71.060 - Inorganic chemicals
ICS 71.060 Details
Inorganic chemicals
Anorganische Chemikalien
Chimie minerale
Anorganske kemikalije
General Information
Frequently Asked Questions
ICS 71.060 is a classification code in the International Classification for Standards (ICS) system. It covers "Inorganic chemicals". The ICS is a hierarchical classification system used to organize international, regional, and national standards, facilitating the search and identification of standards across different fields.
There are 739 standards classified under ICS 71.060 (Inorganic chemicals). These standards are published by international and regional standardization bodies including ISO, IEC, CEN, CENELEC, and ETSI.
The International Classification for Standards (ICS) is a hierarchical classification system maintained by ISO to organize standards and related documents. It uses a three-level structure with field (2 digits), group (3 digits), and sub-group (2 digits) codes. The ICS helps users find standards by subject area and enables statistical analysis of standards development activities.
SIGNIFICANCE AND USE
5.1 This test method is used for determination of the carbon content of water from a variety of natural, domestic, and industrial sources. In its most common form, this test method is used to measure organic carbon as a means of monitoring organic pollutants in industrial wastewater. These measurements are also used in monitoring waste treatment processes.
5.2 The relationship of TOC to other water quality parameters such as chemical oxygen demand (COD) and total oxygen demand (TOD) is described in the literature.4
SCOPE
1.1 This test method covers the determination of total carbon (TC), inorganic carbon (IC), and total organic carbon (TOC) in water, wastewater, and seawater in the range from 0.1 mg/L to 4000 mg/L of carbon.
1.2 This test method was used successfully with reagent water spiked with sodium carbonate, acetic acid, and pyridine. It is the user's responsibility to ensure the validity of this test method for waters of untested matrices.
1.3 This test method is applicable only to carbonaceous matter in the sample that can be introduced into the reaction zone. The syringe needle or injector opening size generally limit the maximum size of particles that can be so introduced.
1.4 In addition to laboratory analyses, this test method may be applied to stream monitoring.
1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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ABSTRACT
This specification covers the requirements for sulfur hexafluoride intended for use as an electrical insulating gas. However, this specification applies only to gas as purchased. Tests for water content, acidity (hydrolyzable fluorides), noncondensable gas and carbon tetrafluoride content, and assay shall be performed and shall conform to the requirements specified.
SCOPE
1.1 This specification applies to sulfur hexafluoride for use as an electrical insulating gas.
Note 1: This specification is intended to apply only to gas as purchased. However, the test methods referred to in this standard may be useful in the evaluation of in-service or used gas. Test Method D2284 may be particularly helpful since many sulfur hexafluoride decomposition products are acidic. Test Method D2284 should not be used to evaluate the total amount of sulfur hexafluoride decomposition nor to identify contaminant species. This can only be done by gas chromatography and similar instrumental techniques.
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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This document specifies a methodology applying poultices for the desalination of porous substrate constituting cultural heritage. The desalination methodology can be applied:
- to salt-loaded porous inorganic materials affected by salt weathering, and/or
- to allow conservation treatments incompatible with soluble salt(s) contamination, or
- to prevent salt damage where contamination is known to be present.
In all cases the desalination aims to decrease the salt content.
Furthermore, this document gives the fundamental requirements for the desalination operation and guidelines for the choice of the most appropriate poultice components according to the characteristics of the substrate and types/quantities of salt(s) present in order to optimize the desalination process.
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SIGNIFICANCE AND USE
4.1 The oil absorption number of a carbon black is related to the processing and vulcanizate properties of rubber compounds containing the carbon black.
SCOPE
1.1 This test method covers the determination of the oil absorption number of carbon black.
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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- Standard10 pagesEnglish languagesale 15% off
This document specifies a methodology applying poultices for the desalination of porous substrate constituting cultural heritage. The desalination methodology can be applied:
- to salt-loaded porous inorganic materials affected by salt weathering, and/or
- to allow conservation treatments incompatible with soluble salt(s) contamination, or
- to prevent salt damage where contamination is known to be present.
In all cases the desalination aims to decrease the salt content.
Furthermore, this document gives the fundamental requirements for the desalination operation and guidelines for the choice of the most appropriate poultice components according to the characteristics of the substrate and types/quantities of salt(s) present in order to optimize the desalination process.
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SIGNIFICANCE AND USE
5.1 This test method may be used for material development, characterization, design data generation, and quality control purposes.
5.2 This test method is primarily concerned with the room temperature determination of the dynamic moduli of elasticity and rigidity of slender rods or bars composed of homogeneously distributed carbon or graphite particles.
5.3 This test method can be adapted for other materials that are elastic in their initial stress-strain behavior, as defined in Test Method E111.
5.4 This basic test method can be modified to determine elastic moduli behavior at temperatures from –75 °C to +2500 °C. Thin graphite rods may be used to project the specimen extremities into ambient temperature conditions to provide resonant frequency detection by the use of transducers as described in 7.1.
SCOPE
1.1 This test method covers determination of the dynamic elastic properties of isotropic and near isotropic carbon and graphite materials at ambient temperatures. Specimens of these materials possess specific mechanical resonant frequencies that are determined by the elastic modulus, mass, and geometry of the test specimen. The dynamic elastic properties of a material can therefore be computed if the geometry, mass, and mechanical resonant frequencies of a suitable (rectangular or cylindrical) test specimen of that material can be measured. Dynamic Young's modulus is determined using the resonant frequency in the flexural or longitudinal mode of vibration. The dynamic shear modulus, or modulus of rigidity, is found using torsional resonant vibrations. Dynamic Young's modulus and dynamic shear modulus are used to compute Poisson's ratio.
1.2 This test method determines elastic properties by measuring the fundamental resonant frequency of test specimens of suitable geometry by exciting them mechanically by a singular elastic strike with an impulse tool. Specimen supports, impulse locations, and signal pick-up points are selected to induce and measure specific modes of the transient vibrations. A transducer (for example, contact accelerometer or non-contacting microphone) senses the resulting mechanical vibrations of the specimen and transforms them into electric signals. (See Fig. 1.) The transient signals are analyzed, and the fundamental resonant frequency is isolated and measured by the signal analyzer, which provides a numerical reading that is (or is proportional to) either the frequency or the period of the specimen vibration. The appropriate fundamental resonant frequencies, dimensions, and mass of the specimen are used to calculate dynamic Young's modulus, dynamic shear modulus, and Poisson's ratio. Annex A1 contains an alternative approach using continuous excitation.
