C08 - Refractories

SIGNIFICANCE AND USE
3.1 Insulating firebrick (IFB) are classified by their bulk density and reheat change (see Classification C155). This test method defines thermal stability by measurement of IFB's reheat change following 24 h at a test temperature.  
3.2 Since this test exposes the entire sample to an isothermal temperature condition, the user should be aware that most applications for IFB involve a thermal gradient which may cause the IFB's dimensions to change differentially.
SCOPE
1.1 This test method covers the determination of the permanent linear (and volume) change of insulating firebrick upon reheating under prescribed conditions.  
1.2 The values stated in inch-pound units are to be regarded as the standard. The values given in parentheses are for information only.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 The cold strength of a refractory material is an indication of its suitability for use in refractory construction. (It is not a measure of performance at elevated temperatures.)  
3.2 These test methods are for determining the room temperature flexural strength in three-point bending (cold modulus of rupture) or compressive strength (cold crushing strength), or both, for all refractory products.  
3.3 Considerable care must be used to compare the results of different determinations of the cold crushing strength or modulus of rupture. The specimen size and shape, the nature of the specimen faces (that is, as-formed, sawed, or ground), the orientation of those faces during testing, the loading geometry, and the rate of load application may all significantly affect the numerical results obtained. Comparisons of the results between different determinations should not be made if one or more of these parameters differ between the two determinations.  
3.4 The relative ratio of the largest grain size to the smallest specimen dimension may significantly affect the numerical results. For example, smaller cut specimens containing large grains may present different results than the bricks from which they were cut. Under no circumstances should 6 in. by 1 in. by 1 in. (152 mm by 25 mm by 25 mm) specimens be prepared and tested for materials containing grains with a maximum grain dimension exceeding 0.25 in. (6.4 mm).  
3.5 This test method is useful for research and development, engineering application and design, manufacturing process control, and for developing purchasing specifications.
SCOPE
1.1 These test methods cover the determination of the cold crushing strength and the modulus of rupture (MOR) of dried or fired refractory shapes of all types.  
1.2 The test methods appear in the following sections:    
Test Method  
Sections    
Cold Crushing Strength  
4 to 8  
Modulus of Rupture  
9 to 13  
1.3 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 This test method determines relative hydration resistance of magnesia grain.  
3.2 This test method is used in industry to evaluate grain samples and is used for specification purposes in some cases.  
3.3 Care must be taken in interpreting the data.
SCOPE
1.1 This test method covers the measurement of the relative resistance of magnesia grain to hydration.  
1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 These test methods are designed for use with carbon-containing products. The residual carbon content of a coked carbon-containing brick or shape is an indication of how much carbon may be available, in service, to resist slag attack on, or oxidation loss of, that body. Apparent carbon yield gives an estimate of the relative efficiency of the total carbonaceous matter to be retained as residual carbon.  
3.2 Residual carbon has a direct bearing on several properties of a pitch or resin-containing refractory, such as ignited porosity, density, strength, and thermal conductivity.  
3.3 These test methods are suitable for product development, manufacturing control, and specification acceptance.  
3.4 These test methods are very sensitive to specimen size, coking rates, etc.; therefore, strict compliance with these test methods is critical.  
3.5 Appreciable amounts of reducible components, such as Fe2O3, will have a noticeable effect on the results. Thus, values obtained by these test methods will be different when brick removed from service is tested. This must be kept in mind when attempting to use these test methods in an absolute sense.  
3.6 Oxidizable components such as metals and carbides can have a noticeable effect on the results. This must be kept in mind when using the second procedure, which is based on measuring weight loss after igniting the coked specimens.  
3.7 Testing of brick or shapes that contain magnesium metal presents special problems since this metal is highly volatile and substantial amounts of the magnesium can be lost from the sample during the coking procedure. This must be kept in mind when interpreting the results of testing of brick that contains magnesium. In addition, magnesium can react readily with atmospheric humidity. This must be kept in mind when storing brick that contains magnesium.
SCOPE
1.1 These test methods cover the determination of residual carbon content in carbon-bearing brick and shapes after a prescribed coking treatment. They provide two procedures. The first procedure is based on the combustion of carbon and its measurement as carbon dioxide. However, when using the first procedure for articles that contain silicon carbide or other carbides, no distinction will be made between carbon present in the form of a carbide and carbon present as elemental carbon. The second procedure provides a method for calculating apparent residual carbon (on the basis of weight loss after igniting the coked specimens), apparent carbonaceous material content, and apparent carbon yield. If the second procedure is used for brick or shapes that contain metallic additives or carbides, it must be recognized that there will be a weight gain associated with the oxidation of the metals, or carbides, or both. Such a weight gain can change the results substantially, and this must be kept in mind when interpreting the data.  
1.2 The values stated in inch-pound units are to be regarded as the standard. The values given in parentheses are for information only.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 The hydration of dead-burned dolomite grains is an important aspect of both manufacturing and using such grains. Moisture from any source will cause the grains to partially disintegrate, eventually making the dead-burned dolomite unfit for use. This test method may prove useful for determining, in a relative manner, which grains are more resistant to hydration than others.  
3.2 Data from one laboratory might help in establishing internal limits for determining whether a particular batch of grain is suitable for refractory production. However, this test method takes great care to run, and is not recommended as a quality control test. Possibly, a specification might be developed between two parties if sufficient care in establishing the bias between the laboratories is carried out.
SCOPE
1.1 This test method covers the determination of the amount of hydration of a granular dead-burned refractory dolomite when exposed to moist air.  
1.2 The values stated in inch-pound units are to be regarded as the standard. The values given in parentheses are for information only.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
2.1 This test method compares relative resistance to hydration of basic refractory brick and shapes in laboratory tests.  
2.2 This test method allows an estimate to be made of the relative potential for hydration.  
2.3 The test method is used in industry and in some cases it is used for specification purposes.  
2.4 The results must be carefully used as a means of predicting whether or not basic brick or shapes will hydrate under actual conditions of storage or service.
