative permeability of products within comparable classes. It may also be used to identify acceptable products for design purposes and to establish permeability criteria for specification acceptance.  
3.3 It must be recognized that permeability can vary in different directions and different parts of a refractory due to factors such as forming procedure, grain size and distribution, and heat treatment.
SCOPE
1.1 This test method covers determination of the permeability of refractory brick and monoliths, from which suitable specimens can be cut, at room temperature.  
1.2 Units—The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.2.1 Exceptions—The apparatus used in this standard is only available in SI units (Section 4). Also, some of the calculations must use SI units only.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 Refractory brick and shapes of different compositions exhibit unique permanent linear changes after heating or reheating. This test method provides a standard procedure for heating various classes of refractories with appropriate heating schedules.  
3.2 Linear reheat changes obtained by this test method are suitable for use in research and development, also often used to establish written specifications between producers and consumers.  
3.3 Care should be exercised in selecting samples that are representative of the product being tested and that the schedule selected is appropriate to the product.
SCOPE
1.1 This test method covers the determination of the permanent linear change of refractory brick when heated under prescribed conditions.  
1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
Note 1: Test methods incorporating additional provisions pertinent to specific refractory materials are given in the following Test Methods: C179, C210, and C605.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 Particle size distribution has a major effect upon most of the refractory properties. These test methods provide a means of measuring the distribution for the purpose of comparison to the desired distribution.  
3.2 These test methods also cover determination of the water content of refractory materials in the wet condition and of air-dried samples received, so that the sieve analysis can be calculated on the dry basis.  
3.3 These methods can produce data for specification acceptance, design purposes, manufacturing control, and research and development.  
3.4 A reference set of standard matched or calibrated sieves4 shall be provided for use in checking the set of sieves used in the actual sieve analysis of samples. The sieves for use in sieve analysis may also be standard matched sieves or may be unmatched sieves conforming to the Specification Table in Specification E11, provided that such sieves will give results that differ by no more than 5 % from those obtained with the reference set when the two sets are compared in accordance with the section of Test Method C429 on testing of sieves and sample splitters.
SCOPE
1.1 These test methods cover a wet and a dry method for sieve analysis of refractory materials.  
1.1.1 Wet Sieve Analysis—Water promotes the slaking of clays and helps to separate fine particles, washing them from the larger grains. This method is recommended for use with materials that require water addition, and that slake in normal industrial use.  
1.1.2 Dry Sieve Analysis—The dry method is not as effective as the wet method in determining the amount of material present in the smaller particle sizes. It is recommended (1) for clays, when the slaking action of water is undesirable, (2) when the material is in the form of coarsely ground grog and calcine, and (3) when the clay is to be used in such a way that the ultimate particle size is of secondary importance.  
1.2 These test methods also cover determination of the water content of refractory materials in the wet condition and of air-dried samples as received, so that the sieve analysis can be calculated on the dry basis. Included is a method for obtaining the water content of other refractory materials, such as plastic refractories and wet mixes.  
1.3 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
2.1 This test method may be used to quickly determine volume and bulk density of a refractory of any shape, provided it has sufficient structural integrity to permit handling. Thus it may be used on unfired or fired, strong or friable shapes.  
2.2 Since the test may be performed quickly, it has found application as manufacturing in-process control as well as in characterizing finished refractory products. Also it may be used to examine specimens after other test or service exposure.
SCOPE
1.1 This test method covers the basic procedure for determining bulk density and volume of refractory shapes. This test is applicable to all refractory shapes or monoliths, burned or unburned, independent of composition or forming method, including materials that slake and hydrate. It is particularly suitable for determining bulk density and volume of complex shapes after forming, since results may be obtained in a matter of minutes.  
1.2 Units—The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.2.1 Exception—The balance used in this standard is only available in SI units (Sections 3 – 6).  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For a specific hazard statement, see Note 2.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
4.1 This test method measures the relative abrasion resistance of various refractory samples under standard conditions at room temperature.  
4.2 The abrasion resistance of a refractory material provides an indication of its suitability for service in abrasive environments.  
4.3 The results obtained by this test method could be different than those obtained in service because of the different conditions encountered.
SCOPE
1.1 This test method covers the determination of relative abrasion resistance of refractory brick at room temperature. This test method can also be applied to castable refractories (see Metric Dimensions, Practice C861 and Practice C865) and plastic refractories (see Practice C1054).  
1.2 Units—When values are stated in both SI and inch-pound units, the units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, use each system independently of the other. Combining values from the two systems may result in nonconformance with the standard. Several values are stated only in SI units as a matter of convention and to permit comparison of results. Included are the abrading media weight (grams), specimen weight (grams), specimen weight loss due to abrasion (grams), and the resultant volume loss (cubic centimeters).  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 Granular refractory materials may be either refractory grain raw materials that are used in the manufacture of finished refractory products, or bulk granular refractory materials that are sold, with or without some degree of processing, to refractory consumers for various uses. In either case, characterizing the properties of a granular refractory material is essential in evaluating its quality or consistency of quality and in determining suitability for end use. One of the important properties is bulk density because of its relationship to end product quality, usage, and performance.  
3.2 The refractories producer can use this test method as one of the quality control tests for his manufactured or mined refractory grain raw materials or for evaluating potential refractory grain raw materials.  
3.3 For the refractories consumer, the principal use of this test method is in the evaluation of the quality or the consistency of quality of the granular material in purchased refractory mixes or in bulk granular refractory materials used by the consumer.  
