Space product assurance - Qualification and Procurement of printed circuit boards

This standard addresses the qualification and procurement of printed circuit boards, which are necessary for all type of space projects.

Raumfahrtproduktsicherung - Qualifizierung und Beschaffung von Leiterplatten

Assurance produit des projets spatiaux - Qualification et approvisionnement des circuits imprimés

Zagotavljanje kakovosti proizvodov v vesoljski tehniki - Kvalifikacija in nabava plošč tiskanih vezij

Ta standard obravnava kvalifikacijo in nabavo plošč tiskanih vezij, ki so potrebna za vse vrste vesoljskih projektov.

General Information

Status
Published
Publication Date
09-Jul-2019
Withdrawal Date
30-Jan-2020
Technical Committee
Current Stage
6060 - Definitive text made available (DAV) - Publishing
Start Date
10-Jul-2019
Due Date
27-Apr-2019
Completion Date
10-Jul-2019

Relations

Standard
EN 16602-70-60:2019 - BARVE
English language
269 pages
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Standards Content (Sample)


SLOVENSKI STANDARD
01-september-2019
Nadomešča:
SIST EN 16602-70-10:2015
SIST EN 16602-70-11:2015
Zagotavljanje kakovosti proizvodov v vesoljski tehniki - Kvalifikacija in nabava
plošč tiskanih vezij
Space product assurance - Qualification and Procurement of printed circuit boards
Raumfahrtproduktsicherung - Qualifizierung und Beschaffung von Leiterplatten
Assurance produit des projets spatiaux - Qualification et approvisionnement des circuits
imprimés
Ta slovenski standard je istoveten z: EN 16602-70-60:2019
ICS:
31.180 Tiskana vezja (TIV) in tiskane Printed circuits and boards
plošče
49.140 Vesoljski sistemi in operacije Space systems and
operations
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

EUROPEAN STANDARD
EN 16602-70-60
NORME EUROPÉENNE
EUROPÄISCHE NORM
July 2019
ICS 31.180; 49.140
Supersedes EN 16602-70-10:2015, EN 16602-70-
11:2015
English version
Space product assurance - Qualification and Procurement
of printed circuit boards
Assurance produit des projets spatiaux - Qualification Raumfahrtproduktsicherung - Qualifizierung und
et approvisionnement des circuits imprimés Beschaffung von Leiterplatten
This European Standard was approved by CEN on 9 November 2018.

CEN and CENELEC members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for
giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical
references concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to
any CEN and CENELEC member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by
translation under the responsibility of a CEN and CENELEC member into its own language and notified to the CEN-CENELEC
Management Centre has the same status as the official versions.

CEN and CENELEC members are the national standards bodies and national electrotechnical committees of Austria, Belgium,
Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany,
Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania,
Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and United Kingdom.