SCOPE
1.1 This test method covers measurement of the relative resistance of basic brick and shapes to hydration.  
1.2 The values stated in inch-pound units are to be regarded as the standard. The values given in parentheses are for information only.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 Refractory brick are used as modular units in furnace construction and should not deviate significantly from the intended configuration with respect to size, bulk density, flat surfaces, and right angles. These test methods are particularly suited for use under field conditions and provide a means to determine whether the brick meets the requirements considered necessary to assure a satisfactory refractory construction.
SCOPE
1.1 These test methods cover procedures for measuring size, dimensional measurement, bulk density, warpage, and squareness of rectangular dense refractory brick and rectangular insulating firebrick. More precise determination of bulk density of refractory brick can be made by Test Methods C20. Stack height is generally determined only for dense refractories.  
Note 1: Test Methods C830 and Test Method C914 are also used to determine bulk density of refractory brick, by different procedures.  
1.2 The test methods appear in the following order:    
Sections    
Size and Bulk Density  
4 through 7    
Warpage of Refractory Brick  
8 through 10    
Squareness of Refractory Brick  
11 through 14  
1.3 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
4.1 The heat of hydration of a calcium aluminate-based castable is liberated over a short period of time (as compared to portland cement). This makes it easy to measure the heat profile using off-the-shelf thermocouple equipment.  
4.2 The heat profile can be used to make inferences about the setting and strength gain behavior of a castable and sometimes the working time of a castable.  
4.3 Factors that should be controlled when comparing two castables include: size, shape, and mass of cast object, start temperature of the mix, temperature of environment, and the thermal conductivity of the environment. If these factors are held constant, then the two castables’ heat profiles can be compared.  
4.4 The temperature increase created by the castable exothermic reaction shall be at least 2.0 °C more than the normal fluctuation of the laboratory temperature so that the time of this increase is easily discernible to the user.  
4.5 Varying the amount of cement in the castable, the amount of water, the type and quantity of admixtures, and so forth, will change the shape, maximum temperature, and time to maximum temperature of the curve.  
4.6 Following is an example of a curve generated for an LCC (see Fig. 1) that does exhibit two peaks, the first one marking the end of working time. In this curve, one could also infer that the start temperature of the mix was 24 °C and also that the hydraulic strength gain reaction was significantly started, but not completed by 6 h.
FIG. 1 Example of LCC Exo Profile
SCOPE
1.1 This guide applies to all castables with a reactive binder system that produces a measurable heat profile during the setting and hardening process. The majority of these systems will have calcium aluminate cement as one component of the binder system.  
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
4.1 The true specific gravity of a material is the ratio of its true density, determined at a specific temperature, to the true density of water, determined at a specific temperature. Thus, the true specific gravity of a material is a primary property which is related to chemical and mineralogical composition.  
4.2 This test method is particularly useful for hydratable materials that are not suitable for test with Test Method C135.  
4.3 For refractory raw materials and products, the true specific gravity is a useful value for: classification, detecting differences in chemical composition between supposedly like samples, indicating mineralogical phases or phase changes, calculating total porosity when the bulk density is known, and for any other test method that requires this value for the calculation of results.  
4.4 This test method is a primary standard method which is suitable for use in specifications, quality control, and research and development. It can also serve as a referee test method in purchasing contracts or agreements.  
4.5 Fundamental assumptions inherent in this test method are the following:  
4.5.1 The sample is representative of the material in general,  
4.5.2 The total sample has been reduced to the particle size specified,  
4.5.3 No contamination has been introduced during processing of the sample,  
4.5.4 The ignition of the sample has eliminated all free or combined water without inducing sintering or alteration,  
4.5.5 An inert gas (helium) has been used in the test, and  
4.5.6 The test method has been conducted in a meticulous manner.  
4.5.7 Deviation from any of these assumptions negates the usefulness of the results.  
4.6 In interpreting the results of this test method, it must be recognized that the specified sample particle size is significantly finer than specified for Test Method C135. Even this finer particle size for the sample does not preclude the presence of some closed pores, and the amount of residual close...
SCOPE
1.1 This test method covers the determination of the true specific gravity of solid materials, and is particularly useful for materials that easily hydrate which are not suitable for test with Test Method C135. This test method may be used as an alternate for Test Methods C135, C128, and C188 for determining true specific gravity.  
1.2 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.2.1 Exception—In 7.3, the equivalent SI unit is expressed in parentheses.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
4.1 This test method was developed for use both by manufacturers as a process control tool for the production of AZS fusion-cast refractories, and by glass manufacturers in the selection of refractories and design of glass-melting furnaces.  
4.2 The results may be considered as representative of the potential for an AZS refractory (specifically, in the tested region) to contribute to glass defect formation during the furnace production operation.  
4.3 The procedures and results may be applied to other refractory types or applications (that is, reheat furnace skid rail brick) in which glass exudation is considered to be important.
SCOPE
1.1 This test method covers a procedure for causing the exudation of a glassy phase to the surface of fusion-cast specimens by subjecting them to temperatures corresponding to glass furnace operating temperatures.  
1.2 This test method covers a procedure for measuring the exudate as the percent of volume increase of the specimen after cooling.  
1.3 Units—The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.3.1 Exception—The balance required for this test method uses only SI units (Section 7).  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
2.1 This test method provides a guide for evaluating the resistance of refractories in glass-melting furnace superstructures to vapor attack. This test method may also be useful for evaluating refractories in other applications where vapor attack occurs.  
2.2 An electric-heated furnace is recommended. Water vapor and other atmospheric components in a gas- or fuel-fired furnace may participate in the chemical and physical reactions being studied. Results may differ, therefore, depending upon the nature and type of firing employed.  
2.3 The degree of correlation between this test method and service performance is not fully determinable. This is intended to be an accelerated test method that generates a substantial degree of reaction in a relatively short amount of time. This acceleration may be accomplished by changing the composition and/or concentration of the reactants, increasing temperatures, or by performing the test in an isothermal environment.  