3.4 This is a primary test method, and thus is suitable for use in specifications, quality control, and research and development. It can also serve as a referee test method in purchasing contracts or agreements and as a base for development of more rapid, secondary test methods for use in quality control on manufactured refractory raw materials.  
3.5 Fundamental assumptions inherent in this test method are that the sample is representative of the material in general, the particle size of the sample is within the range specified by the test method, the material is not readily hydratable, and the size and quantity of pores in the material permits removal of surface water without drainage from the pores themselves. Deviation from any of these assumptions negates the usefulness of the test results.  
3.6 In interpreting the results of this test method, it must be recognized that the specific gravity of the materia...
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1.1 This test method covers a procedure for determining the bulk density of granular refractory materials, commercial products which usually have particles that are retained on a 0.265 in. (6.7 mm) or coarser sieve.  
Note 1: This test method is not suitable for materials that hydrate in boiling water.  
1.2 Units—The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.2.1 Exceptions—In Sections 4, 7, and 8, the apparatus used is only available in SI units.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 Insulating firebrick (IFB) are classified by their bulk density and reheat change (see Classification C155). This test method defines thermal stability by measurement of IFB's reheat change following 24 h at a test temperature.  
3.2 Since this test exposes the entire sample to an isothermal temperature condition, the user should be aware that most applications for IFB involve a thermal gradient which may cause the IFB's dimensions to change differentially.
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1.1 This test method covers the determination of the permanent linear (and volume) change of insulating firebrick upon reheating under prescribed conditions.  
1.2 The values stated in inch-pound units are to be regarded as the standard. The values given in parentheses are for information only.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
4.1 The true specific gravity of a material is the ratio of its true density, determined at a specific temperature, to the true density of water, determined at a specific temperature. Thus, the true specific gravity of a material is a primary property which is related to chemical and mineralogical composition.  
4.2 This test method is particularly useful for hydratable materials that are not suitable for test with Test Method C135.  
4.3 For refractory raw materials and products, the true specific gravity is a useful value for: classification, detecting differences in chemical composition between supposedly like samples, indicating mineralogical phases or phase changes, calculating total porosity when the bulk density is known, and for any other test method that requires this value for the calculation of results.  
4.4 This test method is a primary standard method which is suitable for use in specifications, quality control, and research and development. It can also serve as a referee test method in purchasing contracts or agreements.  
4.5 Fundamental assumptions inherent in this test method are the following:  
4.5.1 The sample is representative of the material in general,  
4.5.2 The total sample has been reduced to the particle size specified,  
4.5.3 No contamination has been introduced during processing of the sample,  
4.5.4 The ignition of the sample has eliminated all free or combined water without inducing sintering or alteration,  
4.5.5 An inert gas (helium) has been used in the test, and  
4.5.6 The test method has been conducted in a meticulous manner.  
4.5.7 Deviation from any of these assumptions negates the usefulness of the results.  
4.6 In interpreting the results of this test method, it must be recognized that the specified sample particle size is significantly finer than specified for Test Method C135. Even this finer particle size for the sample does not preclude the presence of some closed pores, and the amount of residual close...
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1.1 This test method covers the determination of the true specific gravity of solid materials, and is particularly useful for materials that easily hydrate which are not suitable for test with Test Method C135. This test method may be used as an alternate for Test Methods C135, C128, and C188 for determining true specific gravity.  
1.2 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.2.1 Exception—In 7.3, the equivalent SI unit is expressed in parentheses.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 Refractory brick are used as modular units in furnace construction and should not deviate significantly from the intended configuration with respect to size, bulk density, flat surfaces, and right angles. These test methods are particularly suited for use under field conditions and provide a means to determine whether the brick meets the requirements considered necessary to assure a satisfactory refractory construction.
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1.1 These test methods cover procedures for measuring size, dimensional measurement, bulk density, warpage, and squareness of rectangular dense refractory brick and rectangular insulating firebrick. More precise determination of bulk density of refractory brick can be made by Test Methods C20. Stack height is generally determined only for dense refractories.  
Note 1: Test Methods C830 and Test Method C914 are also used to determine bulk density of refractory brick, by different procedures.  
1.2 The test methods appear in the following order:    
Sections    
Size and Bulk Density  
4 through 7    
Warpage of Refractory Brick  
8 through 10    
Squareness of Refractory Brick  
11 through 14  
1.3 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
3.1 Apparent porosity, water absorption, apparent specific gravity, and bulk density are primary properties of refractory shapes. These properties are widely used in the evaluation and comparison of product quality and as part of the criteria for selection and use of refractory products in a variety of industrial applications. These test methods are used for determining any or all of these properties and are particularly useful for testing hydratable products.  
3.2 These test methods are primary standard methods that are suitable for use in quality control, research and development, establishing criteria for and evaluating compliance with specifications, and providing data for design purposes.  
3.3 Fundamental assumptions inherent in these test methods are:  
3.3.1 The test specimens conform to the requirements for size, configuration, and original faces,  
3.3.2 The open pores of the test specimens are fully impregnated with liquid during the vacuum-pressure treatment, and  
3.3.3 The blotting of the saturated test specimens is performed as specified in a consistent and uniform manner to avoid withdrawing liquid from the pores.  
3.3.4 Deviation from any of these assumptions adversely affects the test results.  
3.4 In laboratory studies involving castable specimen, a bias was noted between formed 2 × 2 × 2 in. (50 × 50 × 50 mm) and specimens quartered from larger 9 × 4.5 × 2.5 in. (228 × 114 × 64 mm) cast specimens. Additionally, an error in the apparent porosity determination was found on castables whenever the specimens were heated to 1500°F (816°C) and then exposed to water as a saturation media. The error was attributed to reactivity of cement with water and subsequent re-hydration of cement phases. The higher the cement level of the castable, the greater the error noted. It was concluded that an error in porosity values could occur for refractory materials having a potential to form hydrated species with water. Testing under the same conditions in ke...