FIG. 1 Block Diagram of Typical Test Apparatus
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
5.1 Thermal diffusivity is an important property required for such purposes as design applications under transient heat flow conditions, determination of safe operating temperature, process control, and quality assurance.
5.2 The flash method is used to measure values of thermal diffusivity (α) of a wide range of solid materials. It is particularly advantageous because of the simple specimen geometry, small specimen size requirements, rapidity of measurement, and ease of handling materials having a wide range of thermal diffusivity values over a large temperature range with a single apparatus. The short measurement times involved reduce the chances of contamination and change of specimen properties due to exposure to high temperature environments.
5.3 Thermal diffusivity results in many cases can be combined with values for specific heat (Cp) and density (ρ) to derive thermal conductivity (λ) from the relation λ = αCpρ. For guidance on converting thermal diffusivity to thermal conductivity, refer to Practice C781.
5.4 This test method described in this guide can be used to characterize graphite for design purposes.
5.5 Test Method E1461 is a more detailed form of this test method described in this guide and has applicability to much wider ranges of materials, applications, and temperatures.
SCOPE
1.1 This guide covers the determination of the thermal diffusivity of carbons and graphite at temperatures up to 500 °C. It is applicable only to small easily fabricated specimens. Thermal diffusivity values in the range from 0.04 cm2/s to 2.0 cm2/s are readily measurable by this guide; however, for the reason outlined in Section 7, for materials outside this range this guide may not be applicable.
1.2 Units—The values stated in SI units are to be regarded as the standard. No other units of measurement are included in this standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
4.1 This test method provides a means for assaying nitric acid, based on total acidity. The concentration of nitric acid is important in many of the uses of nitric acid, including specification compliance and manufacturing control.
SCOPE
1.1 This test method covers determination of the assay of nitric acid by total acidity.
1.2 This test method is suitable for concentrations between approximately 50 % and 70 %, calculated as nitric acid.
1.3 The following applies for the purposes of determining the conformance of the test results using this test method to applicable specifications, results shall be rounded off in accordance with the rounding-off method of Practice E29.
1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Section 8.
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
5.1 Control of silica in boiler feedwater and boiler water is necessary to minimize the formation of scale-forming silicates that decrease heat transfer in the boiler. Volatilization and carryover of silica with the steam may cause hard, glassy siliceous deposits to form on turbine blades that reduce turbine efficiency.
5.2 Colloidal silica that is not removed by boiler water pretreatment processes may be solubilized in the boiler and thus contribute to the dissolved silica concentration in the boiler. Both dissolved and total silica are of interest.
SCOPE
1.1 This test method covers the determination of total silica in water.
1.2 This test method is applicable in the range from 25 μg/L to 250 μg/L of silica as SiO2. Higher concentrations may be determined by decreasing the aliquot volume (see Note 6). Concentration range should not be extended by dilution.
1.3 This test method determines total silica, and does not distinguish between soluble and insoluble forms.
1.4 This test method was tested on reagent water only. It is the user's responsibility to assure the validity of the test method for waters of other matrices.
1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
4.1 This guide is intended to help analysts in the semiconductor industry. Examples of the usefulness of anion monitoring include: (1) determining when ion-exchange resin beds (in water-purification systems) need to be regenerated, and (2) ensuring that anion levels are low enough to allow the water to be used for the manufacture of semiconductor devices.
4.2 To ensure that the anions are indeed at low-ppt levels, it is recommended to check the conductivity of a subsample before proceeding with Section 5 of this guide. This check does not need to be exact; its purpose is simply to let the analyst know if the conductivity is higher than that of the highest-level standard solution being tested. Any high reading signifies that the sample, if analyzed, might contaminate the instrument.
SCOPE
1.1 This guide applies to ultrapure water that is thought to contain low ppt (parts-per-trillion, weight/weight) levels of anionic contaminants (for example, bromide, chloride, fluoride, nitrate, nitrite, phosphate, and sulfate). To minimize carry-over problems between analyses, it is best to limit the concentration of any one contaminant to approximately 200 ppt (although this limit is only an approximation and may vary, depending on the user’s application).
1.2 This guide is intended to help analysts avoid contamination of ultrapure-water samples, since contamination control is the primary challenge when quantifying ppt-level anions in grab samples.
1.3 This guide does not include recommendations for collecting samples from the water source.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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ABSTRACT
This specification covers muriatic acid, also known as technical grade hydrochloric acid. This specification includes requirements for muriatic acid available commercially in 20° Baumé and 22° Baumé concentration grades. Muriatic acid shall conform to the following chemical and physical requirements: total acidity of hydrochloric acid; iron content; and Baume gravity. To determine the requirements, a test shall be performed in accordance to the test method.
SCOPE
1.1 This specification covers muriatic acid, also known as technical grade hydrochloric acid.
1.2 The following applies to all specified limits in this specification: for purposes of determining conformance with this specification, an observed value or a calculated value shall be rounded off “to the nearest unit” in the last right hand digit used in expressing the specification limit, in accordance with the rounding-off method of Practice E29.
1.3 This specification includes requirements for muriatic acid available commercially in 20° Baumé and 22° Baumé concentration grades.
1.4 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.
1.5 Review the current Safety Data Sheets (SDS) for detailed information concerning toxicity, first aid procedures, handling, and safety precautions. Consult current OSHA regulations, suppliers’ Safety Data Sheets, and local regulations for all materials used in this specification.
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SCOPE
1.1 This standard covers terminology relating to industrial and specialty chemicals. It is intended to provide an understanding of terms commonly used in test methods, practices, and specifications throughout the industry.
Note 1: The boldface numbers following each definition refer to E15 standards in which the definition appears. Lightface numbers refer to the E15 subcommittee having jurisdiction.
1.2 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
3.1 These test methods provide for the classification of various grades of sulfuric acid and for the determination of various impurities. Acid strength and impurity levels are important factors in many uses of sulfuric acid.
SCOPE
1.1 These test methods cover the analysis of sulfuric acid.
1.2 The following applies for the purposes of determining the conformance of the test results using this test method to applicable specifications, results shall be rounded off in accordance with the rounding-off method of Practice E29.
1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.