2.4 Since the test method may not accurately simulate the service environment, observed results of this test method may not be representative of those found in service. It is imperative that the user understand and consider how the results of this test method may differ from those encountered in service. This is particularly likely if the reaction products, their nature, or their degree differ from those normally found in the actual service environment.  
2.5 It is incumbent upon the user to understand that this is an aggressive, accelerated test method and to be careful in interpreting the results. If, for example, the reaction species have never been found in a real-world furnace, then this test method should not necessarily be considered valid to evaluate the refractory in question.
SCOPE
1.1 This test method covers a procedure for comparing the behavior of refractories in contact with vapors under conditions intended to simulate the environment within a glass-melting or other type of furnace when refractories are exposed to vapors from raw batch, molten glass, fuel, fuel contaminants, or other sources. This procedure is intended to accelerate service conditions for the purpose of determining in a relatively short time the interval resistance to fluxing, bloating, shrinkage, expansion, mineral conversion, disintegration, or other physical changes that may occur.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 Apparent porosity, water absorption, apparent specific gravity, and bulk density are primary properties of refractory shapes. These properties are widely used in the evaluation and comparison of product quality and as part of the criteria for selection and use of refractory products in a variety of industrial applications. These test methods are used for determining any or all of these properties and are particularly useful for testing hydratable products.  
3.2 These test methods are primary standard methods that are suitable for use in quality control, research and development, establishing criteria for and evaluating compliance with specifications, and providing data for design purposes.  
3.3 Fundamental assumptions inherent in these test methods are:  
3.3.1 The test specimens conform to the requirements for size, configuration, and original faces,  
3.3.2 The open pores of the test specimens are fully impregnated with liquid during the vacuum-pressure treatment, and  
3.3.3 The blotting of the saturated test specimens is performed as specified in a consistent and uniform manner to avoid withdrawing liquid from the pores.  
3.3.4 Deviation from any of these assumptions adversely affects the test results.  
3.4 In laboratory studies involving castable specimen, a bias was noted between formed 2 in. by 2 in. by 2 in. (50 mm by 50 mm by 50 mm) and specimens quartered from larger 9 in. by 4.5 in. by 2.5 in. (228 mm by 114 mm by 64 mm) cast specimens. Additionally, an error in the apparent porosity determination was found on castables whenever the specimens were heated to 1500 °F (816 °C) and then exposed to water as a saturation media. The error was attributed to reactivity of cement with water and subsequent re-hydration of cement phases. The higher the cement level of the castable, the greater the error noted. It was concluded that an error in porosity values could occur for refractory materials having a potential to form hydrated species with water. T...
SCOPE
1.1 These test methods cover the determination of the following properties of refractory shapes:  
1.1.1 Apparent porosity,  
1.1.2 Liquid absorption,  
1.1.3 Apparent specific gravity, and  
1.1.4 Bulk density.  
1.2 These test methods are applicable to all refractory shapes except those that chemically react with both water and mineral spirits. When testing a material capable of hydration or other chemical reaction with water but which does not chemically react with mineral spirits, mineral spirits is substituted for water and appropriate corrections for the density differences are applied when making calculations.  
1.3 Units—The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.3.1 Exception—The apparatus used in this standard is only available in SI units.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
Note 1: Test Methods C20 cover procedures for testing properties of refractories that are not attacked by water.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 Fireclay steel-teeming nozzles and sleeves are classified by volume reheat change. Bloating of some refractories results in irregular reheat dimensions, which are difficult to measure. This practice determines the volume without depending upon physical linear measurements.  
3.2 Blast furnace checkers that have irregular cross-sections are classified by “creep properties.” This practice determines the average cross-sectional area.
SCOPE
1.1 This practice covers the methods of calculating areas, volumes, and linear changes of irregularly shaped refractory specimens.  
1.2 The specimens must have a constant cross-sectional area over a length (L).  
1.3 The values stated in SI units are to be regarded as the standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 The mullite content of an alumina-silica refractory material has an important influence on volume stability, load-bearing properties, and its satisfactory use in refractory applications. This classification is considered useful for purchase specifications and quality control.
SCOPE
1.1 This classification covers refractory products consisting predominantly of mullite (3Al2O3·2SiO2) crystals that are formed by either converting any of the sillimanite group of minerals, or synthesizing from appropriate materials in a melt or sinter process.  
1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
2.1 The disintegration of carbon refractories by alkali attack at elevated temperatures is an important consideration in using these materials for certain applications. Disruption of carbon refractories in the test is sensitive to a number of variables, including alkali concentration, temperature, and the presence of water vapor. The procedure is suitable for guidance in product development and for relative comparisons in application work such as in blast furnace service.
SCOPE
1.1 This test method covers the behavior of carbon refractories when subjected to the action of an alkali at an elevated temperature. This destructive condition as encountered in service is accelerated in the test to show in a short time the probable behavior of the carbon refractory during use.  
1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 This test method provides a rapid, inexpensive method for comparing the corrosion resistance of refractories. The isothermal conditions of this test method represent the most severe static corrosion environment possible at the specified test temperature. This test method is suitable for quality control, research and development applications, and for product value studies on similar materials. Tests run at a series of temperatures are often helpful in determining the use temperature limitations of a particular material. Melt-line corrosion results are also a useful indication of relative resistance to both upward and downward drilling corrosion mechanisms. Examination of test specimens also provides information about the tendency for a particular refractory to form stones or other glass defects.  
3.2 Because this test method is both isothermal and static, and since most glass-contact refractories operate in a dynamic system with a thermal gradient, test results do not directly predict service in a furnace. The effects of differing thermal conductivities, refractory thickness, artificial cooling or insulation upon the refractory thermal gradient, and the erosive action of moving molten glass currents are not evaluated with this test.
SCOPE
1.1 This test method covers the determination of the corrosion resistance of refractories in contact with molten glass under static, isothermal conditions.  
1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
5.1 The deformation and end point of a cone corresponds to a certain heat-work condition due to the effects of time, temperature, and atmosphere.  