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1.1 These test methods cover the determination of the following properties of refractory shapes:  
1.1.1 Apparent porosity,  
1.1.2 Liquid absorption,  
1.1.3 Apparent specific gravity, and  
1.1.4 Bulk density.  
1.2 These test methods are applicable to all refractory shapes except those that chemically react with both water and mineral spirits. When testing a material capable of hydration or other chemical reaction with water but which does not chemically react with mineral spirits, mineral spirits is substituted for water and appropriate corrections for the density differences are applied when making calculations.  
1.3 Units—The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.3.1 Exception—The apparatus used in this standard is only available in SI units.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
Note 1: Test Methods C20 cover procedures for testing properties of refractories that are not attacked by water.

SIGNIFICANCE AND USE
3.1 Fireclay steel-teeming nozzles and sleeves are classified by volume reheat change. Bloating of some refractories results in irregular reheat dimensions, which are difficult to measure. This practice determines the volume without depending upon physical linear measurements.  
3.2 Blast furnace checkers that have irregular cross-sections are classified by “creep properties.” This practice determines the average cross-sectional area without requiring area measurements.
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1.1 This practice covers the methods of calculating areas, volumes, and linear changes of irregularly shaped refractory specimens.  
1.2 Areas of irregular (both conventional and shaped) specimens are required for determining the creep of certain refractory products.  
1.3 Linear and volume changes or irregularly shaped refractories are required for determining reheat change.  
1.4 The values stated in SI units are to be regarded as the standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
3.1 Granular refractory materials may be either refractory grain raw materials that are used in the manufacture of finished refractory products, or bulk granular refractory materials that are sold, with or without some degree of processing, to refractory consumers for various uses. In either case, characterizing the properties of a granular refractory material is essential in evaluating its quality or consistency of quality and in determining suitability for end use. One of the important properties is bulk density because of its relationship to end product quality, usage, and performance.  
3.2 The refractories producer can use this test method as one of the quality-control tests for his manufactured or mined refractory grain raw materials or for evaluating potential refractory grain raw materials.  
3.3 For the refractories consumer, the principal use of this test method is in the evaluation of the quality or the consistency of quality of the granular material in purchased refractory mixes or in bulk granular refractory materials used by the consumer.  
3.4 This is a primary test method, and thus is suitable for use in specifications, quality control, and research and development. It can also serve as a referee test method in purchasing contracts or agreements and as a base for development of more rapid, secondary test methods for use in quality control on manufactured refractory raw materials.  
3.5 Fundamental assumptions inherent in this test method are that the sample is representative of the material in general, the particle size of the sample is within the range specified by the test method, the material is not readily hydratable, and the size and quantity of pores in the material permits removal of surface water without drainage from the pores themselves. Deviation from any of these assumptions negates the usefulness of the test results.  
3.6 In interpreting the results of this test method, it must be recognized that the specific gravity of the materia...
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1.1 This test method covers a procedure for determining the bulk density of granular refractory materials, commercial products which usually have particles that are retained on a 0.265-in. (6.7-mm) or coarser sieve.  
Note 1: This test method is not suitable for materials that hydrate in boiling water.  
1.2 Units—The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.2.1 Exceptions—In Sections 4, 7, and 8, the apparatus used is only available in SI units.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
4.1 This test method measures the relative abrasion resistance of various refractory samples under standard conditions at room temperature.  
4.2 The abrasion resistance of a refractory material provides an indication of its suitability for service in abrasive environments.  
4.3 The results obtained by this test method could be different than those obtained in service because of the different conditions encountered.
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1.1 This test method covers the determination of relative abrasion resistance of refractory brick at room temperature. This test method can also be applied to castable refractories (see Metric Dimensions, Practice C861 and Practice C865) and plastic refractories (see Practice C1054).  
1.2 Units—When values are stated in both SI and inch-pound units, the units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, use each system independently of the other. Combining values from the two systems may result in nonconformance with the standard. Several values are stated only in SI units as a matter of convention and to permit comparison of results. Included are the abrading media weight (grams), specimen weight (grams), specimen weight loss due to abrasion (grams), and the resultant volume loss (cubic centimeters).  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
4.1 This test method measures the relative abrasion resistance of various refractory samples under standard conditions at room temperature.  
4.2 The abrasion resistance of a refractory material provides an indication of its suitability for service in abrasive environments.  
4.3 The results obtained by this test method could be different than those obtained in service because of the different conditions encountered.
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1.1 This test method covers the determination of relative abrasion resistance of refractory brick at room temperature. This test method can also be applied to castable refractories (see Metric Dimensions, Practice C861 and Practice C865) and plastic refractories (see Practice C1054).  
1.2 Units—When values are stated in both SI and inch-pound units, the units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, use each system independently of the other. Combining values from the two systems may result in non-conformance with the standard. Several values are stated only in SI units as a matter of convention and to permit comparison of results. Included are the abrading media weight (grams), specimen weight (grams), specimen weight loss due to abrasion (grams), and the resultant volume loss (cubic centimeters).  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
3.1 The true specific gravity of a material is the ratio of its true density, determined at a specific temperature, to the true density of water, determined at a specific temperature. Thus, the true specific gravity of a material is a primary property which is related to chemical and mineralogical composition.  