1.4 The analytical procedures appear in the following order:
Sections
Total Acidity
8 to 16
Baumé Gravity
17 to 26
Nonvolatile Matter
27 to 33
Iron
34 to 43
Sulfur Dioxide
44 to 51
Arsenic
52 to 61
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Consult current OSHA regulations, suppliers’ Safety Data Sheets, and local regulations for all materials used in this specification. Specific hazards statements are given in Section 5.
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
3.1 These test methods provide for the classification of various grades of hydrochloric acid and for the determination of various impurities. Acid strength and impurity levels are important factors in many uses of hydrochloric acid.
SCOPE
1.1 These test methods cover the analysis of hydrochloric acid.
1.2 The following applies for the purposes of determining the conformance of the test results using this test method to applicable specifications, results shall be rounded off in accordance with the rounding-off method of Practice E29.
1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.
1.4 The analytical procedures appear in the following order:
Sections
Total Acidity
8 to 16
Baumé Gravity
17 to 26
Sulfated Ash
27 to 34
Iron
35 to 44
Color
45 to 52
Total Sulfur
53 to 59
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Consult current OSHA regulations, suppliers’ Safety Data Sheets, and local regulations for all materials used in this specification. Specific hazards statements are given in Section 5, 30.1, 39.7, and 48.4.
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
4.1 This test method is applicable only for determination of the volatile moisture content resulting from adsorption of water vapor from the atmosphere, and is not intended to give representative moisture data for graphite that has been exposed to liquid water contamination.
SCOPE
1.1 This test method provides a practical determination for the percentage of moisture in a graphite sample.
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
4.1 This test method provides a practical estimate of nonburnable residues in commercially available graphite materials. The ash values determined by this test method are of use in comparing the relative purity of various grades of graphite. To facilitate use, this test method institutes simplifications that preclude the ability to determine absolutely the ash values of the test graphite material due to uncontrolled sources of trace contamination.
4.2 This test method is not intended for use in determining the ash content of purified graphites, for example, nuclear materials. The relationship between the mineral content of a graphite sample and the ash content of that sample is unknown and is not determined by the application of this test method.
SCOPE
1.1 This test method provides a practical determination for the ash content in a graphite sample.
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
5.1 This test method is applicable to cementitious mixtures that have not been exposed to external chloride ions, other than the negligible quantity of chloride ion exposure from sample preparation using potable water, prior to the test.
5.2 The calculation procedure described in this test method is applicable only to laboratory test specimens exposed to a sodium chloride solution as described in this test method. This calculation procedure is not applicable to specimens exposed to chloride ions during cyclic wetting and drying.
Note 1: The diffusion of ionic species in concrete occurs within the fluid-filled pores, cracks and void spaces. The concentration and valence of other ionic species in the pore fluid also influence the rate of chloride diffusion, and therefore, the apparent diffusion coefficient as determined by this test procedure.
5.3 In most cases, the value of the apparent chloride diffusion coefficient for cementitious mixtures changes over time (see Note 2). Therefore, apparent diffusion coefficients obtained at early ages may not be representative of performance in service.
Note 2: The rate of change of the apparent diffusion coefficient for cementitious mixtures containing pozzolans or blast-furnace slag is typically different than that for mixtures containing only portland cement.
5.4 The apparent chloride diffusion coefficient is used in Fick's second law of diffusion to estimate chloride penetration into cementitious mixtures that are in a saturated condition.
5.5 The apparent chloride diffusion coefficient is commonly used in chloride ingress models based on Fick's second law of diffusion. The apparent diffusion coefficient determined by this method includes bound chloride, so proper use of the apparent chloride diffusion coefficient to predict chloride ingress requires consideration of chloride binding.
5.6 The resistance to chloride penetration is affected by such factors as the environment, finishing, mixture composition, w...
SCOPE
1.1 This test method covers the laboratory determination of the apparent chloride diffusion coefficient for hardened cementitious mixtures.
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
2.1 This terminology ensures that terms peculiar to activated carbon are adequately defined so that other standards in which such terms are used can be understood and interpreted properly.
2.2 This terminology is useful to those who are not conversant with the terms related to activated carbon. However, it is also a ready reference for those directly associated with activated carbon to resolve differences and ensure commonality of usage, particularly in the preparation of ASTM standards.
2.3 Although this terminology is intended to promote uniformity in the usage of terms related to activated carbon, it can never be complete because new terms are constantly arising. The existence of this terminology does not preclude the use or misuse of any term in another context.
SCOPE
1.1 This terminology covers terms particularly related to activated carbon and encompasses finished products, applications, and testing procedures.
1.2 When any of the definitions in this terminology is quoted or published out of context, editorially insert the limiting phrase “in activated carbon” after the dash following the term to properly limit the field of application of the term and definition.
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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ABSTRACT
This specification provides the chemical and physical properties and requirements for nuclear-grade aluminum oxide powder intended for fabrication into shapes for nuclear applications. The materials shall conform to physical requirements as to particle size distribution, and specific surface area, and chemical requirements as to loss-on-ignition, and total and elemental concentrations of all impurities. Impurities may include silicaon, iron-chromium-nickel, magnesium, sodium, calcium, hafnium, fluorine, fluorine-chlorine-iodine-bromine, gadolinium, samarium, europium, and dysprosium.
SCOPE
1.1 This specification provides the chemical and physical requirements for nuclear-grade aluminum oxide powder intended for fabrication into shapes for nuclear applications. Two specific uses for which this powder is intended are Al2O3 pellets and Al2O3 − B4C composite pellets for use as thermal insulator or burnable neutron absorbers, respectively.
1.2 The material described herein shall be particulate in nature.
1.3 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SCOPE
1.1 This specification defines the physical and chemical requirements for zirconium oxide powder intended for fabrication into shapes, either entirely or partially of zirconia, for use in a nuclear reactor core.
1.2 The material described herein shall be particulate in nature.
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SCOPE
1.1 This specification defines the physical and chemical requirements for hafnium oxide powder intended for fabrication into shapes for use in a nuclear reactor core.
1.2 The material described herein shall be particulate in nature.
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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ABSTRACT
This specification applies to pellets of stabilized zirconium oxide used in nuclear reactors. The chemical composition requirements such as the stabilizing additive (calcium oxide or yttrium oxide), analytical chemistry methods, impurity concentration (including hafnium, boron, gadolinium, samarium, europium, dysprosium, cobalt, silicon, iron, calcium, magnesium, aluminum, titanium, thorium, fluorine, chlorine, bromine, iodine, and hydrogen), and moisture concentration are prescribed. The nuclear grade pellets shall conform to the specified physical requirements which includes the following: physical dimensions, density, mechanical properties and test methods such as compressive test and thermal cycling test, and visual appearance such as end chips, circumferential chips, cracks, and fissures. The requirements for cleanliness before and after sampling and packaging are given.