CEN-CENELEC Management Centre:
Rue de la Science 23, B-1040 Brussels
© 2019 CEN/CENELEC All rights of exploitation in any form and by any means Ref. No. EN 16602-70-60:2019 E
reserved worldwide for CEN national Members and for
CENELEC Members.
Table of contents
European Foreword . 13
Introduction . 14
1 Scope . 15
2 Normative references . 16
3 Terms, definitions and abbreviated terms . 18
3.1 Terms from other standards . 18
3.2 Terms specific to the present standard . 19
3.3 Abbreviated terms. 27
3.4 Nomenclature . 29
4 Principles . 30
4.1 General . 30
4.2 Roles . 30
4.3 References to acceptance criteria . 30
5 QA for qualification . 31
5.1 Qualified PCBs . 31
5.2 Ceramic PCB technology . 32
5.3 Flexible PCB . 32
5.3.1 General . 32
5.3.2 Qualification of flexible PCB . 32
5.4 Qualification process . 34
5.5 Request for qualification . 34
5.6 Quality standards . 35
5.7 Description of qualification vehicle . 35
5.8 Evaluation . 36
5.9 Audit . 36
5.10 Qualification test programme . 38
5.11 PID . 38
5.12 Qualification approval . 39
5.13 Process change . 39
5.14 QA report . 40
5.15 Qualification renewal . 40
5.16 Nonconformances during qualification renewal . 41
6 QA for manufacture and procurement . 43
6.1 Overview . 43
6.2 Procurement process . 43
6.2.1 Overview . 43
6.2.2 Procurement specification . 44
6.2.3 Quotation . 44
6.2.4 Purchase order . 45
6.2.5 Design review (DR) . 45
6.2.6 MRR . 45
6.3 Final and in-process inspection. 46
6.4 Quality records for manufacture and procurement . 47
6.5 Control of materials and chemistry . 48
6.6 Control of plating chemistry . 49
6.7 Cleanliness of PCB processes . 50
6.7.1 Overview . 50
6.7.2 Cleanliness control . 51
6.8 Traceability . 52
6.9 Operator and inspector training. 53
6.10 Repair of bare PCBs . 54
6.10.1 Overview . 54
6.10.2 General . 54
6.11 Packaging . 56
6.12 Storage and baking of PCB and coupons . 57
6.13 Shelf-life and relife testing . 57
6.14 QA for PCB procurement in space projects. 58
7 Test and inspection for qualification . 61
7.1 Overview . 61
7.2 Test selection for qualification activities . 64
7.3 Initial qualification of PCB manufacturer . 68
7.4 Initial qualification of PCB technology . 68
7.5 Qualification renewal . 68
7.6 Delta qualification . 68
7.7 Project qualification and RFA . 69
7.7.1 Overview . 69
7.7.2 Requirements for project qualification and RFA . 69
8 Test and inspection for procurement . 74
8.1 Outgoing inspection on PCB . 74
8.2 Outgoing inspection on coupons . 75
8.2.1 Overview . 75
8.2.2 Configuration of coupons for plated holes . 78
8.2.3 Configuration of dedicated coupons . 81
8.2.4 Evaluation of coupons . 82
8.2.5 Delivery of coupons, microsections and spare coupons . 84
8.3 Reporting of outgoing inspection and delivery . 85
8.4 Incoming inspection by procurement authority . 85
8.5 FAI on PCB by microsectioning . 86
9 Test descriptions . 88
9.1 Overview . 88
9.2 Additional tests . 88
9.2.1 Cleanliness . 88
9.2.2 Bake-out . 88
9.2.3 Plated copper tensile strength and elongation . 89
9.2.4 Steam ageing . 89
9.3 Group 1 – Visual inspection and non-destructive tests . 90
9.3.1 Visual inspection - general . 90
9.3.2 Visual inspection for qualitative aspects . 90
9.3.3 Visual inspection for dimensional verification . 90
9.3.4 Impedance test . 94
9.3.5 Dielectric constant and loss tangent . 94
9.3.6 Cleanliness . 94
9.3.7 High resistance electrical test . 95
9.3.8 Continuity test . 97
9.4 Group 2 - Miscellaneous tests . 99
9.4.1 Overview . 99
9.4.2 Peel strength . 100
9.4.3 Flexural fatigue . 101
9.4.4 Bending test . 102
9.4.5 Coating adhesion – tape test . 103
9.4.6 Analysis of tin-lead coating . 104
9.4.7 Outgassing . 104
9.4.8 Thermal analysis . 105
9.4.9 Flammability . 105
9.4.10 Offgassing . 106
9.4.11 Solderability . 106
9.5 Group 3 – Thermal stress and as-received . 110
9.5.1 Overview . 110
9.5.2 Microsectioning . 110
9.5.3 Solder bath float . 115
9.5.4 Rework simulation . 115
9.5.5 Interconnect stress test (IST) . 117
9.6 Group 4 – Assembly and life test - extended. 124
9.6.1 Overview . 124
9.6.2 Test flow for group 4 . 124
9.6.3 Insulation resistance . 126
9.6.4 Dielectric withstanding voltage (DWV) . 127
9.7 Group 5 – ECM tests . 128
9.7.1 Overview . 128
9.7.2 Temperature, Humidity, Bias (THB) . 128
9.7.3 Conductive Anodic Filament (CAF) . 134
9.8 Group 6 – Assembly and life test - short . 140
9.8.1 Overview . 140
9.8.2 Test flow for group 6 . 140
9.8.3 Reflow simulation . 141
9.8.4 Thermal cycling . 141
10 Acceptance criteria . 143
10.1 Overview . 143
10.2 Inspection by microsectioning for dimensional verification . 143
10.3 Inspection by microsectioning for qualitative aspects . 164
10.4 Visual inspection . 194
10.5 Visual inspection of sculptured flex PCB . 210
10.6 Additional requirement to the tables . 229
10.6.1 Annular ring. 229
10.6.2 Pad lift and associated laminate cracks . 230
10.6.3 Miscellaneous . 232
Annex A (normative) Qualification letter – DRD . 235
Annex B (normative) CoC for PCB – DRD . 236
Annex C (normative) Qualification test report – DRD . 250
Annex D (normative) Process Identification Document (PID) for PCB
manufacturing – DRD . 251
Annex E (normative) Process change notice (PCN) – DRD . 254
Annex F (normative) QA report – DRD . 255
Annex G (normative) PCB approval sheet – DRD . 256
Annex H (informative) Example of plated­through hole microsection . 261
Annex I (informative) Cleanliness requirements for laminate and prepreg . 262
Annex J (informative) Example qualification programme . 265
Bibliography . 268