5.2 The precision of this test method is subject to many variables that are difficult to control. Therefore, an experienced operator may be necessary where PCE values are being utilized for specification purposes.  
5.3 PCE values are used to classify fireclay and high-alumina refractories.  
5.4 This is an effective method of identifying fireclay variations, mining control, and developing raw material specifications.  
5.5 Although not recommended, this test method is sometimes applied to materials other than fireclay and high alumina. Such practice should be limited to in-house laboratories and never be used for specification purposes.
SCOPE
1.1 This test method covers the determination of the pyrometric cone equivalent (PCE) of fire clay, fireclay brick, high-alumina brick, and silica fire clay refractory mortar by comparison of test cones with standard pyrometric cones under the conditions prescribed in this test method.  
1.2 Units—The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.2.1 Exceptions—Certain weights are in SI units with inch-pound in parentheses. Also, certain figures have SI units without parentheses. These SI units are to be regarded as standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 The oxidation of silicon carbide refractories at elevated temperatures is an important consideration in the application of these refractories. The product of oxidation is amorphous silica or cristobalite, depending upon the temperature at which oxidation takes place. This oxide formation is associated with expansion and degradation of strength. The quantity of water vapor in the atmosphere greatly affects the rate of oxidation.  
3.2 The test, which creates and measures the expansion, is suitable for guidance in product development and relative comparison in application work where oxidation potential is of concern. The variability of the test is such that it is not recommended for use as a referee test.
SCOPE
1.1 This test method covers the evaluation of the oxidation resistance of silicon carbide refractories at elevated temperatures in an atmosphere of steam. The steam is used to accelerate the test. Oxidation resistance is the ability of the silicon carbide (SiC) in the refractory to resist conversion to silicon dioxide (SiO2) and its attendant crystalline growth.  
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
4.1 This classification categorizes the defined types of fused-cast refractory blocks and shapes into distinct classes based on mineralogical composition. Such classes have historically been useful for relating the defined types and classes with specific industrial applications and for developing product or purchasing specifications.
SCOPE
1.1 This classification covers commercial fusion-cast refractory blocks and shapes. Its purpose is to set forth the various types and classes of these materials according to their mineralogical compositions. These compositions are important to determining their suitability for use in specified applications. This standard is not intended to cover commercial fused grains or beads.  
1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
4.1 This classification categorizes the defined types of refractory brick, with the exception of chrome brick, into distinct classes based on a nominal and minimal value for magnesium oxide content. Chrome brick are treated as a separate class without reference to magnesium oxide content. Such classes have historically been generally useful in relating the defined types to specific industrial applications and in developing product or purchasing specifications.
SCOPE
1.1 This classification categorizes machine-made refractory brick defined as chrome, chrome-magnesia, magnesia-chrome, and magnesia brick (see 3.1). It does not cover products made from electrically fused magnesium oxide or products made by fusion casting. Its purpose is to describe classes distinguished by obvious differences in magnesium oxide (MgO) content except for chrome brick.  
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 The presence of certain impurities in silica brick tends to lower their refractoriness and service limits. This classification permits those familiar with refractories to predict the refractoriness of silica brick from their alkali and alumina contents.
SCOPE
1.1 This classification is limited to silica brick meeting the following requirements:  
1.1.1 Alumina (Al2O3) content of less than 1.50 %.  
1.1.2 Titania (TiO2) content of less than 0.20 %.  
1.1.3 Iron oxide (FeO3) content of less than 2.50 %.  
1.1.4 Calcium oxide (CaO) content of less than 4.00 %.  
1.1.5 Average modulus of rupture of not less than 500 psi (3.45 MPa).  
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 The zircon content and bulk density of a zirconia-silica refractory material have important influences on chemical resistance and its satisfactory use in refractory applications. This classification is considered useful for purchase specifications and quality control.
SCOPE
1.1 This classification covers fired refractory brick and shapes consisting predominantly of zircon (ZrO2·SiO2) and containing, by chemical analysis, not less than 60 % zirconium oxide (ZrO2) and not less than 30 % silica (SiO2).  
1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 Alumina-silica refractory brick is produced from various combinations of alumina and silica-containing materials. These bricks can vary in chemical composition from almost 100 % alumina and little silica to almost 100 % silica and little alumina. It is therefore useful to establish a classification scheme based on physical properties and chemical analysis. One group, fireclay brick, is classified based on physical properties since some overlap of alumina and silica content can occur. A second group, high-alumina brick, is classified primarily based on alumina content. The classification allows those familiar with refractory materials to group similar products from various suppliers in a standard and consistent manner.
SCOPE
1.1 This classification covers machine-made fireclay and high-alumina refractory brick, and its purpose is to set forth the various classes and types of these materials in accordance with their normal and characteristic properties, which are important in their use.  
1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 Refractory mortars are used for laying, bonding and coating refractory brick. They become an integral part of the resulting refractory lining or structure. Therefore, such mortars should be selected in order to closely match those of the brick. A classification system is provided for use in producing, purchasing and using different types of refractory mortars.
SCOPE
1.1 This classification pertains to fireclay and high-alumina refractory mortars that can be trowelled, dipped or painted to join or coat refractory bricks and shapes.  
1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 Alumina and alumina-silicate castable refractories are produced to yield property characteristics commensurate with different end-use properties. Volume stability, modulus of rupture, bulk density, and lime content have become useful measures to distinguish various alumina and alumina-silicate castable formulations for initial fitness for service. This classification is considered useful for purchase specifications and for quality control.
SCOPE
1.1 This classification covers alumina and alumina-silicate castable refractories that, when tempered with water, will develop structural strength by chemical action.  
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 This practice is used to standardize the firing conditions of refractory concrete specimens prepared in accordance with Practice C862. The standards are set down to minimize laboratory-to-laboratory variation and do not attempt to duplicate any particular field applications.
SCOPE
1.1 This practice covers the firing of specimens made from refractory concretes (castable refractories) in accordance with Practice C862 for cast specimens. The procedure is also recommended for heating rates to be used for high-temperature test methods such as Test Methods C16, C583, etc., when these methods are used to test refractory concretes.  
