13.080 - Soil quality. Pedology
ICS 13.080 Details
Soil quality. Pedology
Bodenbeschaffenheit. Bodenkunde
Qualite du sol. Pedologie
Kakovost tal. Pedologija
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- Standard7 pagesEnglish languagesale 15% off
- Standard7 pagesFrench languagesale 15% off
This document specifies a rapid method for assessing solid samples in an aerobic suspension, by determining the inhibition of dehydrogenase activity of Arthrobacter globiformis using the redox dye resazurin.
It is applicable for assessing the effect of water-soluble and solid matter bounded non-volatile contaminants in natural samples, such as soils and waste materials. Although not the main purpose, the contact test can additionally be used for testing the effect of chemicals, as described in the Annex C. The test yields a result within 6 h and can therefore be used for screening potentially contaminated test material.
- Draft33 pagesEnglish languagesale 10% offe-Library read for1 day
This European Standard specifies a method for the determination of the following elements in aqua regia, nitric acid digest solutions of sludge, treated biowaste and soil: Aluminium (Al), antimony (Sb), arsenic (As), barium (Ba), beryllium (Be), bismuth (Bi), boron (B), cadmium (Cd), calcium (Ca), chromium (Cr), cobalt (Co), copper (Cu), gallium (Ga), indium (In), iron (Fe), lead (Pb), lithium (Li), magnesium (Mg), manganese (Mn), mercury (Hg), molybdenum (Mo), nickel (Ni), phosphorus (P), potassium (K), selenium (Se), silicon (Si), silver (Ag), sodium (Na), strontium (Sr), sulfur (S), thallium (Tl), tin (Sn), titanium (Ti), tungsten (W), uranium (U), vanadium (V), zinc (Zn) and zirconium (Zr).
The method has been validated for the elements given in Table A.1. The method is applicable for the other elements listed above, provided the user has verified the applicability.
- Standard37 pagesEnglish languagesale 10% offe-Library read for1 day
This document specifies one of the methods for evaluating the habitat function of soils and determining effects of soil contaminants and substances on the reproduction of Enchytraeus sp. by dermal and alimentary uptake in a chronic test. It is applicable to soils and soil materials of unknown quality, for example, from contaminated sites, amended soils, soils after remediation, agricultural or other sites under concern and waste materials.
This document provides information on how to use this method for testing substances under temperate conditions.
The method is not applicable to substances, for which the air/soil partition coefficient is greater than 1, or to substances for which the vapour pressure exceeds 300 Pa at 25 °C.
NOTE No provision is made in the test method for monitoring the persistence of the substance under test.
- Standard31 pagesEnglish languagesale 10% offe-Library read for1 day
This document specifies one of the methods for evaluating the habitat function of soils and determining effects of soil contaminants and substances on the reproduction of Folsomia candida Willem by dermal and alimentary uptake. This document also provides information on how to use this method for testing substances under temperate conditions.
The chronic test described is applicable to soils and soil materials of unknown quality, e.g. from contaminated sites, amended soils, soils after remediation, industrial, agricultural or other sites of concern and waste materials.
The method is not applicable to volatile substances, i.e. substances for which H (Henry's constant) or the air/water partition coefficient is greater than 1, or for which the vapour pressure exceeds 300 Pa at 25 °C.
- Standard46 pagesEnglish languagesale 10% offe-Library read for1 day
This document specifies a rapid method for assessing solid samples in an aerobic suspension, by determining the inhibition of dehydrogenase activity of Arthrobacter globiformis using the redox dye resazurin. It is applicable for assessing the effect of water-soluble and solid matter bounded non-volatile contaminants in natural samples, such as soils and waste materials. Although not the main purpose, the contact test can additionally be used for testing the effect of chemicals, as described in the Annex C. The test yields a result within 6 h and can therefore be used for screening potentially contaminated test material.