3.2 For refractory raw materials and products the true specific gravity is a useful value for: classification, detecting differences in chemical composition between supposedly like samples, indicating mineralogical phases or phase changes, calculating total porosity when the bulk density is known, and for any other test method which requires this value for the calculation of results.  
3.3 This test method is a primary standard method which is suitable for use in specifications, quality control, and research and development. It can also serve as a referee test method in purchasing contracts or agreements.  
3.4 Fundamental assumptions inherent in this test method are the following:  
3.4.1 The sample is representative of the material in general,  
3.4.2 The total sample has been reduced to the particle size specified,  
3.4.3 No impurity has been introduced during processing of the sample,  
3.4.4 The sample itself is not magnetic and all magnetic material introduced during processing of the sample has been removed,  
3.4.5 The material is not hydratable or reactive with water, and  
3.4.6 The test method has been conducted in a meticulous manner.  
3.4.7 Deviation from any of these assumptions negates the usefulness of the results.  
3.5 In interpreting the results of this test method it must be recognized that the specified sample particle size does not guarantee that all closed pores have been eliminated. The amount of residual closed pores may vary between materials or even between samples of the same or like materials, and the specified sample particle size is not the same as that specified for Test Method C604. The values generated by this ...
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1.1 This test method covers the determination of true specific gravity of refractory materials under prescribed conditions. It is not applicable to materials attacked by water.  
1.2 Units—The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.2.1 Exception—The equipment used in this standard for weights and volumes is only available in SI units.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
3.1 Apparent porosity, water absorption, apparent specific gravity, and bulk density are primary properties of burned refractory brick and shapes. These properties are widely used in the evaluation and comparison of product quality and as part of the criteria for selection and use of refractory products in a variety of industrial applications. These test methods are used for determining any or all of these properties.  
3.2 These test methods are primary standard methods which are suitable for use in quality control, research and development, establishing criteria for and evaluating compliance with specifications, and providing data for design purposes.  
3.3 Fundamental assumptions inherent in these test methods are that the test specimens are not attacked by water, the test specimens conform to the requirements for size, configuration, and original faces, the open pores of the test specimens are fully impregnated with water during the boiling treatment, and the blotting of the saturated test specimens is performed as specified in a consistent and uniform manner to avoid withdrawing water from the pores. Deviation from any of these assumptions adversely affects the test results.  
3.4 In laboratory studies involving castable specimen, a bias was noted between formed 2 by 2 by 2–in. (50 by 50 by 50–mm) and specimens that were quartered from larger 9 by 4.5 by 2.5 (228 by 114 by 64 mm) cast specimens. Additionally, an error in the apparent porosity determination on castables was found whenever the specimens were heated to 1500°F (816°C) and then exposed to water as a saturation media (Test Method C830). The error was attributed to reactivity of cement with water and subsequent re-hydration of cement phases. The higher the cement level of the castable, the greater the error noted. It was concluded that an error in porosity values could occur for refractory materials having a potential to form hydrated species with water.3  
3.5 Certain precautions must be exercis...
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1.1 These test methods cover the determination of the following properties of burned refractory brick:  
1.1.1 Apparent porosity,  
1.1.2 Water absorption,  
1.1.3 Apparent specific gravity, and  
1.1.4 Bulk density.  
1.2 These test methods are not applicable to refractories attacked by water.  
1.3 The values stated in inch-pound units are to be regarded as the standard. The values given in parentheses are for information only.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
2.1 This test method may be used to quickly determine volume and bulk density of a refractory of any shape, provided it has sufficient structural integrity to permit handling. Thus it may be used on unfired or fired, strong or friable shapes.  
2.2 Since the test may be performed quickly, it has found application as manufacturing in-process control as well as in characterizing finished refractory products. Also it may be used to examine specimens after other test or service exposure.
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1.1 This test method covers the basic procedure for determining bulk density and volume of refractory shapes. This test is applicable to all refractory shapes or monoliths, burned or unburned, independent of composition or forming method, including materials that slake and hydrate. It is particularly suitable for determining bulk density and volume of complex shapes after forming, since results may be obtained in a matter of minutes.  
1.2 Units—The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.2.1 Exception—The balance used in this standard is only available in SI units (Sections 3 – 6).  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For a specific hazard statement, see Note 2.

SIGNIFICANCE AND USE
3.1 Particle size distribution has a major affect upon most of the refractory properties. These test methods provide a means of measuring the distribution for the purpose of comparison to the desired distribution.  
3.2 These test methods also cover determination of the water content of refractory materials in the wet condition and of air-dried samples received, so that the sieve analysis can be calculated on the dry basis.  
3.3 These methods can produce data for specification acceptance, design purposes, manufacturing control, and research and development.  
3.4 A reference set of standard matched or calibrated sieves4 shall be provided for use in checking the set of sieves used in the actual sieve analysis of samples. The sieves for use in sieve analysis may also be standard matched sieves or may be unmatched sieves conforming to the Specification Table in Specification E11, provided that such sieves will give results that differ by no more than 5 % from those obtained with the reference set when the two sets are compared in accordance with the section of Test Method C429 on testing of sieves and samples splitters.
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1.1 These test methods cover a wet and a dry method for sieve analysis of refractory materials.  
1.1.1 Wet Sieve Analysis—Water promotes the slaking of clays and helps to separate fine particles, washing them from the larger grains. This method is recommended for use with materials that require water addition, and that slake in normal industrial use.  
1.1.2 Dry Sieve Analysis—The dry method is not as effective as the wet method in determining the amount of material present in the smaller particle sizes. It is recommended (1) for clays, when the slaking action of water is undesirable, (2) when the material is in the form of coarsely ground grog and calcine, and (3) when the clay is to be used in such a way that the ultimate particle size is of secondary importance.  
