SIST EN 1744-1:2010+A1:2013
(Main)Tests for chemical properties of aggregates - Part 1: Chemical analysis
Tests for chemical properties of aggregates - Part 1: Chemical analysis
This European Standard specifies procedures for the chemical analysis of aggregates. It specifies the reference procedures and, in certain cases, an alternative method which can be considered as giving equivalent results.
Unless otherwise stated, the test methods specified in this standard may be used for factory production control, for audit tests or for type tests.
This standard describes the reference methods used for type testing and in cases of dispute (and alternatives methods) for chemical analyses of aggregates. For the purpose of type testing and in cases of dispute only the reference method should be used. For other purposes, in particular factory production control, other methods may be used provided that an appropriate working relationship with the reference method has been established.
Prüfverfahren für chemische Eigenschaften von Gesteinskörnungen - Teil 1: Chemische Analyse
Diese Europäische Norm legt Verfahren für die chemische Analyse von Gesteinskörnungen fest. Sie legt die Referenzverfahren und in bestimmten Fällen ein Alternativverfahren fest, dessen Ergebnisse als gleichwertig zu denen des Referenzverfahrens angesehen werden.
Sofern nicht anders festgelegt, dürfen die in dieser Norm festgelegten Prüfverfahren für die werkseigene Produktionskontrolle, für Audits oder für Erstprüfungen angewendet werden.
Diese Norm beschreibt für die chemische Analyse von Gesteinskörnungen die für die Erstprüfung und in Streitfällen anzuwendenden Referenzverfahren (sowie Alternativverfahren). Für die Erstprüfung und in Streit-fällen sollte nur das Referenzverfahren angewendet werden. Für andere Zwecke, speziell im Rahmen der werkseigenen Pro¬duktionskontrolle, dürfen andere Verfahren angewendet werden, sofern ein ausreichender Zusammenhang zum Referenzverfahren nachgewiesen wurde.
Essais visant à déterminer les propriétés chimiques des granulats - Partie 1: Analyse chimique
La présente Norme européenne décrit les modes opératoires pour l’analyse chimique des granulats. Elle décrit les modes opératoires de référence et dans certains cas, une méthode alternative donnant des résultats similaires.
Sauf prescription, les méthodes d’essais décrits dans cette norme peuvent être utilisées pour le contrôle de fabrication en usine, pour des essais d’audit ou des essais de type.
Cette norme décrit les méthodes de référence utilisées pour les essais de type et en cas de litige (ainsi que les méthodes alternatives), pour l'analyse chimique des granulats. Pour les essais de type et en cas de litige, seule la méthode de référence sera utilisée. Lorsque d'autres objectifs sont visés, en particulier le contrôle de fabrication en usine, d'autres méthodes peuvent être utilisées, à condition que des corrélation appropriées avec la méthode de référence aient été établies.
Preskusi kemičnih lastnosti agregatov - 1. del: Kemijska analiza
Ta evropski standard določa postopke za kemijsko analizo agregatov. Določa referenčne postopke in v nekaterih primerih alternativno metodo, s katero lahko pridobimo enakovredne rezultate. Če ni navedeno drugače, se lahko preskusne metode iz tega standarda uporabljajo za kontrolo proizvodnje v obratu, zunanje kontrolne preskuse ali tipske preskuse. Ta standard opisuje referenčne metode, ki se uporabljajo za tipsko preskušanje in v primerih spora (in alternativnih metod) za kemijsko analizo agregatov. Za namen tipskega preskušanja in v primerih spora naj bi se uporabljala le referenčna metoda. Za druge namene, zlasti za kontrolo proizvodnje v obratu, se lahko uporabijo druge metode, če obstaja primerna delovna povezava z referenčno metodo.
General Information
- Status
- Published
- Publication Date
- 08-Jan-2013
- Technical Committee
- AGR - Aggregates
- Current Stage
- 6060 - National Implementation/Publication (Adopted Project)
- Start Date
- 07-Dec-2012
- Due Date
- 11-Feb-2013
- Completion Date
- 09-Jan-2013
Relations
- Replaces
SIST EN 1744-1:2010 - Tests for chemical properties of aggregates - Part 1: Chemical analysis - Effective Date
- 01-Feb-2013
- Consolidates
SIST EN 1744-1:2010 - Tests for chemical properties of aggregates - Part 1: Chemical analysis - Effective Date
- 18-Jan-2023
- Consolidates
SIST EN 1744-1:2010/kprA1:2012 - Tests for chemical properties of aggregates - Part 1: Chemical analysis - Effective Date
- 01-Feb-2013
Overview
SIST EN 1744-1:2010+A1:2013 - Tests for chemical properties of aggregates (Part 1: Chemical analysis) is a European standard that specifies reference procedures and accepted alternative methods for the chemical analysis of aggregates. It covers sampling, preparation of test portions, reagents, apparatus, test procedures and expression of results for a range of chemical determinations. The standard is intended for type testing and dispute resolution (reference methods mandatory) and can also be used for factory production control, audit tests or routine testing where an appropriate relationship to the reference method has been established.
