Determination of flash/no flash - Closed cup equilibrium method (ISO 1516:2002)

This International Standard specifies a method to determine if paints, varnishes, paint binders, solvents, petroleum or related products, when maintained at a selected equilibrium temperature and under the conditions of the test, give off sufficient flammable vapour to cause ignition on application of an external source of flame applied in a standard manner.
This International Standard is not applicable to water-borne paints which may, however, be tested using ISO 3680.
The method is suitable for use over the temperature range -30 °C to 110 °C, depending on the use of different apparatus listed in Table 1.
The interpretation of results obtained from solvent mixtures containing halogenated hydrocarbons, should be considered with caution, as these mixtures can give anomalous results.

Flammpunktbestimmung - Ja/Nein-Verfahren - Gleichgewichtsverfahren mit geschlossenem Tiegel (ISO 1516:2002)

Diese Internationale Norm legt ein Verfahren fest, mit dem bestimmt werden kann, ob Beschichtungsstoffe, Bindemittel, Lösemittel, Mineralölerzeugnisse und verwandte Produkte, so sie bei einer gewählten Gleichgewichtstemperatur nach festgelegtem Verfahren temperiert werden, genügend brennbare Dämpfe abgeben, um diese durch eine externe Zündflamme, betätigt nach festgelegtem Verfahren, zu entzünden.
Diese Internationale Norm ist nicht anwendbar auf Wasserlacke; diese können nach ISO 3680 [2] geprüft werden.
Dieses Verfahren ist für einen Temperaturbereich von -30 °C bis 110 °C geeignet, je nach Anwendungsbereich der unterschiedlichen, in Tabelle 1 aufgeführten Prüfeinrichtungen.
Die Ergebnisse von Lösemittelgemischen, die halogenierte Kohlenwasserstoffe enthalten, müssen sehr vorsichtig und kritisch interpretiert werden, da solche Gemische anormale Ergebnisse zeigen können.

Essai de point d'éclair de type passe/ne passe pas - Méthode a l'équilibre en vase clos (ISO 1516:2002)

La présente Norme internationale spécifie une méthode permettant de déterminer si des peintures, vernis, bases de peintures, solvants, produits pétroliers ou produits connexes, maintenus dans les conditions de l'essai à une température d'équilibre choisie, génèrent suffisamment de vapeurs inflammables pour provoquer leur inflammation par présentation d'une flamme externe de manière normalisée.
La présente Norme internationale n'est pas applicable aux peintures renfermant de l'eau; celles-ci peuvent être analysées conformément à l'ISO 3680.
La méthode est applicable dans la gamme de température s'étendant de - 30 °C à 110 °C, en utilisant les différents appareils indiqués dans le Tableau 1.
Il convient de considérer avec circonspection les résultats obtenus sur des mélanges de solvants contenant des hydrocarbures halogénés, ces mélanges pouvant donner des résultats anormaux.

Določevanje pojava plamena - Ravnotežna metoda v zaprti posodi (ISO 1516:2002)

General Information

Status
Published
Publication Date
31-Aug-2002
Current Stage
6060 - National Implementation/Publication (Adopted Project)
Start Date
01-Sep-2002
Due Date
01-Sep-2002
Completion Date
01-Sep-2002

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Standards Content (Sample)

SLOVENSKI STANDARD
SIST EN ISO 1516:2002
01-september-2002
'RORþHYDQMHSRMDYDSODPHQD5DYQRWHåQDPHWRGDY]DSUWLSRVRGL ,62
Determination of flash/no flash - Closed cup equilibrium method (ISO 1516:2002)
Flammpunktbestimmung - Ja/Nein-Verfahren - Gleichgewichtsverfahren mit
geschlossenem Tiegel (ISO 1516:2002)

Essai de point d'éclair de type passe/ne passe pas - Méthode a l'équilibre en vase clos

(ISO 1516:2002)
Ta slovenski standard je istoveten z: EN ISO 1516:2002
ICS:
75.080 Naftni proizvodi na splošno Petroleum products in
general
87.040 Barve in laki Paints and varnishes
SIST EN ISO 1516:2002 en

2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

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SIST EN ISO 1516:2002
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SIST EN ISO 1516:2002
EUROPEAN STANDARD
EN ISO 1516
NORME EUROPÉENNE
EUROPÄISCHE NORM
March 2002
ICS 75.080; 87.040
English version
Determination of flash/no flash - Closed cup equilibrium method
(ISO 1516:2002)

Essai de point d'eclair de type passe/ne passe pas - Flammpunktbestimmung - Ja/Nein-Verfahren -

Méthode à l'équilibre en vase clos (ISO 1516:2002) Gleichgewichtsverfahren mit geschlossenem Tiegel (ISO

1516:2002)
This European Standard was approved by CEN on 1 March 2002.

CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European

Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national

standards may be obtained on application to the Management Centre or to any CEN member.

This European Standard exists in three official versions (English, French, German). A version in any other language made by translation

under the responsibility of a CEN member into its own language and notified to the Management Centre has the same status as the official

versions.

CEN members are the national standards bodies of Austria, Belgium, Czech Republic, Denmark, Finland, France, Germany, Greece,

Iceland, Ireland, Italy, Luxembourg, Malta, Netherlands, Norway, Portugal, Spain, Sweden, Switzerland and United Kingdom.

EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION
EUROPÄISCHES KOMITEE FÜR NORMUNG
Management Centre: rue de Stassart, 36 B-1050 Brussels

© 2002 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN ISO 1516:2002 E

worldwide for CEN national Members.
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SIST EN ISO 1516:2002
EN ISO 1516:2002 (E)
CORRECTED 2002-05-08
Foreword
This document (ISO 1516:2002) has been prepared by Technical Committee ISO/TC 28

"Petroleum products and lubricants" in collaboration with Technical Committee CEN/TC 19

"Petroleum products, lubricants and related products", the secretariat of which is held by

NEN.

This European Standard shall be given the status of a national standard, either by publication

of an identical text or by endorsement, at the latest by September 2002, and conflicting

national standards shall be withdrawn at the latest by September 2002.

According to the CEN/CENELEC Internal Regulations, the national standards organizations of

the following countries are bound to implement this European Standard: Austria, Belgium,

Czech Republic, Denmark, Finland, France, Germany, Greece, Iceland, Ireland, Italy,

Luxembourg, Malta, Netherlands, Norway, Portugal, Spain, Sweden, Switzerland and the

United Kingdom.
Endorsement notice

The text of the International Standard ISO 1516:2002 has been approved by CEN as a

European Standard without any modifications.

NOTE Normative references to International Standards are listed in annex ZA (normative).

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SIST EN ISO 1516:2002
EN ISO 1516:2002 (E)
Annex ZA
(normative)
Normative references to international publications
with their relevant European publications

This European Standard incorporates by dated or undated reference, provisions from other

publications. These normative references are cited at the appropriate places in the text and the

publications are listed hereafter. For dated references, subsequent amendments to or revisions

of any of these publications apply to this European Standard only when incorporated in it by

amendment or revision. For undated references the latest edition of the publication referred to

applies (including amendments).

NOTE Where an International Publication has been modified by common modifications,

indicated by (mod.), the relevant EN/HD applies.
Publication Year Title EN Year
ISO 1523 2002 Determination of flash point - Closed EN ISO 1523 2002
cup equilibrium method
ISO 2719 1988 Petroleum products and lubricants - EN 22719 1993
Determination of flash point -
Pensky-Martens closed cup method
ISO 3170 1998 Petroleum liquids - Manual sampling EN ISO 3170 1998
ISO 3171 1988 Petroleum liquids - Automatic EN ISO 3171 1999
pipeline sampling
ISO 13736 1997 Petroleum products and other liquids EN ISO 13736 1997
- Determination of flash point - Abel
closed cup method
ISO 15528 2000 Paints, varnishes and raw materials EN ISO 15528 2000
for paints and varnishes - Sampling
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SIST EN ISO 1516:2002
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SIST EN ISO 1516:2002
INTERNATIONAL ISO
STANDARD 1516
Third edition
2002-03-01
Determination of flash/no flash — Closed
cup equilibrium method
Essai de point d'éclair de type passe/ne passe pas — Méthode à l'équilibre
en vase clos
Reference number
ISO 1516:2002(E)
ISO 2002
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SIST EN ISO 1516:2002
ISO 1516:2002(E)
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© ISO 2002

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or mechanical, including photocopying and microfilm, without permission in writing from either ISO at the address below or ISO's member body

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ii © ISO 2002 – All rights reserved
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SIST EN ISO 1516:2002
ISO 1516:2002(E)
Contents Page

Foreword.....................................................................................................................................................................iv

Introduction.................................................................................................................................................................v

1 Scope ..............................................................................................................................................................1

2 Normative references....................................................................................................................................1

3 Term and definition .......................................................................................................................................2