1.2 The values stated in inch-pound units are to be regarded as the standard. The values given in parentheses are for information only.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 This classification defines a group of classes for use by those producing or purchasing fireclay and high-alumina plastic refractories and ramming mixes. Each class is limited by PCE or alumina content, or both. This classification is frequently used as a specification when the properties shown in Table 1 are the only items specified.  (A) NR = not required.
SCOPE
1.1 This classification covers fireclay and high-alumina plastic refractories and ramming mixes that can be pounded or rammed into place to form a monolithic structure. The terms “plastic” and “ramming mix” are generally intended to describe the workability of the material. In this regard, plastics are considered to be materials having a workability index of more than 15 % in accordance with Test Method C181, while ramming mixes generally have less than 15 % workability by the same procedure.  
1.2 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 This practice is provided to facilitate comparison of physical and mechanical properties of refractory materials by establishing uniform presentation of data.  
3.2 Units have been chosen, where possible, to result in numbers of magnitude familiar in the refractories industry, that is, g/cm3 rather than the SI preferred unit kg/m3. It is recommended that SI prefixes be selected for use with the units such that the resulting numerical values lie between 0.1 and 1000. For most properties, the prefixes kilo (k) and mega (M) are preferred. Other prefixes are given in the following table:    
Multiplication
Factor  
Prefix  
Symbol  
109  
giga  
G  
106  
mega  
M  
103  
kilo  
k  
102  
hectoA  
h  
101  
dekaA  
da  
10−1  
deciA  
d  
10−2  
centiA  
c  
10−3  
milli  
m  
10−6  
micro  
μ  
10−9  
nano  
n (A) To be avoided where practical.    
3.3 The conversion factors, which have been selected for their general utility in the refractories industry, have been taken from Practice E380, where possible. For uniformity, they have been presented to four decimal places. In use, the converted values should be rounded to the same number of significant figures as in the original value.
SCOPE
1.1 This practice presents the units to be employed for reporting the properties of refractories, such as density, crushing stress, modulus of rupture, tensile stress, thermal conductivity, and permeability.  
1.2 For convenience, a table of conversion factors between inch-pound units and SI units is included.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 The dimensions listed in this practice represent the dimensions of rectangular and tapered refractory shapes manufactured and used in the United States.  
3.2 The modular concept of dimensions permits a versatile arrangement of bonding during the construction of masonry units.
SCOPE
1.1 This practice covers the dimensions for rectangular and tapered brick in common usage in the United States.  
1.2 The dimensions are modular based on 38 mm as the basic module as described in Practice C861.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
4.1 This practice defines a procedure that ensures reasonably consistent preparation of specimens for product testing and evaluation.  
4.2 This practice can be used in the laboratories of producers, users, and general interest parties for research and development or quality control work. It is particularly useful for interlaboratory comparisons on products, for repetitive evaluations or comparisons of products or product quality, and in specifying a uniform preparation practice for specimens for acceptance testing.  
4.3 If pitch-impregnated samples are prepared by wet cutting or drilling, care should be taken in drying them. If the samples are heated to facilitate drying, the temperature to which they are heated should not be so high that it causes drainage of pitch from the samples.  
4.4 Porosities of metal-containing brick must be measured using kerosene or mineral spirits, because using water will result in an artificially low result.
SCOPE
1.1 This practice covers a procedure for preparing test specimens from magnesia-carbon and impregnated burned basic brick. This practice generally concerns preparation of test specimens from brick greater than 13 in. (33 cm) in length. These brick are mainly manufactured for use in electric arc furnaces and basic oxygen furnaces.  
1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 This classification establishes an orderly grouping of insulating firebrick to provide group identifications for use by those producing or purchasing these materials. The group identification number is not meant to specifically designate the maximum service temperature, although the number times 100 does approximate the temperature (in degrees Fahrenheit) to be used to check the reheat change and can be used as a guide for relative temperature stability. The bulk density limits the weight per unit volume for any group as sold, but is not meant to be used for detailed engineering calculations.
SCOPE
1.1 This classification covers heat-insulating material known as insulating firebrick. This material is suitable for lining certain kinds of industrial furnaces.  
Note 1: Insulating materials for use below 1000 °F (538 °C) are covered2 by ASTM Committee C16 on Thermal Insulation.  
1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 This test method is used to estimate the application temperature limits of a refractory mortar and will establish its classification.  
3.2 This test method will be regarded as a pass or fail test because the results are based on observations of whether the mortar flowed from the joints as a result of the heat treatment used.  
3.3 Results obtained by this test method will not agree with those obtained in service when heating is done from only one side.  
3.4 This test method is not applicable for testing nonaqueous mortars.
SCOPE
1.1 This test method covers the determination of refractoriness of all types of refractory mortar by heating a pier of brick laid up with the test mortar to learn whether the prescribed heat treatment causes the mortar to flow out of the joints.  
1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 Particle size distribution has a major effect upon most of the refractory properties. These test methods provide a means of measuring the distribution for the purpose of comparison to the desired distribution.  
3.2 These test methods also cover determination of the water content of refractory materials in the wet condition and of air-dried samples received, so that the sieve analysis can be calculated on the dry basis.  
3.3 These methods can produce data for specification acceptance, design purposes, manufacturing control, and research and development.  
3.4 A reference set of standard matched or calibrated sieves4 shall be provided for use in checking the set of sieves used in the actual sieve analysis of samples. The sieves for use in sieve analysis may also be standard matched sieves or may be unmatched sieves conforming to the Specification Table in Specification E11, provided that such sieves will give results that differ by no more than 5 % from those obtained with the reference set when the two sets are compared in accordance with the section of Test Method C429 on testing of sieves and sample splitters.
SCOPE
1.1 These test methods cover a wet and a dry method for sieve analysis of refractory materials.  
1.1.1 Wet Sieve Analysis—Water promotes the slaking of clays and helps to separate fine particles, washing them from the larger grains. This method is recommended for use with materials that require water addition, and that slake in normal industrial use.  