1.2 These test methods also cover determination of the water content of refractory materials in the wet condition and of air-dried samples as received, so that the sieve analysis can be calculated on the dry basis. Included is a method for obtaining the water content of other refractory materials, such as plastic refractories and wet mixes.  
1.3 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
3.1 Insulating firebrick (IFB) are classified by their bulk density and reheat change (see Classification C155). This test method defines thermal stability by measurement of IFB's reheat change following 24 h at a test temperature.  
3.2 Since this test exposes the entire sample to an isothermal temperature condition, the user should be aware that most applications for IFB involve a thermal gradient which may cause the IFB's dimensions to change differentially.
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1.1 This test method covers the determination of the permanent linear (and volume) change of insulating firebrick upon reheating under prescribed conditions.  
1.2 The values stated in inch-pound units are to be regarded as the standard. The values given in parentheses are for information only.  
1.3  This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
3.1 Refractory brick and shapes of different compositions exhibit unique permanent linear changes after heating or reheating. This test method provides a standard procedure for heating various classes of refractories with appropriate heating schedules.  
3.2 Linear reheat changes obtained by this test method are suitable for use in research and development, also often used to establish written specifications between producers and consumers.  
3.3 Care should be exercised in selecting samples that are representative of the product being tested and that the schedule selected is appropriate to the product.
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1.1 This test method covers the determination of the permanent linear change of refractory brick when heated under prescribed conditions.  
1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard. Note 1—Test methods incorporating additional provisions pertinent to specific refractory materials are given in the following Test Methods: C C179179, C C210210, and C C605605.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
4.1 This test method measures the relative abrasion resistance of various refractory samples under standard conditions at room temperature.  
4.2 The abrasion resistance of a refractory material provides an indication of its suitability for service in abrasive environments.  
4.3 The results obtained by this test method could be different than those obtained in service because of the different conditions encountered.
SCOPE
1.1 This test method covers the determination of relative abrasion resistance of refractory brick at room temperature. This test method can also be applied to castable refractories (see Metric Dimensions, Practice C861 and Practice C865) and plastic refractories (see Practice C1054).  
1.2 Units—When values are stated in both SI and inch-pound units, the units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, use each system independently of the other. Combining values from the two systems may result in non-conformance with the standard. Several values are stated only in SI units as a matter of convention and to permit comparison of results. Included are the abrading media weight (grams), specimen weight (grams), specimen weight loss due to abrasion (grams), and the resultant volume loss (cubic centimeters).  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
3.1 This test method is used to measure the rate of flow of air or nitrogen through refractory brick and monoliths and to thus determine the permeability of tested products.  
3.2 This test method is useful in research and development for establishing the relative permeability of products within comparable classes. It may also be used to identify acceptable products for design purposes and to establish permeability criteria for specification acceptance.  
3.3 It must be recognized that permeability can vary in different directions and different parts of a refractory due to factors such as forming procedure, grain size and distribution, and heat treatment.
SCOPE
1.1 This test method covers determination of the permeability of refractory brick and monoliths, from which suitable specimens can be cut, at room temperature.  
1.2 Units—The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.2.1 Exceptions—The apparatus used in this standard is only available in SI units (Section 4). Also, some of the calculations must use SI units only.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
4.1 The true specific gravity of a material is the ratio of its true density, determined at a specific temperature, to the true density of water, determined at a specific temperature. Thus, the true specific gravity of a material is a primary property which is related to chemical and mineralogical composition.  
4.2 This test method is particularly useful for hydratable materials which are not suitable for test with Test Method C135.  
4.3 For refractory raw materials and products the true specific gravity is a useful value for: classification, detecting differences in chemical composition between supposedly like samples, indicating mineralogical phases or phase changes, calculating total porosity when the bulk density is known, and for any other test method that requires this value for the calculation of results.  
4.4 This test method is a primary standard method which is suitable for use in specifications, quality control, and research and development. It can also serve as a referee test method in purchasing contracts or agreements.  
4.5 Fundamental assumptions inherent in this test method are the following:  
4.5.1 The sample is representative of the material in general,  
4.5.2 The total sample has been reduced to the particle size specified,  
4.5.3 No contamination has been introduced during processing of the sample,  
4.5.4 The ignition of the sample has eliminated all free or combined water without inducing sintering or alteration,  
4.5.5 An inert gas (helium) has been used in the test, and  
4.5.6 The test method has been conducted in a meticulous manner.  
4.5.7 Deviation from any of these assumptions negates the usefulness of the results.  
4.6 In interpreting the results of this test method it must be recognized that the specified sample particle size is significantly finer than specified for Test Method C135. Even this finer particle size for the sample does not preclude the presence of some closed pores, and the amount of res...
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1.1 This test method covers the determination of the true specific gravity of solid materials, and is particularly useful for materials that easily hydrate which are not suitable for test with Test Method C135. This test method may be used as an alternate for Test Method C135, Test Method C128, and Test Method C188 for determining true specific gravity.  
1.2 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.2.1 Exception—In 7.3 the equivalent SI unit is expressed in parenthesis.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
This test method measures the relative abrasion resistance of various refractory samples under standard conditions at room temperature.  
The abrasion resistance of a refractory material provides an indication of its suitability for service in abrasive environments.  
The results obtained by this test method could be different than those obtained in service because of the different conditions encountered.
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1.1 This test method covers the determination of relative abrasion resistance of refractory brick at room temperature. This test method can also be applied to castable refractories (see Metric Dimensions, Practice C861 and Practice C865) and plastic refractories (see Practice C1054).
