Abstract

This European standard specifies a method for determining the heat resistance of bonds produced by lasting adhesives.

Status
Published
Publication Date
31-Jan-2002
Current Stage
6060 - National Implementation/Publication (Adopted Project)
Start Date
01-Feb-2002
Due Date
01-Feb-2002
Completion Date
01-Feb-2002

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Standard

SIST EN 12964:2002

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SIST EN 12964:2002 is the Slovenian adoption of EN 12964:2001 from CEN. It specifies a laboratory method for determining the heat resistance of bonds made with lasting adhesives for leather and footwear materials. The method is intended for users who need a repeatable way to compare adhesive performance as temperature rises under load.

What does SIST EN 12964:2002 specify?

SIST EN 12964:2002 specifies one test method for measuring how bonds made with lasting adhesives behave when heated. In practice, it gives a controlled way to prepare bonded strips, heat them in a warm air cabinet, and record the temperature at which the bond fails.

The document is organized into clauses on scope, normative references, terms and definitions, principle, safety, apparatus, adhesive, test material, test pieces, procedures and evaluation, and test report. That structure takes the user from sample identification and specimen preparation through testing and result recording.

What are the key requirements of SIST EN 12964:2002?

Test principle and failure mode

SIST EN 12964:2002 measures heat resistance by bonding two strips of cotton canvas test material and heating the assembled test pieces under a constant load. The key result is the temperature at which the bond reaches cohesion (cohesive) failure while the temperature rises at 2 C/min.

In practice, this means the test is not just about whether a bond breaks, but how much heat it can withstand under a defined mechanical load and heating rate. If adhesive failure appears, the test is repeated with a thicker adhesive coating.

Specimen preparation

SIST EN 12964:2002 requires the test material to be conditioned in the standard atmosphere 23/50 and the bonding surfaces to be prepared according to the adhesive supplier's instructions, or cleaned with a hand brush if no instructions are available. The adhesive sample must be identified and prepared in accordance with EN 1066 and EN 1067, and stored at (23 ± 2) C before use.

For liquid adhesives, the standard specifies controlled application timing, drying intervals, activation of the adhesive coat, and pressing at at least (0,6 ± 0,02) MPa for 15 s. For solid lasting adhesives, it specifies cleaning the applicator, applying one coat, and forming the bond within 5 s.

Test conditions and equipment

SIST EN 12964:2002 specifies a warm air cabinet with forced ventilation, a controlled temperature range from 25 C to 300 C, and a temperature rise of 2 C/min. The cabinet must also support clamping and loading of the test pieces with weights from 1,0 kg to 5,0 kg.

This matters because the result depends on stable heating and a known load. Laboratories need equipment that can reproduce the same stress and temperature path for every test.

Result determination and reporting

SIST EN 12964:2002 requires the test to start 5 minutes after bonding is completed. If no load is specified, a preliminary test is used to find a weight that gives a separation time between 10 min and 30 min, and the final test is then run with that load.

The report records the individual and mean temperatures at separation, with the highest and lowest values ignored in the mean, plus the mode of failure. That gives a usable result for quality control and for comparing adhesive batches or formulations.

What terms does SIST EN 12964:2002 define?

  • Lasting adhesive - an adhesive used to bond a shoe upper to a shoe insole during the lasting process.
  • Cohesion (cohesive) failure - failure within the adhesive layer, which is the preferred failure mode in this test.
  • Standard atmosphere 23/50 - the conditioning atmosphere used for the test material before specimen preparation.
  • Test piece - the bonded strip assembly prepared to the specified form and dimensions for heating.
  • Warm air cabinet - the forced-ventilation chamber used to heat the test pieces at a controlled rate.
  • Heat activator - the device used to bring adhesive coats to the activation temperature before bonding.

Who uses SIST EN 12964:2002?

SIST EN 12964:2002 is used by adhesive manufacturers, footwear laboratories, and quality control teams working with leather and footwear materials. It is relevant where lasting adhesives are selected, checked, or compared for resistance to heat during shoe manufacture and material development.

Buyers and quality managers use it when they need test data that can be repeated by another laboratory. Test technicians use it to prepare specimens, run the heating test, and report the separation temperature in a standard form.

What changed in SIST EN 12964:2002 from the previous edition?

SIST EN 12964:2002 is the Slovenian standard identical to EN 12964:2001.

Which standards are used with SIST EN 12964:2002?