- Standard27 pagesEnglish languagesale 15% off
- Standard29 pagesFrench languagesale 15% off
This document specifies a method for the determination of potential cation exchange capacity (CEC) and the content of exchangeable cations (Ca, K, Mg, Na) in soils using a molar ammonium acetate solution buffered at pH 7 as extractant.
This document is applicable to all types of air-dry soil samples which have been prepared, for example, according to ISO 11464.
- Technical specification13 pagesEnglish languagesale 10% offe-Library read for1 day
- Technical specification8 pagesEnglish languagesale 15% off
- Technical specification8 pagesFrench languagesale 15% off
This European standard specifies a method for the differentiated determination of the organic carbon content (TOC400) which is released at temperatures up to 400 °C, the residual oxidizable carbon (ROC) (including e.g. lignite (brown coal), hard coal, charcoal, black carbon, soot) and the inorganic carbon (TIC900) which is released at temperatures up to 900 °C.
The basis is the dry combustion to CO2 in a in the presence of oxygen using using temperatures ranging from 150°C to 900 °C in dry solid samples of soil, soil with anthropogenic admixtures and solid waste (see Table 1) with carbon contents of more than 1 g per kg (0,1 % C) (per carbon type in the test portion).
- Standard31 pagesEnglish languagesale 10% offe-Library read for1 day
This document specifies a method for sampling, extracting and preserving collembolans and mites from field soils as a prerequisite for using these animals as bio-indicators (e.g. to assess the quality of a soil as a habitat for organisms).
The sampling and extraction methods of this document are applicable to almost all types of soils. Exceptions can be soils from extreme climatic conditions (hard, frozen or flooded soils) and other matrices than soil, e.g. tree trunks, plants or lichens.
- Draft18 pagesEnglish languagesale 10% offe-Library read for1 day
This document specifies a method for sampling, extracting and preserving collembolans and mites from field soils as a prerequisite for using these animals as bio-indicators (e.g. to assess the quality of a soil as a habitat for organisms). The sampling and extraction methods of this document are applicable to almost all types of soils. Exceptions can be soils from extreme climatic conditions (hard, frozen or flooded soils) and other matrices than soil, e.g. tree trunks, plants or lichens.
- Standard14 pagesEnglish languagesale 15% off
- Standard14 pagesFrench languagesale 15% off
This document specifies the identification and the measurement of the activity in soils of a large number of gamma-emitting radionuclides using gamma spectrometry. This non-destructive method, applicable to large-volume samples (up to about 3 l), covers the determination in a single measurement of all the γ-emitters present for which the photon energy is between 5 keV and 3 MeV.
Generic test method and fundamentals using gamma-ray spectrometry are described in ISO 20042.
This document can be applied by test laboratories performing routine radioactivity measurements as a majority of gamma-emitting radionuclides is characterized by gamma-ray emission between 40 keV and 2 MeV.
The method can be implemented using a germanium or other type of detector with a resolution better than 5 keV.
This document addresses methods and practices for determining gamma-emitting radionuclides activity present in soil, including rock from bedrock and ore, construction materials and products, pottery, etc. This includes such soils and material containing naturally occurring radioactive material (NORM) or those from technological processes involving Technologically Enhanced Naturally Occurring Radioactive Materials (TENORM) (e.g. the mining and processing of mineral sands or phosphate fertilizer production and use) as well as of sludge and sediment. This determination of gamma-emitting radionuclides activity is typically performed for the purpose of radiation protection. It is suitable for the surveillance of the environment and the inspection of a site and allows, in case of accidents, a quick evaluation of gamma activity of soil samples. This might concern soils from gardens, farmland, urban or industrial sites that can contain building materials rubble, as well as soil not affected by human activities.
When the radioactivity characterization of the unsieved material above 200 μm or 250 μm, made of petrographic nature or of anthropogenic origin such as building materials rubble, is required, this material can be crushed in order to obtain a homogeneous sample for testing as described in ISO 18589‑2.