SCOPE
1.1 This specification applies to pellets of stabilized zirconium oxide used in nuclear reactors.
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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ABSTRACT
This specification covers the properties and requirements for pellets of stabilized cubic hafnium oxide used in nuclear reactors. Hafnium oxide should consist of a stabilizing agent, the recommended of which is yttrium oxide, though others such as calcium oxide and magnesium oxide may also be used as agreed upon by the buyer and seller. The material shall meet specified values of the following requirements: physical dimensions; density; mechanical properties; phase stabilization; impurity concentration limits; moisture concentration limit; visual appearance; end and circumferential chips; cracks; and fissures and other defects.
SCOPE
1.1 This specification applies to pellets of stabilized cubic hafnium oxide used in nuclear reactors.
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
5.1 Representative samples of industrial chemicals are required for the determination of chemical and physical properties which are used to establish standard volumes, prices, and compliance with commercial and regulatory specifications.
5.2 The objective of sampling is to obtain a small portion (spot sample) of material from a selected area within a container which is representative of the material in the area or, in the case of running or all-level samples, a sample whose composition is representative of the total material in the container. A series of spot samples may be combined to create a representative sample.
5.3 Manual and Automatic Sampling Considerations—The selection of manual or automatic sampling devices is part of establishing a sampling plan applied under all conditions within the scope of this practice provided that the proper sampling procedures are followed. Both types of sampling are commonly used for liquid, solid, and slurry sampling and require adherence to the following:
5.3.1 An adequate frequency of sampling must be selected.
5.3.2 The equipment to support manual or automatic sampling systems may be obtained commercially, fabricated from the designs presented in this practice, or constructed as needed to satisfy process design or other specific requirements.
5.3.3 The sampling equipment must be maintained on a regular basis, and the sampling plan adopted must be strictly followed.
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1.1 This practice covers procedures for sampling several classes of industrial chemicals. It also includes recommendations for determining the number and location of such samples, to ensure their being representative of the lot in accordance with accepted probability sampling principles.
1.2 Although this practice describes specific procedures for sampling various liquids, solids, and slurries, in bulk or in packages, these recommendations only outline the principles to be observed. They should not take precedence over specific sampling instructions contained in other ASTM product or method standards.
1.3 These procedures are covered as follows:
Sections
Statistical Considerations
7 – 11
Simple Liquids
12 – 27
Solids
28 – 35
Slurries
36 – 41
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Sections 6, 19, 20, 30, 34 and 37.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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1.1 This specification applies to pellets of aluminum oxide that may be ultimately used in a reactor core, for example, as filler or spacers within fuel, burnable poison, or control rods. In order to distinguish between the subject pellets and “burnable poison” pellets, it is established that the subject pellets are not intended to be used as neutron-absorbing material.
1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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1.1 This terminology covers a compilation of definitions of technical terms used in the recovered carbon black industry. Terms that are generally understood or adequately defined in other readily available sources are not included.
1.2 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
4.1 The total carbon content of a carbon black is a requirement for the calculation and reporting of carbon dioxide emissions. It can also be used in calculations to estimate yield of the process.
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1.1 This test method covers the instrumental determination of carbon content in a carbon black sample. Values obtained represent the total carbon content.
1.2 The method is applicable to tread, carcass and specialty type carbon blacks obtained from partial combustion or thermal decomposition processes, which typically contain 95 to 100 % carbon.
1.3 The results of these tests can be expressed as mass % carbon.
1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
4.1 General—This guide contains information regarding the use of AOPs to oxidize and eventually mineralize hazardous materials that have entered surface and groundwater as the result of a spill. These guidelines will only refer to those units that are currently applied at a field scale level. The user should review applicable state regulations and guidance on the applicability of AOP (see California DTSC 2010, New Jersey DEP 2017, Oklahoma DEQ 2017).
Note 1: Commercialization of AOP for the treatment of wastewater and process water is fairly mature. Several transnational companies offer mobile and large-scale processing units for the treatment of persistent chemicals of concern. Standard Guides D5745, E2081, and E2616 may be useful. Fig. 1 illustrates the general AOP process.
FIG. 1 Schematic Illustration of Hydroxyl Radical's Generation for the Degradation of Organic Pollutants
Source: Amor, Carlos, et al. Application of Advanced Oxidation Processes for the Treatment of Recalcitrant Agro-Industrial Wastewater: A Review. Water 2019, 11(2), 205; https://doi.org/10.3390/w11020205 (open access publication)
Fig. 2 illustrates the range of AOP technologies.
FIG. 2 Examples of Advanced Oxidation Processes
Source: Amor, Carlos, et al. Application of Advanced Oxidation Processes for the Treatment of Recalcitrant Agro-Industrial Wastewater: A Review. Water 2019, 11(2), 205; https://doi.org/10.3390/w11020205 (open access publication)
4.2 Oxidizing Agents:
4.2.1 Hydroxyl Radical (OH)—The OH radical is the most common oxidizing agent employed by this technology due to its powerful oxidizing ability. When compared to other oxidants such as molecular ozone , hydrogen peroxide, or hypochlorite, its rate of attack is commonly much faster. In fact, it is typically one million (106) to one billion (109) times faster than the corresponding attack with molecular ozone (Keller and Reed, 1991 (1)).9 The three most common methods for generating the hydroxyl radical ar...
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1.1 This guide covers the considerations for advanced oxidation processes (AOPs) in the mitigation of spilled chemicals and hydrocarbons dissolved into ground and surface waters.
1.2 This guide addresses the application of advanced oxidation alone or in conjunction with other technologies.
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
In addition, it is the responsibility of the user to ensure that such activity takes place under the control and direction of a qualified person with full knowledge of any potential safety and health protocols.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
5.1 Two- and three-parameter formulations exist for the Weibull distribution. This practice is restricted to the two-parameter formulation. An objective of this practice is to obtain point estimates of the unknown Weibull distribution parameters by using well-defined functions that incorporate the failure data. These functions are referred to as estimators. It is desirable that an estimator be consistent and efficient. In addition, the estimator should produce unique, unbiased estimates of the distribution parameters (6). Different types of estimators exist, such as moment estimators, least-squares estimators, and maximum likelihood estimators. This practice details the use of maximum likelihood estimators.