1.2 Units—When values are stated in both SI and inch-pound units, the units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, use each system independently of the other. Combining values from the two systems may result in non-conformance with the standard. Several values are stated only in SI units as a matter of convention and to permit comparison of results. Included are the abrading media weight (grams), specimen weight (grams), specimen weight loss due to abrasion (grams), and the resultant volume loss (cubic centimeters).
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
Apparent porosity, water absorption, apparent specific gravity, and bulk density are primary properties of refractory shapes. These properties are widely used in the evaluation and comparison of product quality and as part of the criteria for selection and use of refractory products in a variety of industrial applications. These test methods are used for determining any or all of these properties and are particularly useful for testing hydratable products.
These test methods are primary standard methods that are suitable for use in quality control, research and development, establishing criteria for and evaluating compliance with specifications, and providing data for design purposes.
Fundamental assumptions inherent in these test methods are:
The test specimens conform to the requirements for size, configuration, and original faces,
The open pores of the test specimens are fully impregnated with liquid during the vacuum-pressure treatment, and
The blotting of the saturated test specimens is performed as specified in a consistent and uniform manner to avoid withdrawing liquid from the pores.
Deviation from any of these assumptions adversely affects the test results.
In laboratory studies involving castable specimen, a bias was noted between formed 2 × 2 × 2 in. (50 × 50 × 50 mm) and specimens quartered from larger 9 × 4.5 × 2.5 in. (228 × 114 × 64 mm) cast specimens. Additionally, an error in the apparent porosity determination was found on castables whenever the specimens were heated to 1500°F (816°C) and then exposed to water as a saturation media. The error was attributed to reactivity of cement with water and subsequent re-hydration of cement phases. The higher the cement level of the castable, the greater the error noted. It was concluded that an error in porosity values could occur for refractory materials having a potential to form hydrated species with water. Testing under the same conditions in kerosene produced results that were believed to b...
SCOPE
1.1 These test methods cover the determination of the following properties of refractory shapes:
1.1.1 Apparent porosity,
1.1.2 Liquid absorption,
1.1.3 Apparent specific gravity, and
1.1.4 Bulk density.
1.2 These test methods are applicable to all refractory shapes except those that chemically react with both water and mineral spirits. When testing a material capable of hydration or other chemical reaction with water but which does not chemically react with mineral spirits, mineral spirits is substituted for water and appropriate corrections for the density differences are applied when making calculations.
1.3 Units—The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.
1.3.1 Exception—The apparatus used in this standard is only available in SI units.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
Note 1—Test Methods C20 cover procedures for testing properties of refractories that are not attacked by water.

SIGNIFICANCE AND USE
Fireclay steel-teeming nozzles and sleeves are classified by volume reheat change. Bloating of some refractories results in irregular reheat dimensions, which are difficult to measure. This practice determines the volume without depending upon physical linear measurements.
Blast furnace checkers that have irregular cross-sections are classified by “creep properties.” This practice determines the average cross-sectional area without requiring area measurements.
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1.1 This practice covers the methods of calculating areas, volumes, and linear changes of irregularly shaped refractory specimens.
1.2 Areas of irregular (both conventional and shaped) specimens are required for determining the creep of certain refractory products.
1.3 Linear and volume changes or irregularly shaped refractories are required for determining reheat change.
1.4 The values stated in SI units are to be regarded as the standard.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
Particle size distribution has a major affect upon most of the refractory properties. These test methods provide a means of measuring the distribution for the purpose of comparison to the desired distribution.  
These test methods also cover determination of the water content of refractory materials in the wet condition and of air-dried samples received, so that the sieve analysis can be calculated on the dry basis.
These methods can produce data for specification acceptance, design purposes, manufacturing control, and research and development.  
A reference set of standard matched or calibrated sieves shall be provided for use in checking the set of sieves used in the actual sieve analysis of samples. The sieves for use in sieve analysis may also be standard matched sieves or may be unmatched sieves conforming to the Specification Table in Specification E11, provided that such sieves will give results that differ by no more than 5 % from those obtained with the reference set when the two sets are compared in accordance with the section of Test Method C429 on testing of sieves and samples splitters.
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1.1 These test methods cover a wet and a dry method for sieve analysis of refractory materials.  
1.1.1 Wet Sieve Analysis—Water promotes the slaking of clays and helps to separate fine particles, washing them from the larger grains. This method is recommended for use with materials that require water addition, and that slake in normal industrial use.  
1.1.2 Dry Sieve Analysis—The dry method is not as effective as the wet method in determining the amount of material present in the smaller particle sizes. It is recommended (1) for clays, when the slaking action of water is undesirable, (2) when the material is in the form of coarsely ground grog and calcine, and (3) when the clay is to be used in such a way that the ultimate particle size is of secondary importance.  
1.2 These test methods also cover determination of the water content of refractory materials in the wet condition and of air-dried samples as received, so that the sieve analysis can be calculated on the dry basis. Included is a method for obtaining the water content of other refractory materials, such as plastic refractories and wet mixes.  
1.3 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
Refractory brick are used as modular units in furnace construction and should not deviate significantly from the intended configuration with respect to size, bulk density, flat surfaces, and right angles. These test methods are particularly suited for use under field conditions and provide a means to determine whether the brick meets the requirements considered necessary to assure a satisfactory refractory construction.
SCOPE
1.1 These test methods cover procedures for measuring size, dimensional measurement, bulk density, warpage, and squareness of rectangular dense refractory brick and rectangular insulating firebrick. More precise determination of bulk density of refractory brick can be made by Test Methods C20. Stack height is generally determined only for dense refractories.