- Standard45 pagesEnglish languagesale 10% offe-Library read for1 day
This document specifies the identification and the measurement of the activity in soils of a large number of gamma-emitting radionuclides using gamma spectrometry. This non-destructive method, applicable to large-volume samples (up to about 3 l), covers the determination in a single measurement of all the γ-emitters present for which the photon energy is between 5 keV and 3 MeV.
Generic test method and fundamentals using gamma-ray spectrometry are described in ISO 20042.
This document can be applied by test laboratories performing routine radioactivity measurements as a majority of gamma-emitting radionuclides is characterized by gamma-ray emission between 40 keV and 2 MeV.
The method can be implemented using a germanium or other type of detector with a resolution better than 5 keV.
This document addresses methods and practices for determining gamma-emitting radionuclides activity present in soil, including rock from bedrock and ore, construction materials and products, pottery, etc. This includes such soils and material containing naturally occurring radioactive material (NORM) or those from technological processes involving Technologically Enhanced Naturally Occurring Radioactive Materials (TENORM) (e.g. the mining and processing of mineral sands or phosphate fertilizer production and use) as well as of sludge and sediment. This determination of gamma-emitting radionuclides activity is typically performed for the purpose of radiation protection. It is suitable for the surveillance of the environment and the inspection of a site and allows, in case of accidents, a quick evaluation of gamma activity of soil samples. This might concern soils from gardens, farmland, urban or industrial sites that can contain building materials rubble, as well as soil not affected by human activities.
When the radioactivity characterization of the unsieved material above 200 μm or 250 μm, made of petrographic nature or of anthropogenic origin such as building materials rubble, is required, this material can be crushed in order to obtain a homogeneous sample for testing as described in ISO 18589‑2.
- Standard45 pagesEnglish languagesale 10% offe-Library read for1 day
This document specifies a method for the determination of the following elements in aqua regia, nitric acid or mixture of hydrochloric (HCl), nitric (HNO3) and tetrafluoroboric (HBF4)/hydrofluoric (HF) acid digests of soil, treated biowaste, waste, sludge and sediment:
Aluminium (Al), antimony (Sb), arsenic (As), barium (Ba), beryllium (Be), bismuth (Bi), boron (B), cadmium (Cd), calcium (Ca), cerium (Ce), chromium (Cr), cobalt (Co), copper (Cu), dysprosium (Dy), erbium (Er), europium (Eu), gallium (Ga), gadolinium (Gd), germanium (Ge), gold (Au), hafnium (Hf), holmium (Ho), indium (In), iridium (Ir), iron (Fe), lanthanum (La), lead (Pb), lithium (Li), lutetium (Lu) magnesium (Mg), manganese (Mn), mercury (Hg), molybdenum (Mo), neodymium (Nd), nickel (Ni), palladium (Pd), phosphorus (P), platinum (Pt), potassium (K), praseodymium (Pr), rhodium (Rh), ruthenium (Ru), samarium (Sm), scandium (Sc), selenium (Se), silicon (Si), silver (Ag), sodium (Na), strontium (Sr), sulfur (S), tantalum (Ta), tellurium (Te), terbium (Tb), thallium (Tl), thulium (Tm), thorium (Th), tin (Sn), titanium (Ti), tungsten (W), vanadium (V), yttrium (Y), ytterbium (Yb), zinc (Zn) and zirconium (Zr).
The method is also applicable to other extracts or digests originating from, for example, DTPA extraction, fusion methods or total digestion methods, provided the user has verified the applicability.
The method has been validated for the elements given in Table A.1 (sludge), Table A.2 (compost) and Table A.3 (soil). The method is applicable for other solid matrices and other elements as listed above, provided the user has verified the applicability.
This method is also applicable for the determination of major, minor and trace elements in aqua regia and nitric acid digests and in eluates of construction products (EN 17200[22]).
NOTE Construction products include e.g. mineral-based products; bituminous products; metals; wood-based products; plastics and rubbers; sealants and adhesives; paints and coatings.