5.2 Tensile and flexural specimens are the most commonly used test configurations for graphite. The observed strength values depend on specimen size and test geometry. Tensile and flexural test specimen failure data for a nearly isotropic graphite (7) is depicted in Fig. 1. Since the failure data for a graphite material can be dependent on the test specimen geometry, Weibull distribution parameter estimates (m, Sc) shall be computed for a given specimen geometry.
FIG. 1 Failure Strengths for Tensile Test Specimens (left) and Flexural Test Specimens (right) for a Nearly Isotropic Graphite (7)
5.3 The bias and uncertainty of Weibull parameters depend on the total number of test specimens. Variability in parameter estimates decreases exponentially as more specimens are collected. However, a point of diminishing returns is reached where the cost of performing additional strength tests may not be justified. This suggests a limit to the number of test specimens for determining Weibull parameters to obtain a desired level of confidence associated with a parameter estimate. The number of specimens needed depends on the precision required in the resulting parameter estimate or in the resulting confidence bounds. Details relating to the computation of confidence bo...
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1.1 This practice covers the reporting of uniaxial strength data for graphite and the estimation of probability distribution parameters for both censored and uncensored data. The failure strength of graphite materials is treated as a continuous random variable. Typically, a number of test specimens are failed in accordance with the following standards: Test Methods C565, C651, C695, C749, Practice C781 or Guide D7775. The load at which each specimen fails is recorded. The resulting failure stresses are used to obtain parameter estimates associated with the underlying population distribution. This practice is limited to failure strengths that can be characterized by the two-parameter Weibull distribution. Furthermore, this practice is restricted to test specimens (primarily tensile and flexural) that are primarily subjected to uniaxial stress states.
1.2 Measurements of the strength at failure are taken for various reasons: a comparison of the relative quality of two materials, the prediction of the probability of failure for a structure of interest, or to establish limit loads in an application. This practice provides a procedure for estimating the distribution parameters that are needed for estimating load limits for a particular level of probability of failure.
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
3.1 This test method is primarily concerned with the oxidation mass loss of manufactured carbon and graphite materials in air at temperatures from 371 °C to 677 °C.
3.2 The test method will provide acceptable results at preselected test temperatures that yield less than 10 % mass loss in 100 h. These results can be used to determine relative service temperatures.
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1.1 This test method provides a comparative oxidation mass loss of manufactured carbon and graphite materials in air.
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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ABSTRACT
This specification covers technical grade calcium chloride typically used for, but not limited to, dust control, stabilization, ice/snow removal, other road-conditioning purposes, acceleration of the set of concrete, and as a desiccant. Two types of calcium chloride are covered, as follows: Type S (solid), flake, pellet, or granular calcium chloride in varying concentrations; and Type L (liquid), water solutions of calcium chloride in varying concentrations. Concentrations shall be expressed as a percentage of the total. Impurities such as alkali chlorides, magnesium, and calcium hydroxide should be within specified composition limits.
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1.1 This specification covers calcium chloride, technical grade, typically used for, but not limited to, dust control, stabilization, ice/snow removal, other road-conditioning purposes, acceleration of the set of concrete, and as a desiccant.
1.2 The values stated in SI units are to be regarded as the standard.
1.3 For purposes of determining conformance to this specification, values for chemical analysis shall be rounded to the nearest 0.1 %, and values for grading shall be rounded to the nearest 1 %, in accordance with the rounding method in Practice E29.
1.4 The text of this standard references notes and footnotes, which provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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1.1 This specification covers average or minimum wall thickness electric resistance welded (ERW) tubing to be used for boilers, heat exchangers, condensers, and similar heat-transfer apparatus.
1.2 The tubing sizes and thicknesses usually furnished to the specification are 0.375 in. [9.5 mm] inside diameter (ID) to 1.5 in. [38 mm] outside diameter (OD) and 0.020 to 0.079 in. [0.5 to 2 mm], inclusive, in wall thickness. Tubing having other dimensions may be furnished provided such tubes comply with all other requirements of this specification.
1.3 The steel materials shall have the (1) external tube surface, (2) internal tube surface, or (3) both internal and external tube surfaces textured to improve heat transfer or fluid flow or both. Textured surface(s) are produced by cold forming a specified configuration on the surface(s) of base strip material before welding.
1.4 Optional supplementary requirements are provided and, when desired, shall be so stated on the purchase order.
1.5 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. Within the text, the SI units are shown in brackets. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard. The inch-pound units shall apply unless the “M” designation (SI) of the product specification is specified in the order.
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
5.1 This test method can be used to measure the rate of oxidation for various grades of manufactured carbon and graphite in standard conditions, and can be used for quality control purposes.
5.2 The following conditions are standardized in this test method: size and shape of the graphite specimens; their placement in the vertical furnace with upwards air flow; the method for continuous weight variation measurement using an analytical scale with under-the-scale port; the air flow rate, which must be high enough to ensure that oxidation is not oxygen-starved at the highest temperature used; the initial and final points on the weight loss curve used for calculation of oxidation rate.
5.3 This test method also provides kinetic parameters (apparent activation energy and logarithm of pre-exponential factor) for the oxidation reaction, and a standard oxidation temperature. The results characterize the effect of temperature on oxidation rates in air, and the oxidation resistance of machined carbon or graphite specimens with standard size and shape, in the kinetic, or chemically controlled, oxidation regime. This information is useful for discrimination between material grades with different impurity levels, grain size, pore structure, degree of graphitization, or antioxidation treatments, or a combination thereof.
5.4 Accurately determined kinetic parameters, like activation energy and logarithm of pre-exponential factor, can be used for prediction of oxidation rates in air as a function of temperature in conditions similar to those of this test method. However, extrapolation of such predictions outside the temperature range where Arrhenius plots are linear (outside the kinetic or chemically controlled regime of oxidation) should be made with extreme caution. In conditions where (1) oxidation rates become controlled by a mechanism other than chemical reactions (such as in-pore diffusion or boundary transport of the oxidant gas), or (2) the oxidant supply rate is no...