4 Principle..........................................................................................................................................................2

5 Chemicals and materials...............................................................................................................................2

6 Apparatus .......................................................................................................................................................2

7 Apparatus preparation ..................................................................................................................................3

8 Sampling.........................................................................................................................................................4

9 Sample handling ............................................................................................................................................4

10 Test temperature............................................................................................................................................5

11 Procedure .......................................................................................................................................................5

12 Expression of results ....................................................................................................................................7

13 Precision.........................................................................................................................................................7

14 Test report ......................................................................................................................................................7

Annex A (informative) Precision data from ISO 1523 ..............................................................................................8

Bibliography................................................................................................................................................................9

© ISO 2002 – All rights reserved iii
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SIST EN ISO 1516:2002
ISO 1516:2002(E)
Foreword

ISO (the International Organization for Standardization) is a worldwide federation of national standards bodies (ISO

member bodies). The work of preparing International Standards is normally carried out through ISO technical

committees. Each member body interested in a subject for which a technical committee has been established has

the right to be represented on that committee. International organizations, governmental and non-governmental, in

liaison with ISO, also take part in the work. ISO collaborates closely with the International Electrotechnical

Commission (IEC) on all matters of electrotechnical standardization.

International Standards are drafted in accordance with the rules given in the ISO/IEC Directives, Part 3.

The main task of technical committees is to prepare International Standards. Draft International Standards adopted

by the technical committees are circulated to the member bodies for voting. Publication as an International

Standard requires approval by at least 75 % of the member bodies casting a vote.

Attention is drawn to the possibility that some of the elements of this International Standard may be the subject of

patent rights. ISO shall not be held responsible for identifying any or all such patent rights.

ISO 1516 was prepared jointly by Technical Committees ISO/TC 28, Petroleum products and lubricants and

ISO/TC 35, Paints and varnishes.

This third edition cancels and replaces the second edition (ISO 1516:1981), which has been technically revised.

Annex A of this International Standard is for information only.
iv © ISO 2002 – All rights reserved
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SIST EN ISO 1516:2002
ISO 1516:2002(E)
Introduction

This International Standard describes one of two closed cup equilibrium methods for carrying out a flash/no flash

test for paints, varnishes, petroleum and related products, and it should be read in conjunction with the second

equilibrium method, ISO 3680 ([2] in the bibliography), when selecting a method.

The determination of the flash point using the same equipment is described in ISO 1523.

This test method does not determine the flash point of the product under test, but merely its behaviour at the

selected equilibrium temperature as may be required to comply with laws or regulations relating to the storage,

transport and use of flammable products. For this purpose, it is unnecessary to determine the exact flash point, but

it is necessary to determine whether or not flashing occurs at a given temperature. By the procedure specified,

differences between test apparatus of various standard designs are minimized by ensuring that the test is carried

out only when the product under test and the air/vapour mixture above it in the test vessel are considered to be in

temperature equilibrium.
© ISO 2002 – All rights reserved v
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SIST EN ISO 1516:2002
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SIST EN ISO 1516:2002
INTERNATIONAL STANDARD ISO 1516:2002(E)
Determination of flash/no flash — Closed cup equilibrium method

WARNING — The use of this International Standard may involve hazardous materials, operations and

equipment. This International Standard does not purport to address all of the safety problems associated

with its use. It is the responsibility of the user of this International Standard to establish appropriate safety

and health practices and determine the applicability of regulatory limitations prior to use.

1 Scope

This International Standard specifies a method to determine if paints, varnishes, paint binders, solvents, petroleum

or related products, when maintained at a selected equilibrium temperature and under the conditions of the test,

give off sufficient flammable vapour to cause ignition on application of an external source of flame applied in a

standard manner.

This International Standard is not applicable to water-borne paints which may, however, be tested using ISO 3680

([2] in the bibliography).

The method is suitable for use over the temperature range – 30 °C to 110 °C, depending on the use of different

apparatus listed in Table 1.

The interpretation of results obtained from solvent mixtures containing halogenated hydrocarbons should be

considered with caution, as these mixtures can give anomalous results.
2 Normative references

The following normative documents contain provisions which, through reference in this text, constitute provisions of

this International Standard. For dated references, subsequent amendments to, or revisions of, any of these

publications do not apply. However, parties to agreements based on this International Standard are encouraged to

investigate the possibility of applying the most recent editions of the normative documents indicated below. For

undated references, the latest edition of the normative document referred to applies. Members of ISO and IEC

maintain registers of currently valid Internationa
...

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