Key topics and technical requirements
- Scope and application: Defines when reference vs. alternative methods must be used (type testing/dispute vs. factory production control).
- Reagents and apparatus: Lists required chemicals and laboratory equipment specific to each chemical test.
- Sampling and sample preparation: Procedures for representative sampling, drying and extraction of aggregates prior to analysis.
- Chloride determination: Water-soluble chloride methods including the Volhard (reference) method, potentiometric (alternative) and Mohr (factory control) method.
- Sulfate and sulfur tests: Water-soluble sulfates, acid-soluble sulfates, total sulfur (acid digestion reference and high-temperature combustion alternative).
- Sulfide determination: Acid-soluble sulfide content and procedures to detect potentially reactive sulfide particles.
- Organic and contaminant tests: Tests for humus, fulvo acids, organic contaminants and lightweight contaminators that affect concrete surface finish.
- Free lime and slag assessments: Methods for free CaO determination (complexometry, conductometry, acidimetry) and procedures for assessing expansion potential of steel and blast-furnace slags.
- Quality aspects: Repeatability/reproducibility, expression of mass/volume, treatment of results and special checks (e.g., AgNO3 chloride absence test).
Practical applications and who uses it
- Aggregate producers and quarry operators: To validate product quality and demonstrate compliance with chemical acceptance criteria.
- Construction material laboratories and testing facilities: For type testing, dispute resolution and establishing factory production control methods referenced to the standard.
- Civil and structural engineers, specifiers and contractors: To assess suitability of aggregates for concrete and asphalt, mitigating risks from chlorides, sulfates, sulfides, free lime or deleterious organics.
- Regulators and certification bodies: For conformity assessment, audits and standardised reporting of chemical properties.
Related standards and references
- The standard is published under CEN and adopted nationally (SIST). For broader conformity and performance requirements consult other EN and national standards on aggregate properties and concrete materials; check CEN listings for related parts and updates.
Keywords: SIST EN 1744-1:2010+A1:2013, EN 1744-1, chemical analysis of aggregates, water-soluble chloride, sulfate testing, total sulfur, factory production control, reference methods, Volhard, potentiometry, Mohr.
Frequently Asked Questions
SIST EN 1744-1:2010+A1:2013 is a standard published by the Slovenian Institute for Standardization (SIST). Its full title is "Tests for chemical properties of aggregates - Part 1: Chemical analysis". This standard covers: This European Standard specifies procedures for the chemical analysis of aggregates. It specifies the reference procedures and, in certain cases, an alternative method which can be considered as giving equivalent results. Unless otherwise stated, the test methods specified in this standard may be used for factory production control, for audit tests or for type tests. This standard describes the reference methods used for type testing and in cases of dispute (and alternatives methods) for chemical analyses of aggregates. For the purpose of type testing and in cases of dispute only the reference method should be used. For other purposes, in particular factory production control, other methods may be used provided that an appropriate working relationship with the reference method has been established.
This European Standard specifies procedures for the chemical analysis of aggregates. It specifies the reference procedures and, in certain cases, an alternative method which can be considered as giving equivalent results. Unless otherwise stated, the test methods specified in this standard may be used for factory production control, for audit tests or for type tests. This standard describes the reference methods used for type testing and in cases of dispute (and alternatives methods) for chemical analyses of aggregates. For the purpose of type testing and in cases of dispute only the reference method should be used. For other purposes, in particular factory production control, other methods may be used provided that an appropriate working relationship with the reference method has been established.
SIST EN 1744-1:2010+A1:2013 is classified under the following ICS (International Classification for Standards) categories: 71.040.40 - Chemical analysis; 91.100.15 - Mineral materials and products. The ICS classification helps identify the subject area and facilitates finding related standards.