  • EN 923 - provides the general adhesive terms and definitions used in the document, including cohesive failure.
  • EN 1066 - covers sampling of adhesives.
  • EN 1067 - covers examination and preparation of samples for testing.
  • ISO 554 - provides the standard atmospheres for conditioning and testing, used here for the test material conditioning step.

What does the SIST EN 12964:2002 document contain?

SIST EN 12964:2002 contains the full test procedure, from apparatus requirements to the final report. It includes the test-piece form and dimensions in Figure 1, and the arrangement for applying solid lasting adhesives in Figure 2.

It also gives the required conditioning, cutting, bonding, activation, pressing, heating, loading, and evaluation steps. The reporting clause lists the adhesive identification, test material identification, bonding procedure, applicator, test type, results, failure mode, deviations, and test date.

Relations

Effective Date
03-Jun-2026
Effective Date
28-Jan-2026
Effective Date
28-Jan-2026
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28-Jan-2026
Effective Date
28-Jan-2026

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Standard

SIST EN 12964:2002

English language (10 pages)
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Frequently Asked Questions

SIST EN 12964:2002 is a standard published by the Slovenian Institute for Standardization (SIST). Its full title is "Adhesives for leather and footwear materials - Lasting adhesives - Testing heat resistance of bonds at increasing temperature". This standard covers: This European standard specifies a method for determining the heat resistance of bonds produced by lasting adhesives.

This European standard specifies a method for determining the heat resistance of bonds produced by lasting adhesives.

SIST EN 12964:2002 is classified under the following ICS (International Classification for Standards) categories: 59.140.30 - Leather and furs; 61.060 - Footwear; 83.180 - Adhesives. The ICS classification helps identify the subject area and facilitates finding related standards.

SIST EN 12964:2002 has the following relationships with other standards: It is inter standard links to SIST ISO 554:1995, SIST EN ISO 15605:2004, SIST EN 1067:2006, SIST EN 915:1996, SIST EN 923:2016. Understanding these relationships helps ensure you are using the most current and applicable version of the standard.

SIST EN 12964:2002 is available in PDF format for immediate download after purchase. The document can be added to your cart and obtained through the secure checkout process. Digital delivery ensures instant access to the complete standard document.

Standards Content (Sample)


2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.Lepila za usnje in obutvene materiale - Trajna lepila - Preskušanje toplotne odpornosti stikov pri povišani temperaturiKlebstoffe für Leder und Schuhwerkstoffe - Zwickklebstoffe - Prüfung der Wärmebeständigkeit von Klebungen bei steigender TemperaturAdhésifs pour cuir et matériaux pour articles chaussants - Adhésifs a haute ténacité - Contrôle de la résistance a la chaleur des joints a une température élevée.Adhesives for leather and footwear materials - Lasting adhesives - Testing heat resistance of bonds at increasing temperature83.180LepilaAdhesives61.060ObuvalaFootwear59.140.30Usnje in krznoLeather and fursICS:Ta slovenski standard je istoveten z:EN 12964:2001SIST EN 12964:2002en01-februar-2002SIST EN 12964:2002SLOVENSKI
STANDARD
EUROPEAN STANDARDNORME EUROPÉENNEEUROPÄISCHE NORMEN 12964April 2001ICS 83.180English versionAdhesives for leather and footwear materials - Lastingadhesives - Testing heat resistance of bonds at increasingtemperatureAdhésifs pour cuir et matériaux pour articles chaussants -Adhésifs à haute ténacité - Contrôle de la résistance à lachaleur des joints à une température élevéeKlebstoffe für Leder und Schuhwerkstoffe - Zwickklebstoffe- Prüfung der Wärmebeständigkeit von Klebungen beisteigender TemperaturThis European Standard was approved by CEN on 1 March 2001.CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this EuropeanStandard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such nationalstandards may be obtained on application to the Management Centre or to any CEN member.This European Standard exists in three official versions (English, French, German). A version in any other language made by translationunder the responsibility of a CEN member into its own language and notified to the Management Centre has the same status as the officialversions.CEN members are the national standards bodies of Austria, Belgium, Czech Republic, Denmark, Finland, France, Germany, Greece,Iceland, Ireland, Italy, Luxembourg, Netherlands, Norway, Portugal, Spain, Sweden, Switzerland and United Kingdom.EUROPEAN COMMITTEE FOR STANDARDIZATIONCOMITÉ EUROPÉEN DE NORMALISATIONEUROPÄISCHES KOMITEE FÜR NORMUNGManagement Centre: rue de Stassart, 36
B-1050 Brussels© 2001 CENAll rights of exploitation in any form and by any means reservedworldwide for CEN national Members.Ref. No. EN 12964:2001 ESIST EN 12964:2002