Note 1—Test Methods C830 and Test Method C914 are also used to determine bulk density of refractory brick, by different procedures.

SIGNIFICANCE AND USE
Apparent porosity, water absorption, apparent specific gravity, and bulk density are primary properties of burned refractory brick and shapes. These properties are widely used in the evaluation and comparison of product quality and as part of the criteria for selection and use of refractory products in a variety of industrial applications. These test methods are used for determining any or all of these properties.  
These test methods are primary standard methods which are suitable for use in quality control, research and development, establishing criteria for and evaluating compliance with specifications, and providing data for design purposes.  
Fundamental assumptions inherent in these test methods are that the test specimens are not attacked by water, the test specimens conform to the requirements for size, configuration, and original faces, the open pores of the test specimens are fully impregnated with water during the boiling treatment, and the blotting of the saturated test specimens is performed as specified in a consistent and uniform manner to avoid withdrawing water from the pores. Deviation from any of these assumptions adversely affects the test results.  
In laboratory studies involving castable specimen, a bias was noted between formed 2 by 2 by 2–in. (50 by 50 by 50–mm) and specimens that were quartered from larger 9 by 4.5 by 2.5 (228 by 114 by 64 mm) cast specimens. Additionally, an error in the apparent porosity determination on castables was found whenever the specimens were heated to 1500°F (816°C) and then exposed to water as a saturation media (Test Method C830). The error was attributed to reactivity of cement with water and subsequent re-hydration of cement phases. The higher the cement level of the castable, the greater the error noted. It was concluded that an error in porosity values could occur for refractory materials having a potential to form hydrated species with water.  
Certain precautions must be exercised in interpreting and...
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1.1 These test methods cover the determination of the following properties of burned refractory brick:  
1.1.1 Apparent porosity,  
1.1.2 Water absorption,  
1.1.3 Apparent specific gravity, and  
1.1.4 Bulk density.  
1.2 These test methods are not applicable to refractories attacked by water.  
1.3 The values stated in inch-pound units are to be regarded as the standard. The values given in parentheses are for information only.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
This test method may be used to quickly determine volume and bulk density of a refractory of any shape, provided it has sufficient structural integrity to permit handling. Thus it may be used on unfired or fired, strong or friable shapes.  
Since the test may be performed quickly, it has found application as manufacturing in-process control as well as in characterizing finished refractory products. Also it may be used to examine specimens after other test or service exposure.
SCOPE
1.1 This test method covers the basic procedure for determining bulk density and volume of refractory shapes. This test is applicable to all refractory shapes or monoliths, burned or unburned, independent of composition or forming method, including materials that slake and hydrate. It is particularly suitable for determining bulk density and volume of complex shapes after forming, since results may be obtained in a matter of minutes.  
1.2 Units—The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.
1.2.1 Exception—The balance used in this standard is only available in SI units (Sections 3-6).
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For a specific hazard statement, see Note 2.

SIGNIFICANCE AND USE
This test method measures the relative abrasion resistance of various refractory samples under standard conditions at room temperature.
The abrasion resistance of a refractory material provides an indication of its suitability for service in abrasion or erosive environments.
The results obtained by this test method could be different than those obtained in service because of the different conditions encountered.
SCOPE
1.1 This test method covers the determination of relative abrasion resistance of refractory brick at room temperature. This test method can also be applied to castable refractories (see Metric Dimensions, Practice C 861 and Practice C 865) and plastic refractories (see Practice C 1054).
1.2 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
Granular refractory materials may be either refractory grain raw materials that are used in the manufacture of finished refractory products, or bulk granular refractory materials that are sold, with or without some degree of processing, to refractory consumers for various uses. In either case, characterizing the properties of a granular refractory material is essential in evaluating its quality or consistency of quality and in determining suitability for end use. One of the important properties is bulk density because of its relationship to end product quality, usage, and performance.
The refractories producer can use this test method as one of the quality-control tests for his manufactured or mined refractory grain raw materials or for evaluating potential refractory grain raw materials.  
For the refractories consumer, the principal use of this test method is in the evaluation of the quality or the consistency of quality of the granular material in purchased refractory mixes or in bulk granular refractory materials used by the consumer.  
This is a primary test method, and thus is suitable for use in specifications, quality control, and research and development. It can also serve as a referee test method in purchasing contracts or agreements and as a base for development of more rapid, secondary test methods for use in quality control on manufactured refractory raw materials.  
Fundamental assumptions inherent in this test method are that the sample is representative of the material in general, the particle size of the sample is within the range specified by the test method, the material is not readily hydratable, and the size and quantity of pores in the material permits removal of surface water without drainage from the pores themselves. Deviation from any of these assumptions negates the usefulness of the test results.  
In interpreting the results of this test method, it must be recognized that the specific gravity of the material as well as the porosity...
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1.1 This test method covers a procedure for determining the bulk density of granular refractory materials, commercial products which usually have particles that are retained on a 0.265-in. (6.7-mm) or coarser sieve.
Note 1—This test method is not suitable for materials that hydrate in boiling water.  
1.2 Units—The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.
1.2.1 Exceptions—In Sections 4, 7, and 8, the apparatus used is only available in SI units.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
The true specific gravity of a material is the ratio of its true density, determined at a specific temperature, to the true density of water, determined at a specific temperature. Thus, the true specific gravity of a material is a primary property which is related to chemical and mineralogical composition.  
For refractory raw materials and products the true specific gravity is a useful value for: classification, detecting differences in chemical composition between supposedly like samples, indicating mineralogical phases or phase changes, calculating total porosity when the bulk density is known, and for any other test method which requires this value for the calculation of results.  