SIST EN 1744-1:2010+A1:2013 has the following relationships with other standards: It is inter standard links to SIST EN 1744-1:2010, SIST EN 1744-1:2010, SIST EN 1744-1:2010/kprA1:2012. Understanding these relationships helps ensure you are using the most current and applicable version of the standard.
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Standards Content (Sample)
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.Prüfverfahren für chemische Eigenschaften von Gesteinskörnungen - Teil 1: Chemische AnalyseEssais visant à déterminer les propriétés chimiques des granulats - Partie 1: Analyse chimiqueTests for chemical properties of aggregates - Part 1: Chemical analysis91.100.15Mineralni materiali in izdelkiMineral materials and products71.040.40Kemijska analizaChemical analysisICS:Ta slovenski standard je istoveten z:EN 1744-1:2009+A1:2012SIST EN 1744-1:2010+A1:2013en,fr,de01-februar-2013SIST EN 1744-1:2010+A1:2013SLOVENSKI
STANDARDSIST EN 1744-1:20101DGRPHãþD
EUROPEAN STANDARD NORME EUROPÉENNE EUROPÄISCHE NORM
EN 1744-1:2009+A1
November 2012 ICS 91.100.15 Supersedes EN 1744-1:2009English Version
Tests for chemical properties of aggregates - Part 1: Chemical analysis
Essais visant à déterminer les propriétés chimiques des granulats - Partie 1: Analyse chimique
Prüfverfahren für chemische Eigenschaften von Gesteinskörnungen - Teil 1: Chemische Analyse This European Standard was approved by CEN on 17 October 2009 and includes Amendment 1 approved by CEN on 15 October 2012.
CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management Centre has the same status as the official versions.
CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION EUROPÄISCHES KOMITEE FÜR NORMUNG
Management Centre:
Avenue Marnix 17,
B-1000 Brussels © 2012 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN 1744-1:2009+A1:2012: ESIST EN 1744-1:2010+A1:2013
Precision . 60SIST EN 1744-1:2010+A1:2013
EN 932-1, Tests for general properties of aggregates — Part 1: Methods for sampling EN 932-2, Tests for general properties of aggregates — Part 2: Methods for reducing laboratory samples EN 932-5, Tests for general properties of aggregates — Part 5: Common equipment and calibration EN 932-6, Tests for general properties of aggregates — Part 6: Definitions of repeatability and reproducibility EN 933-2, Tests for geometrical properties of aggregates — Part 2: Determination of particle size distribution — Test sieves, nominal size of apertures EN 1015-4, Methods of test for mortar for masonry — Part 4: Determination of consistence of fresh mortar (by plunger penetration) EN 1015-9, Methods of test for mortar for masonry — Part 9: Determination of workable life and correction time of fresh mortar EN 1015-11, Methods of test for mortar for masonry — Part 11: Determination of flexural and compressive strength of hardened mortar EN 1097-6, Tests for mechanical and physical properties of aggregates — Part 6: Determination of particle density and water absorption ISO 384:1978, Laboratory glassware — Principles of design and construction of volumetric glassware ISO 385, Laboratory glassware — Burettes SIST EN 1744-1:2010+A1:2013
NOTE 3 Unless otherwise stated reagent solutions may be assumed to have long-term stability. NOTE 4 All chemicals should be treated as potential poisons with toxic properties and appropriate precautions taken before their use. Always take time to assess possible hazards before starting any procedures and constant attention should be maintained. SIST EN 1744-1:2010+A1:2013