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1.1 This test method recommends a standard procedure for measuring oxidation rates in air of various grades of nuclear graphite and/or manufactured carbon. Following the standard procedure recommended here, one can obtain kinetic parameters that characterize the oxidation resistance in standard conditions of tested materials and that can be used to for materials selection and qualification, and for quality control purposes in the fabrication process.
1.2 This test method covers the rate of oxidative weight loss per exposed nominal geometric surface area, or per initial weight of machined test specimens of standard size and shape, or both. The test is valid in the temperature range where the rate of air oxidation of graphite and manufactured carbon is limited by reaction kinetics.
1.3 This test method also provides a standard oxidation temperature (as defined in 3.1.7), and the kinetic parameters of the oxidation reaction, namely the apparent activation energy and the logarithm of pre-exponential factor in Arrhenius equation. The kinetic parameters of Arrhenius equation are calculated from the temperature dependence of oxidation rates measured over the temperature range where Arrhenius plots (as defined in 3.1.8) are linear, which is defined as the “kinetic” or “chemical control” oxidation regime. For typical nuclear grade graphite materials it was found that the practical range of testing temperatures is from about 500 °C to 550 °C up to about 700 °C to 750 °C.
1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.6 This international s...
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SIGNIFICANCE AND USE
4.1 CCl4 and CHCl3 may be present in trace amounts in liquid chlorine. The use of chlorine to purify water would then transfer these compounds to the water. Therefore, when the concentrations of the CCl4 and CHCl3 in the liquid chlorine are known, the maximum amounts contributed to the water by the chlorine can be estimated.
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1.1 This test method is designed for the determination of carbon tetrachloride (CCl4) and chloroform (CHCl3) in liquid chlorine. The lower limit of detection is dependent on the sample size and the instrument used; five ppm (w/w) is achievable.
1.2 In determining the conformance of the test results using this method to applicable specifications, results shall be rounded off in accordance with the rounding-off method of Practice E29.
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific hazards statements are given in Section 7 and in 9.2.3.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
5.1 The copper oxides layer present on the surface of the copper rod has a detrimental effect on both final surface quality of the copper wire produced by cold drawing of the rod, and on the drawing process itself leading to wire breaks and excessive wear of the drawing dies. Thus, it is critical to use adequate cleaning techniques during the copper rod manufacturing process in order to limit the depth of the residual copper oxide layer on the finished rod, and it is necessary to have a method to accurately measure the copper oxide depth.
5.2 This test method is the most common test method used by continuous casting and rolling mills to measure the depth of residual surface oxides after the copper rod has been cleaned.
5.3 Applicability of the test method for any other purpose or product has not been evaluated. Suitability beyond the stated scope shall be evaluated before use.
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1.1 This specification established a quantitative, laboratory conducted, electrolytic reduction method to determine the thickness of surface copper oxide films on copper rod produced to Specification B49 for further fabrication into electrical conductors.
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
5.1 The sulfur print reveals the distribution of sulfur as sulfide inclusions in the specimen. The sulfur print complements macroetch methods by providing an additional procedure for evaluating the homogeneity of a steel product.
5.2 Sulfur prints of as-cast specimens generally reveal the solidification pattern and may be used to assess the nature of deoxidation, that is, rimming action versus killed steel sulfur distributions.
5.3 Sulfur prints will reveal segregation patterns, including refilled cracks, and may reveal certain physical irregularities, for example, porosity or cracking.
5.4 The nature of metal flow, such as in various forging operations, can be revealed using sulfur prints of specimens cut parallel to the metal flow direction.
5.5 The sulfur print method is suitable for process control, research and development studies, failure analysis, and for material acceptance purposes.
5.6 The intensity of the sulfur print is influenced by the concentration of sulfur in the steel, the chemical composition of the sulfide inclusions, the aggressiveness of the aqueous acid solution, and the duration of the contact printing between the acid soaked emulsion coated paper and the ground surface of the specimen (this time is the order of seconds rather than minutes). Very low sulfur content steels will produce too faint an image to be useful for macrostructural evaluations. Selection of appropriate printing practices including selection of type of emulsion coated media, acid type and strength, will yield satisfactory prints. Very faint images in the sulfur print can be made more visible by scanning the sulfur print into a PC, and using a photo editor to increase the color saturation. Steels with compositions that produce predominantly titanium or chromium sulfides will not produce useful images.
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1.1 This practice provides information required to prepare sulfur prints (also referred to as Baumann Prints) of most ferrous alloys to reveal the distribution of sulfide inclusions.
1.2 The sulfur print reveals the distribution of sulfides in steels with bulk sulfur contents between about 0.010 and 0.40 weight percent.
1.3 Certain steels contain complex sulfides that do not respond to the test solutions, for example, steels containing titanium sulfides or chromium sulfides.
1.4 The sulfur print test is a qualitative test. The density of the print image should not be used to assess the sulfur content of a steel. Under carefully controlled conditions, it is possible to compare print image intensities if the images are formed only by manganese sulfides.
1.5 The sulfur print image will reveal details of the solidification pattern or metal flow from hot or cold working on appropriately chosen and prepared test specimens.
1.6 This practice does not address acceptance criteria based on the use of the method.
1.7 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.8 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific precautionary statements, see Section 9.
1.9 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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This document specifies a thermal pre-ageing procedure for leather to obtain indications about the tendency to the formation of hexavalent chromium under specified conditions and the determination of hexavalent chromium according to ISO 17075‑1 or ISO 17075‑2.
This thermal pre-ageing procedure does not simulate any real condition in leather production or use.
It is applicable to all types of chromium tanned leather.
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SIGNIFICANCE AND USE
5.1 The molten salt reactor is a nuclear reactor which uses graphite as reflector and structural material and fluoride molten salt as coolant. The graphite components will be submerged in the molten salt during the lifetime of the reactor. The porous structure of graphite may lead to molten salt permeation, which can affect the thermal and mechanical properties of graphite. Consequently, it is important to assess the effect of impregnation of molten salt on the properties of the as-manufactured graphite material.
5.2 The purpose of this guide is to report considerations that should be included in the preparation of graphite specimens representative of that after exposure to a molten salt environment. The degree to which the molten salt will infiltrate the graphite will depend upon a number of factors, including the type of graphite and the type and extent of porosity, the properties of the molten salt, the impregnation pressure and temperature, and the duration of the exposure of the graphite to the molten salt.