1.1.2 Dry Sieve Analysis—The dry method is not as effective as the wet method in determining the amount of material present in the smaller particle sizes. It is recommended (1) for clays, when the slaking action of water is undesirable, (2) when the material is in the form of coarsely ground grog and calcine, and (3) when the clay is to be used in such a way that the ultimate particle size is of secondary importance.  
1.2 These test methods also cover determination of the water content of refractory materials in the wet condition and of air-dried samples as received, so that the sieve analysis can be calculated on the dry basis. Included is a method for obtaining the water content of other refractory materials, such as plastic refractories and wet mixes.  
1.3 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
4.1 This test method measures the relative abrasion resistance of various refractory samples under standard conditions at room temperature.  
4.2 The abrasion resistance of a refractory material provides an indication of its suitability for service in abrasive environments.  
4.3 The results obtained by this test method could be different than those obtained in service because of the different conditions encountered.
SCOPE
1.1 This test method covers the determination of relative abrasion resistance of refractory brick at room temperature. This test method can also be applied to castable refractories (see Metric Dimensions, Practice C861 and Practice C865) and plastic refractories (see Practice C1054).  
1.2 Units—When values are stated in both SI and inch-pound units, the units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, use each system independently of the other. Combining values from the two systems may result in nonconformance with the standard. Several values are stated only in SI units as a matter of convention and to permit comparison of results. Included are the abrading media weight (grams), specimen weight (grams), specimen weight loss due to abrasion (grams), and the resultant volume loss (cubic centimeters).  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 Granular refractory materials may be either refractory grain raw materials that are used in the manufacture of finished refractory products, or bulk granular refractory materials that are sold, with or without some degree of processing, to refractory consumers for various uses. In either case, characterizing the properties of a granular refractory material is essential in evaluating its quality or consistency of quality and in determining suitability for end use. One of the important properties is bulk density because of its relationship to end product quality, usage, and performance.  
3.2 The refractories producer can use this test method as one of the quality control tests for his manufactured or mined refractory grain raw materials or for evaluating potential refractory grain raw materials.  
3.3 For the refractories consumer, the principal use of this test method is in the evaluation of the quality or the consistency of quality of the granular material in purchased refractory mixes or in bulk granular refractory materials used by the consumer.  
3.4 This is a primary test method, and thus is suitable for use in specifications, quality control, and research and development. It can also serve as a referee test method in purchasing contracts or agreements and as a base for development of more rapid, secondary test methods for use in quality control on manufactured refractory raw materials.  
3.5 Fundamental assumptions inherent in this test method are that the sample is representative of the material in general, the particle size of the sample is within the range specified by the test method, the material is not readily hydratable, and the size and quantity of pores in the material permits removal of surface water without drainage from the pores themselves. Deviation from any of these assumptions negates the usefulness of the test results.  
3.6 In interpreting the results of this test method, it must be recognized that the specific gravity of the materia...
SCOPE
1.1 This test method covers a procedure for determining the bulk density of granular refractory materials, commercial products which usually have particles that are retained on a 0.265 in. (6.7 mm) or coarser sieve.  
Note 1: This test method is not suitable for materials that hydrate in boiling water.  
1.2 Units—The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.2.1 Exceptions—In Sections 4, 7, and 8, the apparatus used is only available in SI units.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 The true specific gravity of a material is the ratio of its true density, determined at a specific temperature, to the true density of water, determined at a specific temperature. Thus, the true specific gravity of a material is a primary property which is related to chemical and mineralogical composition.  
3.2 For refractory raw materials and products the true specific gravity is a useful value for: classification, detecting differences in chemical composition between supposedly like samples, indicating mineralogical phases or phase changes, calculating total porosity when the bulk density is known, and for any other test method which requires this value for the calculation of results.  
3.3 This test method is a primary standard method which is suitable for use in specifications, quality control, and research and development. It can also serve as a referee test method in purchasing contracts or agreements.  
3.4 Fundamental assumptions inherent in this test method are the following:  
3.4.1 The sample is representative of the material in general,  
3.4.2 The total sample has been reduced to the particle size specified,  
3.4.3 No impurity has been introduced during processing of the sample,  
3.4.4 The sample itself is not magnetic and all magnetic material introduced during processing of the sample has been removed,  
3.4.5 The material is not hydratable or reactive with water, and  
3.4.6 The test method has been conducted in a meticulous manner.  
3.4.7 Deviation from any of these assumptions negates the usefulness of the results.  
3.5 In interpreting the results of this test method it must be recognized that the specified sample particle size does not guarantee that all closed pores have been eliminated. The amount of residual closed pores may vary between materials or even between samples of the same or like materials, and the specified sample particle size is not the same as that specified for Test Method C604. The values generated by this ...
SCOPE
1.1 This test method covers the determination of true specific gravity of refractory materials under prescribed conditions. It is not applicable to materials attacked by water.  
1.2 Units—The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.2.1 Exception—The equipment used in this standard for weights and volumes is only available in SI units.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 This test method indicates the ability of a refractory product to withstand the stress generated by sudden changes in temperature.  
3.2 Because the recommended furnace temperature of this cycling test is 1200 °C (2190 °F), this test method may not indicate the ability of a refractory product to withstand cycling at higher or lower temperatures, especially if the existing morphology of the refractory product changes.  
3.3 This test method is useful for research and development, as well as for comparing refractory products. The precision should be considered when using this test for specification purposes.  
3.4 Ruggedness tests found the following variables to be rugged:    
Temperature  
+5 °C    
Hot spacing  
1/2 to 3/4 in. (12.77 to 19 mm)    
Cold spacing  
1/2 to 3/4 in. (12.77 to 19 mm)    
Center versus end gripping of the bars    
Hot hold time  
10 to 15 min    
Cold hold time  
10 to 15 min    
Operator air speed  
0 to 2 mi/h (0 to 3.2 km/h)    
Initially cold or heated samples    
Last in, first out (LIFO); or first in, first out (FIFO)
removal from the furnace  
Sawed or original surface as tensile face during MOR testing    
Bar thickness  
0.96 to 1.04 in. (24.5 to 26.4 mm)
SCOPE
1.1 This test method is used for determining the strength loss or reduction in continuity, or both, of prism-shaped specimens which are cut from refractory brick or shapes and subjected to thermal cycling.  