Figures
Figure 3-1: Example of material supplier treatment side of foil (white arrows) and PCB
manufacturer treatment side of foil (opposite side) . 25
Figure 7-1: Test flow for qualification . 62
Figure 8-1: Flow for preparation, test and inspection of procurement coupons . 78
Figure 8-2: Example of Bn coupon with 3 holes per drilling sequence . 79
Figure 8-3: Example of placement of coupons and PCB in usable area of
manufacturing panel . 80
Figure 8-4: Example of vias manufactured at different plating and drilling sequences . 81
Figure 8-5: Example of target quality of microsection of rigid-flex interface with UV
fluorescent resin and polarised light . 84
Figure 9-1: Conductor width (w) measured at the foot as seen in a cross-section. . 91
Figure 9-2: Warp . 92
Figure 9-3: Twist. 93
Figure 9-4: Horizontal adjacency on layer Ln and vertical adjacency on the layers
above and below. . 97
Figure 9-5: Midpoint classification . 97
Figure 9-6: Setting of test point assignments. The numbers 1 to 7 correspond to the
conditions of requirement 9.3.8.2g. . 99
Figure 9-7: Example of target quality of microsection of innerlayer (top) and knee of the
hole (bottom), as-polished (left) and after micro-etch (right). . 113
Figure 9-8: Examples of inadequate quality of microsection showing in the top image
inadequate polishing, leaving scratches on surface, in the middle image
over-etched sample and in the bottom image inadequate lighting, revealing
no detail on metallisation, nor on laminate by transparency. 114
Figure 9-9: Examples of barrel cracks after IST testing showing a nominal crack size
(left) and a large crack filled with SnPb (right) . 123
Figure 9-10: THB test pattern . 130
Figure 9-11: Build-up for THB test vehicle . 130
Figure 9-12: Insulation resistance during THB Ambient (until sample nr 1000) and THB
ECM showing continuous breach of insulation on 4 patterns in the lower
graph. The top graph shows stable insulation. . 133
Figure 9-13: Horizontal microsection showing fibre contamination on tracks in prepreg
resin causing breach of insulation. . 133
Figure 9-14: Lay-out of CAF pattern . 137
Figure 9-15: Schematic for CAF growth . 137
Figure 10-1: Annular ring internal . 145
Figure 10-2: Annular ring external . 146
Figure 10-3: Copper foil thickness . 147
Figure 10-4: Three measurements of copper plating thickness at locations that are at 25
%, 50 % and 75 % of the height of the hole . 149
Figure 10-5: Measurement “average on resin” is performed on zone A. Measurement
“on any local thin areas on resin or glass” is performed on Zone B . 149
Figure 10-6: Glass fibre protrusion in case of negative etchback (left) and positive
etchback (right) . 150
Figure 10-7: Example of negative etchback (left) and approximately neutral etchback
(right) . 150
Figure 10-8: Wicking is measured from resin of hole wall (red arrows). In case it
exceeds the annular ring, the insulation distance to adjacent circuitry (blue
arrow) can be reduced. . 151
Figure 10-9: Example of wicking . 151
Figure 10-10: Wrap target condition . 152
Figure 10-11: Wrap thickness below requirement, not acceptable . 152
Figure 10-12:Projected-peak-to-peak insulation . 153
Figure 10-13: Example of glass compression . 153
Figure 10-14: Microvia insulation . 154
Figure 10-15: Penetration of capture pad for µvia, not acceptable . 154
Figure 10-16: Microvia aspect ratio, X ≥ Z. 155
Figure 10-17: Dimple in microvia . 155
Figure 10-18: ICD on capture pad (pictures are unetched) . 155
Figure 10-19: Microvia plating, target condition . 156
Figure 10-20: Example of void in microvia plating . 156
Figure 10-21: Tin-lead thickness in PTH schematic (left) and a typical microsection
(right) . 158
Figure 10-22: Tin-lead thickness on PTH corner – target thickness (left), coverage of less
than 1 µm (middle), absence of SnPb on IMC (right) . 158
Figure 10-23: Tin-lead thickness on pad . 158
Figure 10-24: Undercut. 161
Figure 10-25: Example of spurious copper . 161
Figure 10-26: Overhang of electrolytic Au . 162
Figure 10-27: Example of dimensional verification of rigid-flex interface . 163
Figure 10-28: Examples of acceptable voids . 167
Figure 10-29: Examples of unacceptable voids . 167
Figure 10-30: Examples of separation between hole wall and resin inside blind via . 167
Figure 10-31: Example of acceptable thin line separation . 168
Figure 10-32: Example of non-acceptable bulging . 168
Figure 10-33: Example of dimple on blind via . 169
Figure 10-34: Example of bump on blind via . 169
Figure 10-35: Example of plating nodule . 170
Figure 10-36: Example of burrs reducing hole diameter . 170
Figure 10-37: Example of voids – top image shows etch-out and bottom image shows
an encapsulated void or inclusion. 172
Figure 10-38: Skip plating on flex laminate as-polished (top) and after micro-etch
(bottom). 172
Figure 10-39: Skip plating on glass fibres . 172
Figure 10-40: Open wedge void (top), enclosed wedge void (middle), copper filled
wedge (bottom) . 174