(16,987 ± 0,001) g of the dried silver nitrate, dissolving in water and diluting to 1 l in a volumetric flask (5.3.6). Store the solution in the amber-coloured glass reagent bottle (5.2.14) and protect from prolonged exposure to sunlight. 4.2.2 Thiocyanate (KSCN or NH4SCN) solution, approximately 0,1 mol/l, prepared by dissolving 9,7 g of potassium thiocyanate or 7,6 g ammonium thiocyanate in water and diluting to 1 l in a volumetric flask. Pipette 25 ml of silver nitrate solution (4.2.1) into a conical flask (5.3.5) and add 5 ml of nitric acid (4.2.3) and 1 ml of ammonium iron (III) sulfate indicator solution (4.2.5). Add the thiocyanate solution from a burette (5.2.13) until the first permanent colour change occurs, that is from white opalescence to pale brown. Note the volume of thiocyanate solution added. Calculate the concentration of the thiocyanate solution cT, (in mol/l), from the following equation: cT
=
2,5/V1 (1) where V1 is the volume of thiocyanate added (in ml). Standardize the solution at weekly intervals, or before use if the tests are less frequent. 4.2.3 Nitric acid (HNO3), approximately 6 mol/l, prepared by adding 100 ml of nitric acid (4.1) to 150 ml water, boiling the diluted acid in a fume cupboard (5.2.17) until it is colourless and leave to cool to room temperature. 4.2.4 Chloride free technical grade 3,5-trimethylhexan-1-ol. 4.2.5 Ammonium iron (III) sulfate NH4Fe(SO4)2.12H2O indicator solution, prepared by adding 60 g of water to 50 g ammonium iron (III) sulfate, warming to dissolve, and adding 10 ml nitric acid (4.2.3). Leave the solution to cool to room temperature and store in a glass bottle (5.2.15). SIST EN 1744-1:2010+A1:2013
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La norme SIST EN 1744-1:2010+A1:2013 fixe des procédures précises pour l'analyse chimique des granulats. Elle est conçue pour assurer une cohérence dans les méthodes d'analyse utilisées, ce qui renforce la fiabilité des résultats obtenus. Dans le cadre de son champ d'application, cette norme précise les méthodes de référence qui doivent être employées pour les essais de type et en cas de litige. Cela garantit que les analyses chimiques des granulats soient non seulement standardisées, mais aussi acceptées universellement dans la mesure où elles sont conformes aux spécifications établies. Les méthodes alternatives proposées dans ce document peuvent être considérées comme équivalentes, ce qui offre une flexibilité précieuse tout en maintenant un haut niveau de précision. Un des points forts de cette norme est son application dans le contrôle de production en usine, ce qui permet d'assurer la qualité des granulats tout au long du processus de production. Les méthodes spécifiées peuvent également être utilisées pour des essais d'audit, offrant ainsi une flexibilité supplémentaire tout en maintenant des normes de qualité strictes. La pertinence de la norme SIST EN 1744-1:2010+A1:2013 ne peut être sous-estimée dans le contexte actuel de l'industrie des matériaux de construction, où la qualité et la conformité sont essentielles. Grâce à sa clarté et à la structure de ses procédures, cette norme s'inscrit dans une logique d'amélioration continue et de conformité réglementaire, ce qui est crucial pour les entreprises cherchant à optimiser leurs processus de contrôle qualité tout en respectant les exigences légales.
SIST EN 1744-1:2010+A1:2013 표준은 골재의 화학적 성질에 대한 테스트를 위한 매우 중요한 지침을 제공합니다. 이 표준은 골재의 화학 분석을 위한 절차를 상세히 명시하고 있으며, 특정 경우에 동등한 결과를 제공할 수 있는 대체 방법도 포함되어 있습니다. 표준의 주요 초점은 공장 생산 제어, 감사 테스트 또는 유형 테스트를 위한 테스트 방법으로써 지정된 방법들이 사용될 수 있다는 점입니다. SIST EN 1744-1:2010+A1:2013의 강점은 유형 테스트 및 분쟁 발생 시 사용되는 참조 방법을 상세히 규정하고 있다는 것입니다. 이 표준은 화학 분석의 정확성과 일관성을 보장하기 위해 구체적인 프로토콜을 제시하며, 이를 통해 공정 품질 관리에 필요한 신뢰성을 제공합니다. 또한, 다른 목적으로 사용될 수 있는 방법 또한 허용되지만 이 경우에는 참조 방법과의 적절한 작업 관계가 수립되어 있어야 한다는 점을 강조합니다. 이 표준은 주요한 적합성을 갖추고 있습니다. 기본적으로 공장 생산 제어 및 다양한 테스트 상황에서 활용될 수 있는 신뢰할 수 있는 방법론을 제공합니다. 이는 건설 산업에서 골재의 품질을 보장하고, 최종 제품의 안전성과 내구성을 확보하는 데 필수적입니다. 따라서, SIST EN 1744-1:2010+A1:2013은 화학적 성질의 테스트에 있어 실질적이고 중요하며, 이 분야의 전문가들에게 필수적인 기준으로 자리 잡고 있습니다.