1.2 The strength loss is measured by the difference in modulus of rupture (MOR) between uncycled specimens and the specimens subjected to thermal cycling.  
1.3 The reduction in structural continuity is estimated by the difference in sonic velocity before and after thermal cycling.  
1.4 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 Apparent porosity, water absorption, apparent specific gravity, and bulk density are primary properties of burned refractory brick and shapes. These properties are widely used in the evaluation and comparison of product quality and as part of the criteria for selection and use of refractory products in a variety of industrial applications. These test methods are used for determining any or all of these properties.  
3.2 These test methods are primary standard methods which are suitable for use in quality control, research and development, establishing criteria for and evaluating compliance with specifications, and providing data for design purposes.  
3.3 Fundamental assumptions inherent in these test methods are that the test specimens are not attacked by water, the test specimens conform to the requirements for size, configuration, and original faces, the open pores of the test specimens are fully impregnated with water during the boiling treatment, and the blotting of the saturated test specimens is performed as specified in a consistent and uniform manner to avoid withdrawing water from the pores. Deviation from any of these assumptions adversely affects the test results.  
3.4 In laboratory studies involving castable specimens, a bias was noted between formed 2 by 2 by 2 in. (50 by 50 by 50 mm) and specimens that were quartered from larger 9 by 4.5 by 2.5 (228 by 114 by 64 mm) cast specimens. Additionally, an error in the apparent porosity determination on castables was found whenever the specimens were heated to 1500 °F (816 °C) and then exposed to water as a saturation media (Test Methods C830). The error was attributed to reactivity of cement with water and subsequent re-hydration of cement phases. The higher the cement level of the castable, the greater the error noted. It was concluded that an error in porosity values could occur for refractory materials having a potential to form hydrated species with water.3  
3.5 Certain precautions must be exe...
SCOPE
1.1 These test methods cover the determination of the following properties of burned refractory brick:  
1.1.1 Apparent porosity,  
1.1.2 Water absorption,  
1.1.3 Apparent specific gravity, and  
1.1.4 Bulk density.  
1.2 These test methods are not applicable to refractories attacked by water.  
1.3 The values stated in inch-pound units are to be regarded as the standard. The values given in parentheses are for information only.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
2.1 This test method may be used to quickly determine volume and bulk density of a refractory of any shape, provided it has sufficient structural integrity to permit handling. Thus it may be used on unfired or fired, strong or friable shapes.  
2.2 Since the test may be performed quickly, it has found application as manufacturing in-process control as well as in characterizing finished refractory products. Also it may be used to examine specimens after other test or service exposure.
SCOPE
1.1 This test method covers the basic procedure for determining bulk density and volume of refractory shapes. This test is applicable to all refractory shapes or monoliths, burned or unburned, independent of composition or forming method, including materials that slake and hydrate. It is particularly suitable for determining bulk density and volume of complex shapes after forming, since results may be obtained in a matter of minutes.  
1.2 Units—The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.2.1 Exception—The balance used in this standard is only available in SI units (Sections 3 – 6).  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For a specific hazard statement, see 3.2.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
5.1 The thermal expansion under load and the 20 to 50 h creep properties of a refractory are useful in characterizing the load-bearing capacity of a refractory that is uniformly heated. Directly applicable examples are blast furnace stoves and glass furnace checkers.
SCOPE
1.1 This test method covers the procedure for measuring the linear change of refractory specimens that are subjected to compressive stress while being heated and while being held at elevated temperatures.  
1.2 This test method does not apply to materials whose strength depends on pitch or carbonaceous bonds unless appropriate atmospheric control is used (see 7.3).  
1.3 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 The thermal conductivity of monolithic refractories is a property required for selecting their thermal transmission characteristics. Users select monolithic refractories to provide specified conditions of heat loss and cold face temperature, without exceeding the temperature limitation of the monolithic refractory. This test method establishes placement of thermocouples and positioning of test specimens in the calorimeter.  
3.2 This procedure must be used with Test Method C201 and requires a large thermal gradient and steady-state conditions. The results are based upon a mean temperature.  
3.3 The data from this test method are suitable for specification acceptance, estimating heat loss and surface temperature, and the design of multi-layer refractory construction.  
3.4 The use of these data requires consideration of the actual application environment and conditions.
SCOPE
1.1 This test method supplements Test Method C201, and shall be used in conjunction with that test method for determining the thermal conductivity of unfired monolithic refractories.  
1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 Measuring the modulus of rupture of refractories at elevated temperatures has become a widely accepted means to evaluate materials at service temperatures. Many consumer companies have specifications based on this type of test.  
3.2 This test method is limited to furnaces operating under oxidizing conditions. However, with modifications for atmosphere control in other test furnaces, the major criteria of this test procedure may be employed without change.  
3.3 This test method is designed for progressive application of a force or stress on a specimen supported as a simple beam with center-point loading. Test apparatus designed for the progressive application of a strain may yield different results, especially since refractory materials will reach a semiplastic state at elevated temperatures where Hooke's law does not apply, that is, stress is then not proportional to strain.  
3.4 This test method applies to fired dense refractory brick and shapes, chemically bonded brick and shapes, shapes formed from castables, plastics, or ramming materials, and any other refractory that can be formed to the required specimen dimension.
SCOPE
1.1 This test method covers determination of the high-temperature modulus of rupture of refractory brick or monolithic refractories in an oxidizing atmosphere and under action of a force or stress that is increased at a constant rate.  
1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
2.1 This practice defines a procedure that ensures consistent preparation of specimens for product testing and evaluation.  