- Standard37 pagesEnglish languagesale 10% offe-Library read for1 day
This document specifies a method for the determination of the following elements in aqua regia, nitric acid or mixture of hydrochloric (HCl), nitric (HNO3) and tetrafluoroboric (HBF4)/hydrofluoric (HF) acid digests of soil, treated biowaste, waste, sludge and sediment: Aluminium (Al), antimony (Sb), arsenic (As), barium (Ba), beryllium (Be), bismuth (Bi), boron (B), cadmium (Cd), calcium (Ca), cerium (Ce), chromium (Cr), cobalt (Co), copper (Cu), dysprosium (Dy), erbium (Er), europium (Eu), gallium (Ga), gadolinium (Gd), germanium (Ge), gold (Au), hafnium (Hf), holmium (Ho), indium (In), iridium (Ir), iron (Fe), lanthanum (La), lead (Pb), lithium (Li), lutetium (Lu) magnesium (Mg), manganese (Mn), mercury (Hg), molybdenum (Mo), neodymium (Nd), nickel (Ni), palladium (Pd), phosphorus (P), platinum (Pt), potassium (K), praseodymium (Pr), rhodium (Rh), ruthenium (Ru), samarium (Sm), scandium (Sc), selenium (Se), silicon (Si), silver (Ag), sodium (Na), strontium (Sr), sulfur (S), tantalum (Ta), tellurium (Te), terbium (Tb), thallium (Tl), thulium (Tm), thorium (Th), tin (Sn), titanium (Ti), tungsten (W), vanadium (V), yttrium (Y), ytterbium (Yb), zinc (Zn) and zirconium (Zr). The method is also applicable to other extracts or digests originating from, for example, DTPA extraction, fusion methods or total digestion methods, provided the user has verified the applicability. The method has been validated for the elements given in Table A.1 (sludge), Table A.2 (compost) and Table A.3 (soil). The method is applicable for other solid matrices and other elements as listed above, provided the user has verified the applicability. This method is also applicable for the determination of major, minor and trace elements in aqua regia and nitric acid digests and in eluates of construction products (EN 17200[22]). NOTE Construction products include e.g. mineral-based products; bituminous products; metals; wood-based products; plastics and rubbers; sealants and adhesives; paints and coatings.
- Standard29 pagesEnglish languagesale 15% off
- Standard31 pagesFrench languagesale 15% off
This document specifies a method for the determination of potential cation exchange capacity (CEC) and the content of exchangeable cations (Ca, K, Mg, Na) in soils using a molar ammonium acetate solution buffered at pH 7 as extractant. This document is applicable to all types of air-dry soil samples which have been prepared, for example, according to ISO 11464.
- Technical specification13 pagesEnglish languagesale 10% offe-Library read for1 day
- Technical specification8 pagesEnglish languagesale 15% off
- Technical specification8 pagesFrench languagesale 15% off
This document specifies a test with which in situ available concentrations of inorganic substances (such as heavy metals, arsenic and phosphorus) and organic substances in soil and soil-like materials can be simulated under forced aerobic and anaerobic conditions. The toxicity can then be estimated based on these available concentrations. The test described in this document aims to measure the release of inorganic and organic substances from soil and soil-like material as well as to produce eluates for subsequent ecotoxicological testing. For ecotoxicological testing, see ISO 15799 and ISO 17616. The eluate obtained can subsequently be characterized by physical, chemical and ecotoxicological methods in accordance with existing standard methods. The test is not suitable for substances that are volatile under ambient conditions. This procedure is not applicable to materials with a dry-matter-content ratio lower than 33 %. This test is mainly aimed at being used for routine and control purposes, and it cannot be used alone to describe all leaching properties of a soil. Additional leaching tests are needed for that extended goal. This document does not address issues related to health and safety. It only determines the leaching properties outlined in Clause 4.