Page 2EN 12964:2001ContentsPageForeword.31Scope.42Normative references.43Terms and definitions.44Principle.45Safety.46Apparatus.47Adhesive.68Test material.69Test pieces.610Procedures and evaluation.1011Test report.10SIST EN 12964:2002

Page 3EN 12964:2001ForewordThis European Standard has been prepared by Technical Committee CEN/TC 193, "Adhesives", the secretariat ofwhich is held by AENOR.This European Standard shall be given the status of a national standard, either by publication of an identical text orby endorsement, at the latest by October 2001, and conflicting national standards shall be withdrawn at the latestby October 2001.According to the CEN/CENELEC Internal Regulations, the national standards organizations of the followingcountries are bound to implement this European Standard: Austria, Belgium, Czech Republic, Denmark, Finland,France, Germany, Greece, Iceland, Ireland, Italy, Luxembourg, Netherlands, Norway, Portugal, Spain, Sweden,Switzerland and the United Kingdom.SIST EN 12964:2002

Page 4EN 12964:20011 ScopeThis European standard specifies a method for determining the heat resistance of bonds produced by lastingadhesives.2 Normative referencesThis European Standard incorporates by dated or undated reference, provisions from other publications. Thesenormative references are cited at the appropriate places in the text and the publications are listed hereafter. Fordated references, subsequent amendments to or revisions of any of these publications apply to this EuropeanStandard only when incorporated in it by amendment or revision. For undated references the latest edition of thepublication referred to applies (including amendments).EN 923Adhesives — Terms and definitionsEN 1066Adhesives — SamplingEN 1067Adhesives — Examination and preparation of samples for testingISO 554Standard atmospheres for conditioning and/or testing —Specifications3 Terms and definitionsFor the purposes of this standard the terms and definitions in accordance with EN 923, and the following term anddefinition apply.3.1lasting adhesiveadhesive used for bonding a shoe upper to a shoe insole during the lasting process.4 PrincipleStrips of specified length and width are cut from a cotton canvas test material. The lasting adhesive to be tested iscoated onto these strips and two strips are bonded to produce test pieces of a specified form.The heat resistance of the bonds is determined by heating the test pieces to cohesion (cohesive) failure in a warmair cabinet under a specified constant load and at a temperature increasing at a rate of 2 C/min.5 SafetyPersons using this standard shall be familiar with normal laboratory practice.This standard does not purport to address all safety problems, if any, associated with its use.It is the responsibility of the user to establish safety and health practices and to ensure compliance with anyEuropean and national regulatory conditions.6 ApparatusThe items required will depend on the types of materials used:SIST EN 12964:2002

Page 5EN 12964:20016.1 Cutting knifeSharp knife, for cutting test pieces in accordance with 9.3.2. The angle between the inner and outer cutting surfaceshall be approximately 20;6.2 Hand brushFor cleaning the surface of the test material;6.3 Adhesive applicatorTo ensure a uniform and even coating of the adhesive under test using preferably the type of applicatorrecommended by the manufacturer of the adhesive.Unless otherwise specified, for lasting adhesives supplied in liquid form use a brush, a roller or a coating machine,for solid lasting adhesives use an applicator equipped with a melting chamber and an applicator nozzle with thefollowing requirements:a) The melting chamber shall heat the adhesive by an electric device to its application temperature (usuallybetween 100 C and 300 C). The temperature of the nozzle shall be kept within ± 5 C of the specifiedtemperature.b) The applicator shall allow the even distribution of the adhesive over the test piece surface. It shall include an airdriven or mechanical system which produces a controlled dose of the melted adhesive. The use of a nozzle withseveral orifices is recommended as it facilitates the distribution of the melted adhesive over the whole surface ofthe test material.c) During application, the test material shall rest on a mobile carriage/ traveller which allows the application of theadhesive along the length of the test piece at a controlled speed.6.4 Heat activatorFor heating adhesive coats to the required temperature.6.5 Equipment for measurement of temperatureThermocouple, thermoindicator papers or melting powders for measuring the temperature of activated adhesivecoats or a non-contact temperature measurement device.6.6 Pressing deviceProviding an even pressure of up to 0,6 MPa over the whole of the surface to be bonded;6.7 Warm air cabinetWith forced ventilation capable of maintaining temperatures between 25 C and 300 C wit
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