Figure 10-41: Schematic of wedge void dimensions . 174
Figure 10-42: Example of wedge voids . 174
Figure 10-43: Example of resin void . 175
Figure 10-44: Example of delamination . 176
Figure 10-45: Pad lift schematic . 177
Figure 10-46: Examples of pad lift cracks. The right image is unacceptable because
cracks continue until the hole wall . 178
Figure 10-47: Acceptable (green) and non-acceptable (red) dielectric cracks . 180
Figure 10-48: Examples of laminate cracks . 180
Figure 10-49: Example of C foil separation as-polished and after micro-etch . 182
Figure 10-50: Example of interface line between plated copper layers on a non-etched
microsection . 182
Figure 10-51: Interconnect after stress, target condition, after microetch (top) and as-
polished (bottom) . 183
Figure 10-52: Examples of ICD . 183
Figure 10-53: Example of smear . 184
Figure 10-54: Example of hole wall pull away - showing separation of copper in a straight
line (left) or slightly bulging outward (right) . 185
Figure 10-55: Example of resin recession - showing concave retraction of resin . 185
Figure 10-56: Target condition . 186
Figure 10-57: Acceptable nail heading . 186
Figure 10-58:Unacceptable nail heading, exceeding 50 % of innerlayer copper
thickness . 186
Figure 10-59: Examples of CIC connection, target condition (left), nailheading (middle),
separation to CIC (right) . 187
st nd
Figure 10-60: Examples of swirl (1 and 2 image) and demarcation line (3rd). In the
nd
2 picture the difference between no-flow prepreg (top) and laminate
(bottom) is noticeable . 189
Figure 10-61: Example of dotted interface line observed in dark field out of focus (right),
which is not visible in focus (middle) and in bright field (left) . 189
Figure 10-62: Example of metallic contamination in laminate . 190
Figure 10-63: Acceptable adhesion between coverlay and prepreg . 191
Figure 10-64: Delamination between coverlay and prepreg . 191
Figure 10-65 Example of voids in acrylic adhesive in rigid-to-flex interface. 192
Figure 10-66: Example of adhesive filet recession into rigid section as observed in
microsection . 193
Figure 10-67: Conductor width . 195
Figure 10-68: Conductor spacing . 196
Figure 10-69: Example of lifted land . 197
Figure 10-70: Example of visible copper on top surface (left) and on side of track (right) . 197
Figure 10-71: Example of measling . 198
Figure 10-72: Examples of crazing . 198
Figure 10-73: Examples of contamination and inhomogeneity . 199
Figure 10-74: Example of scratches on conductors and dielectric . 200
Figure 10-75: Haloing at edge . 202
Figure 10-76: Haloing from non-plated hole to footprint for stiffener . 202
Figure 10-77: Granular aspect . 203
Figure 10-78: Dewetting . 203
Figure 10-79: Example of unclear marking . 204
Figure 10-80: Example of resin squeeze out . 205
Figure 10-81: Example of adhesive filet recession into rigid section as observed in
visual inspection . 205
Figure 10-82: Examples of fibre protrusion . 206
Figure 10-83: Example of acceptable incidental haloing ≤ 1 mm into rigid section . 207
Figure 10-84: Example of an acceptable superficial scratch . 209
Figure 10-85: Examples of non-acceptable cut and blister, evident by a sharp
indentation . 209
Figure 10-86: Examples of burrs on edge of flex . 209
Figure 10-87: Misregistration of top and bottom coverlay . 212
Figure 10-88: Misregistration of hole in coverlay to the conductor . 212
Figure 10-89: Examples of white spot configurations and black spot contamination . 214
Figure 10-90: Examples of fibre contamination . 214
Figure 10-91: Examples of SnPb infiltration on sculptured pad (left) and on tracks
(right) . 215
Figure 10-92: Bare copper on fingers . 216
Figure 10-93: Misregistration of pads . 217
Figure 10-94: Hole misregistration causing reduced annular ring . 218
Figure 10-95: Schematic of conductor width and spacing and local defects . 220
Figure 10-96: Examples of nick near pad, nick on conductor, overetching reducing
thickness of conductor, nick on finger, pinhole and local reduced track width
(left to right) . 220
Figure 10-97: Examples of insufficient spacing between conductors, copper residue
between pads, copper residue to edge of flex, bump on conductor (left to
right) . 220
Figure 10-98: Adhesive in plated holes . 221
Figure 10-99: Example of adhesive in plated holes . 221
Figure 10-100: SnPb coverage on pads . 222
Figure 10-101: Pad diameter reduction due to local coverage by coverlay or resin
squeeze out . 222
Figure 10-102: Copper wrinkle . 223
Figure 10-103: Tear in hole and edge of coverlay . 224
Figure 10-104: Burrs on holes . 224
Figure 10-105: Nick on edge of coverlay . 224
Figure 10-106: Coverlay scratch – Non acceptable . 225
Figure 10-107: Acceptable aspect of finger after bending . 226
Figure 10-108: Unacceptable aspect of finger after bending . 226
Figure 10-109: Cross-section of hole: Copper conductor shown . 228
Figure 10-110: Calculation of remaining insulation distance . 233