- Standard20 pagesEnglish languagesale 15% off
- Standard21 pagesFrench languagesale 15% off
This document specifies methods for quantitative determination of seven selected polychlorinated biphenyls (PCB28, PCB52, PCB101, PCB118, PCB138, PCB153 and PCB180) in soil, sludge, sediment, treated biowaste, and waste using GC-MS and GC-ECD (see Table 2). The limit of detection depends on the determinants, the equipment used, the quality of chemicals used for the extraction of the sample and the clean-up of the extract. Under the conditions specified in this document, lower limit of application from 1 μg/kg (expressed as dry matter) for soils, sludge and biowaste to 10 μg/kg (expressed as dry matter) for solid waste can be achieved. For some specific samples the limit of 10 μg/kg cannot be reached. Sludge, waste and treated biowaste may differ in properties, as well as in the expected contamination levels of PCB and presence of interfering substances. These differences make it impossible to describe one general procedure. This document contains decision tables based on the properties of the sample and the extraction and clean-up procedure to be used. NOTE The analysis of PCB in insulating liquids, petroleum products, used oils and aqueous samples is referred to in EN 61619, EN 12766-1 and ISO 6468 respectively. The method can be applied to the analysis of other PCB congeners not specified in the scope, provided suitability is proven by proper in-house validation experiments.
- Standard40 pagesEnglish languagesale 15% off
This document provides specific requirements and recommendations on soil sampling and semi-quantitative measurements in field investigations for volatile organic compounds (VOCs) that are not explicitly covered in the existing ISO 18400 series. In addition, it provides information on the preparation steps (choosing a sampling strategy, defining a sampling plan); describes sampling techniques (drilling techniques, sampling devices and procedures) and field measurements; and gives advice on conservation, packaging, transport and delivery to the laboratory in the context of VOCs (see soil sampling process described in Figure 2). VOCs to which this document can be applied include: — volatile aromatic hydrocarbons such as benzene, toluene, ethylbenzene, naphthalene; — aliphatic ethers such as methyl tert.-butyl ether(MTBE), ethyl tert.-butyl ether (ETBE) and tert.-amyl methyl ether (TAME); — volatile halogenated hydrocarbons such as tetrachloroethene and, trichloroethene. The document does not cover the volatile non-organic compounds. However, some information about these is provided in Annex D. This document provides requirements and guidance on the selection of drilling and sampling techniques for determining VOCs and how to use them. It clarifies the applicability and limits of the drilling and sampling techniques, taking into account the physical, chemical or biological reactions that can occur in soil. This document gives requirements and recommendations on the use of instrumental measurement techniques for determination of VOC concentrations in air, firstly in relation to worker safety, and subsequently for semi-quantitative measurements of volatiles during soil sampling. The following subjects are outside the scope of this document: — direct quantitative measurement of volatile compounds by field analysis laboratories; — investigations and evaluation of soil gas quality (these are dealt with ISO 18400 204); — safety risk assessment; and — analytical procedures.
- Standard52 pagesEnglish languagesale 15% off
- Standard54 pagesFrench languagesale 15% off
This document specifies one of the methods for evaluating the habitat function of soils and determining effects of soil contaminants and substances on the reproduction of Folsomia candida Willem by dermal and alimentary uptake. This document also provides information on how to use this method for testing substances under temperate conditions.
The chronic test described is applicable to soils and soil materials of unknown quality, e.g. from contaminated sites, amended soils, soils after remediation, industrial, agricultural or other sites of concern and waste materials.
The method is not applicable to volatile substances, i.e. substances for which H (Henry's constant) or the air/water partition coefficient is greater than 1, or for which the vapour pressure exceeds 300 Pa at 25 °C.
- Standard46 pagesEnglish languagesale 10% offe-Library read for1 day
This document specifies one of the methods for evaluating the habitat function of soils and determining effects of soil contaminants and substances on the reproduction of Folsomia candida Willem by dermal and alimentary uptake. This document also provides information on how to use this method for testing substances under temperate conditions. The chronic test described is applicable to soils and soil materials of unknown quality, e.g. from contaminated sites, amended soils, soils after remediation, industrial, agricultural or other sites of concern and waste materials. The method is not applicable to volatile substances, i.e. substances for which H (Henry's constant) or the air/water partition coefficient is greater than 1, or for which the vapour pressure exceeds 300 Pa at 25 °C.