Die Norm SIST EN 1744-1:2010+A1:2013 bietet eine umfassende Grundlage für die chemische Analyse von Gesteinskörnungen. Sie definiert präzise Verfahren zur chemischen Analyse und stellt sicher, dass die Ergebnisse konsistent und zuverlässig sind. Ein herausragendes Merkmal dieser Norm ist die spezifizierte Verwendung von Referenzmethoden, die für Typprüfungen und in Streitfällen entscheidend sind. Die Stärke dieser Norm liegt in ihrer klaren Struktur, die sowohl die Referenzmethoden als auch alternative Methoden umfasst, die als gleichwertig gelten können. Dies erlaubt eine gewisse Flexibilität, insbesondere bei der Verwendung der Tests für die Werkseigenen Produktionskontrollen. Die Möglichkeit, alternative Methoden zu verwenden, sofern eine entsprechende Beziehung zur Referenzmethode hergestellt wurde, unterstützt die Anwendung der Norm in der Praxis. Darüber hinaus ist die Norm von großer Relevanz für die Qualitätssicherung in der Bauindustrie, da sie sicherstellt, dass die chemischen Eigenschaften der Gesteinskörnungen den erforderlichen Standards entsprechen. Dadurch wird das Vertrauen in die Qualität von Baustellenmaterialien gestärkt, was letztendlich zu einer höheren Sicherheit und Langlebigkeit von Bauwerken beiträgt. Zusammengefasst bietet die SIST EN 1744-1:2010+A1:2013 nicht nur klare Anweisungen für die chemische Analyse von Gesteinskörnungen, sondern fördert auch die Anwendung konsistenter und zuverlässiger Testmethoden im Produktionsprozess. Ihre Relevanz in der Industrie macht sie zu einem unverzichtbaren Referenzdokument für Fachleute in der Materialprüfung und Qualitätskontrolle.
SIST EN 1744-1:2010+A1:2013は、骨材の化学的特性に関するテストを規定したヨーロッパ規格です。この標準は、骨材の化学分析の手順を明確に示しており、特にタイプテストおよび紛争が発生した場合に使用されるリファレンス手法を中心に構成されています。また、特定の状況においては同等の結果をもたらすと考えられる代替方法も示しています。 この標準の強みは、骨材の品質管理や工場生産管理において使用できるテスト方法を提供している点です。工場での生産管理や監査テスト、タイプテストの目的で使用できる検査方法が明示されているため、実務における適用性が高いのが特徴です。特に、タイプテストおよび紛争時には、リファレンス手法のみを使用することが推奨されており、そのための明確なガイドラインが設けられています。 また、工場生産管理の目的では、リファレンス手法との適切な作業関係が構築された場合、他の方法の使用が許可されています。これにより、より柔軟なアプローチが可能になり、実際の運用において効率を図ることができます。 このように、SIST EN 1744-1:2010+A1:2013は、骨材の化学分析に関する包括的な指針を提供しており、その適用範囲の広さや実務への関連性の高さから、土木・建設業界において非常に重要なスタンダードとなっています。
The SIST EN 1744-1:2010+A1:2013 standard encompasses a comprehensive framework for the chemical analysis of aggregates, emphasizing clarity and precision in testing methodologies. Its scope is meticulously defined, ensuring that it serves as a reliable reference for professionals in the construction and materials science fields. By specifying both reference procedures and alternative methods, the standard strikes a balance between rigor and practicality, ensuring that users have options while adhering to a robust analytical foundation. One of the primary strengths of this standard is its utility across various applications, including factory production control, audit tests, and type tests. This versatility makes the SIST EN 1744-1:2010+A1:2013 essential for ensuring quality and compliance in aggregate production. The inclusion of alternative methods-while clearly delineated from the reference methods-adds flexibility for users, thereby accommodating diverse operational contexts without compromising on the integrity of results. Particularly important is the guidance around the use of reference methods in disputes and for type testing; the standard mandates that only the reference method be applied in these scenarios, thereby upholding the consistency and reliability of chemical analyses in aggregates. This aspect not only enhances the quality assurance process but also provides a clear protocol for addressing discrepancies, which is invaluable for maintaining industry standards. In summary, the SIST EN 1744-1:2010+A1:2013 standard is a critical resource that addresses the comprehensive chemical analysis of aggregates. Its well-defined scope, combined with the strengths of its flexible testing methods and stringent requirements for dispute resolution, underscores its relevance in ensuring quality control across the aggregates industry. As such, it is a foundational document for anyone involved in the testing and analysis of construction materials, affirming its position as a cornerstone of best practices in this field.
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