Figure H-1 : Typical phenomena in cross-section of PTH. Not all phenomena are
specified in ECSS-Q-ST-70-60 in the same way. . 261

Tables
Table 6-1: Example of lead time in weeks (wk) for various phases of PCB procurement,
manufacture, test and inspection. . 43
Table 7-1: List of coupons with pattern ID, description and references to definition
requirements . 63
Table 7-2: Test matrix for qualification and procurement . 66
Table 8-1: Sampling plan for outgoing visual inspection on PCB . 75
Table 8-2: Overview of coupons . 76
Table 9-1: Nonconformance criteria for solderability of PTH . 109
Table 9-2: CAF pattern dimensions – via-to-via straight . 136
Table 9-3: CAF pattern dimensions – via-to-via staggered . 136
Table 9-4: CAF pattern dimensions – via-to-plane . 136
Table 10-1: Annular ring internal . 145
Table 10-2: Annular ring external . 146
Table 10-3: Copper foil thickness . 147
Table 10-4: Copper plating thickness . 148
Table 10-5: Etchback and glass fibre protrusion . 150
Table 10-6: Wicking . 151
Table 10-7: Wrap copper . 152
Table 10-8: Dielectric thickness – standard technology . 153
Table 10-9: Dielectric thickness – microvia layers . 154
Table 10-10: Dimension and aspect of microvias . 155
Table 10-11: Microvia plating voids . 156
Table 10-12: Tin-lead thickness and composition . 157
Table 10-13: Dimensional requirements for electrolytic and chemical Ni, Pd, Au . 159
Table 10-14: Undercut and spurious copper . 160
Table 10-15: Overhang. 162
Table 10-16: Rigid-flex interface -dimensional verification . 163
Table 10-17: Blind, buried and plugged via filling. 166
Table 10-18: Cap lift on blind via and plugged via . 168
Table 10-19: Blind and plugged via planarity . 169
Table 10-20: Burrs and nodules . 170
Table 10-21: Voids and inclusions in copper plating . 171
Table 10-22: Wedge voids . 173
Table 10-23: Resin void . 175
Table 10-24: Delamination, blistering, crazing, measling . 176
Table 10-25: Pad Lift . 177
Table 10-26: Dielectric cracks . 179
Table 10-27: Cracks and separation in copper . 181
Table 10-28: Interconnect defect, ICD .
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