- Standard38 pagesEnglish languagesale 15% off
- Standard43 pagesFrench languagesale 15% off
This document specifies the identification and the measurement of the activity in soils of a large number of gamma-emitting radionuclides using gamma spectrometry. This non-destructive method, applicable to large-volume samples (up to about 3 l), covers the determination in a single measurement of all the γ-emitters present for which the photon energy is between 5 keV and 3 MeV. Generic test method and fundamentals using gamma-ray spectrometry are described in ISO 20042. This document can be applied by test laboratories performing routine radioactivity measurements as a majority of gamma-emitting radionuclides is characterized by gamma-ray emission between 40 keV and 2 MeV. The method can be implemented using a germanium or other type of detector with a resolution better than 5 keV. This document addresses methods and practices for determining gamma-emitting radionuclides activity present in soil, including rock from bedrock and ore, construction materials and products, pottery, etc. This includes such soils and material containing naturally occurring radioactive material (NORM) or those from technological processes involving Technologically Enhanced Naturally Occurring Radioactive Materials (TENORM) (e.g. the mining and processing of mineral sands or phosphate fertilizer production and use) as well as of sludge and sediment. This determination of gamma-emitting radionuclides activity is typically performed for the purpose of radiation protection. It is suitable for the surveillance of the environment and the inspection of a site and allows, in case of accidents, a quick evaluation of gamma activity of soil samples. This might concern soils from gardens, farmland, urban or industrial sites that can contain building materials rubble, as well as soil not affected by human activities. When the radioactivity characterization of the unsieved material above 200 μm or 250 μm, made of petrographic nature or of anthropogenic origin such as building materials rubble, is required, this material can be crushed in order to obtain a homogeneous sample for testing as described in ISO 18589‑2.
- Standard35 pagesEnglish languagesale 15% off
- Standard36 pagesFrench languagesale 15% off
This document outlines methodologies for soil temperature measurement and provides guidance on the selection of a measurement method depending on measurement purposes. It also gives guidance on characteristics, performance and use of infrared (IR) thermometers which is now widely applied to obtain rapid measurements and thermistors which have been commonly used to obtain more accurate measurements.
- Standard9 pagesEnglish languagesale 15% off
This document specifies a method for determining of perchlorate in soil and soil-like materials using liquid chromatography connected to a tandem mass spectrometry (LC-MS/MS). It defines pretreatment (including drying and sieving) of sample, extraction, clean-up, analysis using LC-MS/MS, and calculation of perchlorate content in dry soil. Under the conditions specified in this document, the limit of quantitation (LOQ) is approximately 4,6 μg/kg-dry soil.
- Standard12 pagesEnglish languagesale 15% off
This document describes a method for the determination of the loss on ignition (wLOI) of fine, intermediate, composite and coarse soils, organic soils and anthropogenic materials (according to EN 16907-2) after ignition under air at 550°C.
The loss of mass suffered by these materials at 550 °C is usually due to the release of volatile compounds, water (absorbed, crystalized or structural) and gases from decomposition of organic matter and inorganic substances such as sulfur, sulphides or hydroxides (e.g. H2O, CO2, SO2).
A method is given in Annex B in order to estimate the organic matter content (COM) from the value of wLOI for clayed soils.
- Standard12 pagesEnglish languagesale 10% offe-Library read for1 day
This document specifies one of the methods for evaluating the habitat function of soils and determining effects of soil contaminants and substances on the reproduction of Enchytraeus sp. by dermal and alimentary uptake in a chronic test. It is applicable to soils and soil materials of unknown quality, for example, from contaminated sites, amended soils, soils after remediation, agricultural or other sites under concern and waste materials.
This document provides information on how to use this method for testing substances under temperate conditions.
The method is not applicable to substances, for which the air/soil partition coefficient is greater than 1, or to substances for which the vapour pressure exceeds 300 Pa at 25 °C.