5.3 The user of this guide will need to select impregnation parameters sufficiently representative of those in a molten salt reactor based on parameters provided by the designer. Alternatively, the user may select a standard set of impregnation conditions to allow comparisons across a range of graphites.
5.4 This guide is not intended to be prescriptive. A typical apparatus and associated procedure are described. Some indication of the sensitivity of the procedure to graphite type and impregnation conditions is given in He, et al.5
5.5 There are four major practical issues that must be addressed during the impregnation process:
5.5.1 The density of molten salt is greater than that of graphite. A specially designed tool is required to submerge graphite samples in the molten salt during the impregnation process.
5.5.2 Some molten salts (for example, FLiBe) are poisonous and it is therefore necessary to provide containment by performing proced...
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1.1 This guide covers procedures for the impregnation of graphite with molten salt under a consistent pressure and temperature. Such procedures are necessary if the user wishes to prepare graphite specimens for testing that represent material that has been exposed to a molten salt environment in a molten salt nuclear reactor. The user will need to ensure that impregnation temperature and pressure conditions reflect those pertaining to the molten salt environment, noting that the properties of the material will change once it becomes irradiated.
Note 1: The term impregnation is used throughout this guide as this is the correct term for the described process. Other terms such as infiltration and intrusion may be encountered by the user in other texts and the term intrusion is commonly used to describe penetration of open porosity in graphite in a molten salt reactor environment.
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this guide.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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ABSTRACT
This specification covers industrial grade chlorine normally available as a liquid in pressurized metal containers. Liquid chlorine shall conform to the following requirements: gaseous impurities content, moisture content, and nonvolatile material content.
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1.1 This specification covers industrial grade chlorine normally available as a liquid in pressurized metal containers.
1.2 The following applies to all specified limits in this specification: for purposes of determining conformance with this specification, an observed value or a calculated value shall be rounded off “to the nearest unit” in the last right-hand digit used in expressing the specification limit, in accordance with the rounding-off method of Practice E29.
1.3 Units—The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.
1.4 Review the current Safety Data Sheets (SDS) for detailed information concerning toxicity, first aid procedures, handling and safety precautions.
1.5 The following safety hazards caveat pertains only to the test methods listed in Sections 3 and 4. This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
5.1 The Molten Salt Reactor is a nuclear reactor which uses graphite as reflector and structural material, and molten salt as coolant. The graphite components will be submerged in the molten salt during the lifetime of the reactor. The porous structure of graphite may lead to molten salt permeation, which can affect the thermal and mechanical properties of graphite. Consequently, it may be necessary to measure the various strengths of the manufactured graphite materials after impregnation with molten salt and before exposure to the reactor environment in a range of test configurations in order for designers or operators to assess their performance.
Note 1: Depending upon the salt selected for the reactor, there may be some chemical reaction between the salt and the graphite that could affect properties. The user should establish, prior to following this guide, that any interactions between the molten salt and graphite are understood and any implications for the validity of the strength tests have been assessed.
5.2 For gas-cooled reactors, the strength of a graphite specimen is usually measured at room temperature. However, for molten salt reactors, the operating temperature of the reactor must be higher than the melting temperature of the salt, and so the salt will be in solid state at room temperature. Consequently, room temperature measurements may not be representative of the performance of the material at its true operating conditions. It is therefore necessary to measure the strength at an elevated temperature where the salt is in liquid form.
Note 2: Users should be aware that a small increase in graphite strength is expected with increasing temperature. Testing at the plant operating temperature will eliminate this small uncertainty.
5.3 The purpose of this guide is to provide considerations, which should be included in testing graphite specimens impregnated with molten salt at elevated temperature.
5.4 For the test results to be meaningful, the...
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1.1 This guide covers the best practice for strength measurements at elevated temperature of graphite impregnated with molten salt.
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
5.1 The greater a carbon black resists compression by having substantial aggregate irregularity and non-sphericity, the greater the compressed volume and void volume. Also, the more that a carbon black resists compression, the greater the energy required to compress the sample per unit void volume.
5.2 Structure is a property that strongly influences the physical properties developed in carbon black-elastomer compounds for use in tires, mechanical rubber goods, and other manufactured rubber products. Structure by void volume is based on compression while structure measurements by OAN (Test Method D2414) and COAN (Test Method D3493) are based on oil absorption.
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1.1 This test method covers a procedure to measure a carbon black structure property by Void Volume at mean pressure. Compressed void volumes are obtained by measuring the compressed volume of a weighed sample in a cylindrical chamber as a function of pressure exerted by a movable piston. A profile of void volume as a function of pressure provides a means to assess carbon black structure at varying levels of density and aggregate reduction. For the purposes of standardized testing a single value of void volume is reported at 50 MPa mean pressure.
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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- Standard4 pagesEnglish languagesale 15% off
SIGNIFICANCE AND USE
5.1 Volatile matter, when determined as herein described, may be used as a relative measure of the extent of carbonization in an activated carbon and the extent of loading of volatile material on an activated carbon that has been used in an adsorption application.
5.2 Combined with other information, the volatile matter of an activated carbon may be useful in evaluating its performance in an adsorption application.
5.3 Other automated methods for the determination of the volatile content of solids, such as using a thermogravimetric analyzer (TGA), can be used in place of this test method with equally reliable results.
SCOPE
1.1 This test method covers the determination of the percentage of gaseous products, exclusive of moisture vapor, present in virgin and used activated carbons which are released under specific conditions of the test.
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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ABSTRACT
This specification covers technical-grade calcium hypochlorite in granular form. Sampled specimens shall be tested and conform accordingly to chemical and physical requirements such as available chlorides, moisture content, and particle sizes through a U.S. 14 and U.S. 100 mesh.
SCOPE
1.1 This specification covers technical-grade calcium hypochlorite in granular form.
1.2 The following applies to all specified limits in this specification: for purposes of determining conformance with this specification, an observed value or a calculated value shall be rounded off “to the nearest unit” in the last right-hand digit used in expressing the specification limit, in accordance with the rounding-off method of Practice E29.
1.3 Units—The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.
1.4 Review the current Safety Data Sheets (SDS) for detailed information concerning toxicity, first aid procedures, handling and safety precautions.