2.2 This practice can be used in the laboratories of producers, users, and general-interest parties for research and development or quality-control work. It is particularly useful for interlaboratory comparisons or products, for repetitive evaluations or comparisons of products or product quality, and in specifying a uniform preparation practice for specimens for acceptance testing.  
2.3 In using this practice it must be recognized that the structure of laboratory-cast specimens may differ significantly from the structure of material cast in field applications.
SCOPE
1.1 This practice covers a procedure for preparing test specimens from a basic refractory castable by casting prepared material in a mold. Specimens prepared in accordance with this procedure are intended for use in ASTM test methods.  
1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
2.1 This practice defines a procedure that ensures consistent preparation of specimens for product testing and evaluation.  
2.2 This practice can be used in the laboratories of producers, users, and general-interest parties for research and development or quality-control work. It is particularly useful for interlaboratory comparisons on products, for repetitive evaluations or comparisons of products or product equality, and in specifying a uniform preparation practice for specimens for acceptance testing.  
2.3 In using this practice, it must be recognized that the structure of laboratory-pressed specimens may differ significantly from the structure of material gunned in field applications.
SCOPE
1.1 This practice covers a procedure for preparing test specimens from basic refractory gunning products by pressing prepared material in a mold. After pressing, test specimens prepared from dolomitic mixes are subjected to a prescribed heat treatment. Specimens prepared in accordance with this procedure are intended for use in ASTM test methods.  
1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 The properties of refractories can be affected by their method of installation. This practice attempts to minimize the variables encountered during installation by pneumatic gunning.  
3.2 This practice provides parameters to produce gunned specimens for use in other ASTM test methods.  
3.3 This practice may be used to produce specimens for acceptance testing, service evaluation, manufacturing control, and research and development.  
3.4 Differences between various kinds of equipment and the differences in procedures and operator techniques may result in significant variations in the physical properties of the gunned specimens. It is recommended that the same operator use the same equipment to produce specimens for referee testing agreed to by the involved testing parties. The specific operating parameters should be shown in the report.  
3.5 Although this practice is specifically designed for refractories containing calcium aluminate cement, it may be used with minor modifications for gun mixes containing other bond systems.
SCOPE
1.1 This practice covers a procedure for preparing refractory specimens usually containing calcium aluminate cement with or without metal fibers by cold nozzle-mix gunning. Specimens prepared in accordance with this practice are intended for use in standard ASTM test methods required for evaluating gunned materials.  
1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
2.1 This practice defines a procedure that ensures consistent preparation of specimens for product testing and evaluation.  
2.2 This practice can be used in the laboratories of producers, users, and general-interest parties for research and development or quality-control work. It is particularly useful for interlaboratory comparisons of products, for repetitive evaluations or comparisons of products or product quality, and in specifying a uniform preparation practice for specimens for acceptance testing.  
2.3 In using this practice it must be recognized that the structure of laboratory-pressed specimens may differ significantly from the structure of material rammed in field applications.
SCOPE
1.1 This practice covers a procedure for preparing test specimens from basic refractory ramming products by pressing prepared material in a mold. Specimens prepared in accordance with this procedure are intended for use in ASTM test methods.  
1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 This practice is used to standardize mixing, mold conditions, placement, and curing of refractory concrete specimens to be used for testing and evaluation under other test methods.  
3.2 This practice standardizes laboratory conditions for producing refractory concrete specimens to minimize laboratory-to-laboratory variation and does not attempt to duplicate the conditions of field installations.  
3.3 This practice can be used for the preparation of specimens used in referee testing.
SCOPE
1.1 This practice covers the mixing, casting, and curing of monolithic refractory concrete specimens under laboratory conditions for use in further testing. It does not apply to monolithic castable refractories intended primarily for gunning applications.  
1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.3 Various specimen sizes are required for specific test methods. Refer to these test methods to determine the size and number of specimens, which will be required from the sample.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
5.1 This test method is used to determine the sonic velocity and approximate Young's modulus of refractory shapes at room temperature. Since this test is nondestructive, specimens may be used for other tests as desired.  
5.2 This test method is useful for research and development, engineering application and design, manufacturing quality and process control, and for developing purchasing specifications.
SCOPE
1.1 This test method describes a procedure for measuring the sonic velocity in refractory materials at room temperature. The sonic velocity can be used to obtain an approximate value for Young's modulus.  
1.2 The sonic velocity may be measured through the length, thickness, and width of the specimen.  
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
2.1 This test method is used to determine the relative resistance of various refractories to disintegration caused by exposure to a CO atmosphere. The results obtained by this method can be used to select refractories that are resistant to CO disintegration.  
2.2 This test method is suitable for research and development and for establishing CO disintegration criteria for specification acceptance.  
2.3 The disintegration of test specimens is accelerated by providing a higher concentration of CO than anticipated in most service environments. The effects on the test specimens may be different than those found for refractories in actual service conditions.
SCOPE
1.1 This test method covers the comparative behavior of refractories under the disintegrating action of carbon monoxide (CO). The test method is an accelerated exposure to CO to determine potential material behavior in a relatively short time.  
1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
4.1 Young’s modulus is a fundamental mechanical property of a material.  
4.2 This test method is used to determine the dynamic modulus of elasticity of rectangular shapes. Since the test is nondestructive, specimens may be used for other tests as desired.  
4.3 This test method is useful for research and development, engineering application and design, manufacturing process control, and for developing purchasing specifications.  
4.4 The fundamental assumption inherent in this test method is that a Poisson’s ratio of 1/6 is typical for heterogeneous refractory materials. The actual Poisson's ratio may differ.
SCOPE
1.1 This test method covers a procedure for measuring the resonance frequency in the flexural (transverse) mode of vibration of rectangular refractory brick or rectangularly shaped monoliths at room temperature. Young's modulus is calculated from the resonance frequency of the shape, its mass (weight), and dimensions.  
1.2 Units—The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.2.1 Although the Hertz (Hz) is an SI unit, it is derived from seconds which is also an inch-pound unit.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.