This test method is a primary standard method which is suitable for use in specifications, quality control, and research and development. It can also serve as a referee test method in purchasing contracts or agreements.  
Fundamental assumptions inherent in this test method are the following:  
The sample is representative of the material in general,  
The total sample has been reduced to the particle size specified,  
No impurity has been introduced during processing of the sample,  
The sample itself is not magnetic and all magnetic material introduced during processing of the sample has been removed,  
The material is not hydratable or reactive with water, and  
The test method has been conducted in a meticulous manner.  
Deviation from any of these assumptions negates the usefulness of the results.  
In interpreting the results of this test method it must be recognized that the specified sample particle size does not guarantee that all closed pores have been eliminated. The amount of residual closed pores may vary between materials or even between samples of the same or like materials, and the specified sample particle size is not the same as that specified for Test Method C 604. The values generated by this test method may, therefore, be close approximations rather tha...
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1.1 This test method covers the determination of true specific gravity of refractory materials under prescribed conditions. It is not applicable to materials attacked by water.  
1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.
1.2.1 Exception—The equipment used in this standard for weights and volumes is only available in SI units.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
This test method measures the relative abrasion resistance of various refractory samples under standard conditions at room temperature.
The abrasion resistance of a refractory material provides an indication of its suitability for service in abrasion or erosive environments.
The results obtained by this test method could be different than those obtained in service because of the different conditions encountered.
SCOPE
1.1 This test method covers the determination of relative abrasion resistance of refractory brick at room temperature. This test method can also be applied to castable refractories (see Metric Dimensions, Practice C 861 and Practice C 865) and plastic refractories (see Practice C 1054).
1.2 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
Refractory brick and shapes of different compositions exhibit unique permanent linear changes after heating or reheating. This test method provides a standard procedure for heating various classes of refractories with appropriate heating schedules.  
Linear reheat changes obtained by this test method are suitable for use in research and development, also often used to establish written specifications between producers and consumers.  
Care should be exercised in selecting samples that are representative of the product being tested and that the schedule selected is appropriate to the product.
SCOPE
1.1 This test method covers the determination of the permanent linear change of refractory brick when heated under prescribed conditions.  
1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.
Note 1—Test methods incorporating additional provisions pertinent to specific refractory materials are given in the following Test Methods: C 179, C 210, and C 605.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SCOPE
1.1 This test method covers the determination of relative abrasion resistance of refractory brick at room temperature. This test method can also be applied to castable refractories (see Metric Dimensions, Practice C 861 and Practice C 865) and plastic refractories (see Practice C 1054).
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are provided for information only.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
Granular refractory materials may be either refractory grain raw materials that are used in the manufacture of finished refractory products, or bulk granular refractory materials that are sold, with or without some degree of processing, to refractory consumers for various uses. In either case, characterizing the properties of a granular refractory material is essential in evaluating its quality or consistency of quality and in determining suitability for end use. One of the important properties is bulk density because of its relationship to end product quality, usage, and performance.
The refractories producer can use this test method as one of the quality-control tests for his manufactured or mined refractory grain raw materials or for evaluating potential refractory grain raw materials.  
For the refractories consumer, the principal use of this test method is in the evaluation of the quality or the consistency of quality of the granular material in purchased refractory mixes or in bulk granular refractory materials used by the consumer.  
This is a primary test method, and thus is suitable for use in specifications, quality control, and research and development. It can also serve as a referee test method in purchasing contracts or agreements and as a base for development of more rapid, secondary test methods for use in quality control on manufactured refractory raw materials.  
Fundamental assumptions inherent in this test method are that the sample is representative of the material in general, the particle size of the sample is within the range specified by the test method, the material is not readily hydratable, and the size and quantity of pores in the material permits removal of surface water without drainage from the pores themselves. Deviation from any of these assumptions negates the usefulness of the test results.  
In interpreting the results of this test method, it must be recognized that the specific gravity of the material as well as the porosity...
SCOPE
1.1 This test method covers a procedure for determining the bulk density of granular refractory materials, commercial products which usually have particles that are retained on a 0.265-in. (6.7-mm) or coarser sieve.
Note 1—This test method is not suitable for materials that hydrate in boiling water.
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
This test method is used to measure the rate of flow of air or nitrogen through refractory brick and monoliths and to thus determine the permeability of tested products.  
This test method is useful in research and development for establishing the relative permeability of products within comparable classes. It may also be used to identify acceptable products for design purposes and to establish permeability criteria for specification acceptance.  
It must be recognized that permeability can vary in different directions and different parts of a refractory due to factors such as forming procedure, grain size and distribution, and heat treatment.
SCOPE
1.1 This test method covers determination of the permeability of refractory brick and monoliths, from which suitable specimens can be cut, at room temperature.  
1.2 Units—The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.
1.2.1 Exceptions—The apparatus used in this standard is only available in SI units (Section 4). Also, some of the calculations must use SI units only.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

SIGNIFICANCE AND USE
This test method is used to measure the rate of flow of air or nitrogen through refractory brick and monoliths and to thus determine the permeability of tested products.  
This test method is useful in research and development for establishing the relative permeability of products within comparable classes. It may also be used to identify acceptable products for design purposes and to establish permeability criteria for specification acceptance.  
It must be recognized that permeability can vary in different directions and different parts of a refractory due to factors such as forming procedure, grain size and distribution, and heat treatment.
SCOPE
1.1 This test method covers determination of the permeability of refractory brick and monoliths, from which suitable specimens can be cut, at room temperature.
This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.