1.5 The following safety hazards caveat pertains only to the test methods listed in Sections 3 – 5. This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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- Technical specification2 pagesEnglish languagesale 15% off
SIGNIFICANCE AND USE
5.1 This test method may be run together with Test Method C1432 to analyze for trace impurities in Pu metal. Using the technique described in this test method and the technique described in Test Method C1432 will provide the analyst with a more thorough verification of the impurity concentrations contained in the Pu metal sample. In addition, Test Method C1432 can be used to determine impurity concentrations for analytes such as Ca, Fe, Na, and Si, which have not been determined using this test method.
5.2 This test method can be used on Pu matrices in nitrate solutions.
5.3 This test method has been validated for use on materials that meet the specifications described in Specification C757 and Test Methods C758 and C759.
5.4 This test method has been validated for all elements listed in Table 1. (A) Without outlying value.
SCOPE
1.1 This test method covers the determination of trace elements in plutonium (Pu) materials such as Pu metal, Pu oxides, and Pu/uranium (U) mixed oxides. The Pu sample is dissolved in acid, and the concentration of the trace impurities are determined by Inductively Coupled Plasma-Mass Spectroscopy (ICP-MS).
1.2 This test method is specific for the determination of trace impurities where the samples are dissolved and the oxidation state is adjusted to the Pu(IV) and, if applicable, the U(VI) state. It may be applied to other matrices; however, it is the responsibility of the user to evaluate the performance of other matrices.
1.3 The use of a quadrupole ICP-MS or a high resolution ICP-MS (HR-ICP-MS) can be employed in all applications relevant to this test method. HR-ICP-MS is a better option in many cases since it can reduce or potentially eliminate interferences encountered in the following complex sample matrices.
1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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- Standard5 pagesEnglish languagesale 15% off
ABSTRACT
This set of guidelines is offered to users of activated carbon to provide a better understanding of the reactivation process and some of the problems associated with sending carbon off-site or to a third party for thermal reactivation. It is not intended to serve as an operating procedure for those companies or persons that actually operate reactivation facilities. This is true because each reactivation facility is unique, using different types of furnaces, using various operating and performance requirements, and running spent activated carbons either in aggregate pools (combining different suppliers of carbon) or in custom segregated lots. Additionally, proprietary information for each facility relative to the particular equipment used cannot be addressed in a general set of guidelines. The equipment used for thermal reactivation process usually consists of rotary kilns, vertical tube furnaces, fluidized beds, or a multiple hearth furnace. All of these can be fired directly or indirectly. Auxiliary equipment to the furnace or kiln consists of feed screws, dewatering screws, direct feed bins, dust control equipment, product coolers, screening equipment, off-gas pollution abatement equipment, and tankage.
SCOPE
1.1 This set of guidelines is offered to users of activated carbon to provide a better understanding of the reactivation process and some of the problems associated with sending carbon offsite or to a third party for thermal reactivation. It is not intended to serve as an operating procedure for those companies or persons that actually operate reactivation facilities. This is true because each reactivation facility is unique, using different types of furnaces, using various operating and performance requirements, and running spent activated carbons either in aggregate pools (combining different suppliers of carbon) or in custom segregated lots. Additionally, proprietary information for each facility relative to the particular equipment used cannot be addressed in a general set of guidelines.
1.2 This standard does not purport to address any environmental regulatory concerns associated with its use. It is the responsibility of the user of this standard to establish appropriate practices for reactivation prior to use.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
5.1 The mean maximum reflectance of the vitrinite component in coal as determined by this test method is often used as an indicator of rank as presented in Classification D388, independent of petrographic composition, and in the characterization of coal as feedstock for carbonization, gasification, liquefaction, and combustion processes.
5.2 This test method is for use in scientific and industrial research.
SCOPE
1.1 This test method covers the microscopical determination of both the mean maximum and mean random reflectances measured in oil of polished surfaces of vitrinite and other macerals present in coals ranging in rank from lignite to anthracite. This test method can be used to determine the reflectance of other macerals.
1.2 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
4.1 This test method is used to measure the total and external surface area of carbon blacks based on multipoint nitrogen adsorption. The NSA measurement is based on the B.E.T. theory and it includes the total surface area, inclusive of micropores, pore diameters less than 2 nm (20 Å). The external surface area, based on the statistical thickness method (STSA), is defined as the specific surface area that is accessible to rubber.
4.2 CTAB Surface Area (formerly Test Method D3765) has been withdrawn. The CTAB value may be estimated from the STSA value using Eq 1. The equation is based on a linear regression of the STSA and CTAB measured values of the SRB 5 standards.
SCOPE
1.1 This test method covers the determination of the total surface area by the Brunauer, Emmett, and Teller (B.E.T. NSA) theory of multilayer gas adsorption behavior using multipoint determinations and the external surface area based on the statistical thickness surface area method.
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. (The minimum safety equipment should include protective gloves, sturdy eye and face protection).
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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- Standard6 pagesEnglish languagesale 15% off
SIGNIFICANCE AND USE
4.1 Carbon and graphite can usually support higher loads in compression than in any other mode of stress. This test, therefore, provides a measure of the maximum load-bearing capability of carbon and graphite objects.
SCOPE
1.1 This test method covers the determination of the compressive strength of carbon and graphite at room temperature.
1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
4.1 The purpose of this practice is to identify sample and test parameters that may influence graphite irradiation test results. This practice should not be construed as a requirement or recommendation that proprietary information be disclosed.
4.2 Irradiation results on graphite include dimensional changes and changes in properties that are used in reactor design. The irradiation data are reported in government documents, open literature publications, and are assembled into data manuals for use by reactor designers.
SCOPE
1.1 This practice covers information recommended for inclusion in reports giving graphite irradiation results.
1.2 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
4.1 These test methods may be used for quality control testing of established grades of carbon and graphite materials, in the development of new grades, and for other purposes where relative strength levels are the primary quantities of interest. This test method may be applicable only if the ratio of specimen diameter to grain size, or flaw size, is greater than 5.
4.2 These test methods do not substitute for that described in Test Method C749, but are useful where less sophisticated data and less expensive techniques are sufficient.
4.3 Carbon and graphite materials exhibit significant physical property differences within parent materials. Exact sampling patterns and grain orientations must be specified in order to make meaningful tensile strength comparisons.
SCOPE
1.1 These test methods cover the apparatus, specimen, and procedures for the tension testing of carbon and graphite mechanical materials with a grain size smaller than 0.79 mm.
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.2.1 Exception—All of the figures are dimensioned in inches in accordance with the original standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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