NOTE No provision is made in the test method for monitoring the persistence of the substance under test.
- Standard31 pagesEnglish languagesale 10% offe-Library read for1 day
This document specifies one of the methods for evaluating the habitat function of soils and determining the effects of soil contaminants and chemicals on the reproduction of Eisenia fetida/Eisenia andrei by dermal and alimentary uptake. This chronic test is applicable to soils and soil materials of unknown quality, e.g. from contaminated sites, amended soils, soils after remediation, agricultural or other sites concerned, and waste materials.
This method is designed mainly for determining the effects of soil contaminants and chemicals on the reproduction of Eisenia fetida/Eisenia andrei. Technical information is also provided on how to use Eisenia fetida/andrei for testing chemicals under tropical conditions (see Annex A). Finally, this method also includes technical information on how to use it with other environmentally relevant earthworm species: e.g., Aporrectodea caliginosa and Dendrodrilus rubidus (see Annexes B and C).
This method does not apply to substances for which the air/soil partition coefficient is greater than one, or to substances with vapour pressure exceeding 300 Pa, at 25 °C. This method does not take into account the persistence of the substance during the test.
- Standard44 pagesEnglish languagesale 10% offe-Library read for1 day
This document specifies one of the methods for evaluating the habitat function of soils and determining effects of soil contaminants and substances on the reproduction of Enchytraeus sp. by dermal and alimentary uptake in a chronic test. It is applicable to soils and soil materials of unknown quality, for example, from contaminated sites, amended soils, soils after remediation, agricultural or other sites under concern and waste materials. This document provides information on how to use this method for testing substances under temperate conditions. The method is not applicable to substances, for which the air/soil partition coefficient is greater than 1, or to substances for which the vapour pressure exceeds 300 Pa at 25 °C. NOTE No provision is made in the test method for monitoring the persistence of the substance under test.
- Standard23 pagesEnglish languagesale 15% off
- Standard25 pagesFrench languagesale 15% off
This document specifies a method for the determination of the loss on ignition (wLOI) of fine, intermediate, composite and coarse soils, organic soils and anthropogenic materials (according to
EN 16907 2) after ignition under air at 550°C.
NOTE The loss of mass suffered by these materials at 550 °C is usually due to the release of volatile compounds, water (absorbed, crystalized or structural) and gases from decomposition of organic matter and inorganic substances such as sulfur, sulfides or hydroxides (e.g. H2O, CO2, SO2).
A method is given in Annex B in order to estimate the organic matter content (COM) from the value of wLOI for clayey soils.
- Standard12 pagesEnglish languagesale 10% offe-Library read for1 day
This document specifies a method for quantitative determination of 17 2,3,7,8-chlorine substituted dibenzo-p-dioxins and dibenzofurans and dioxin-like polychlorinated biphenyls in sludge, treated biowaste and soil using liquid column chromatographic clean-up methods and GC/HRMS. The analytes to be determined with this document are listed in Table 1. The limit of detection depends on the kind of sample, the congener, the equipment used and the quality of chemicals used for extraction and clean-up. Under the conditions specified in this document, limits of detection better than 1 ng/kg (expressed as dry matter) can be achieved. This method is “performance based”. The method can be modified if all performance criteria given in this method are met. NOTE In principle, this method can also be applied for sediments, mineral wastes and for vegetation. It is the responsibility of the user of this document to validate the application for these matrices. For measurement in complex matrices like fly ashes adsorbed on vegetation, it can be necessary to further improve the clean-up. This can also apply to sediments and mineral wastes.
- Standard37 pagesEnglish languagesale 15% off
- Standard40 pagesFrench languagesale 15% off
This document specifies a method for sampling and handling free-living nematodes from terrestrial field soils as a prerequisite for using them as bio-indicators (e.g. to assess the quality of a soil as a habitat for organisms).
This document applies to all terrestrial biotopes in which nematodes occur. The sampling design of field studies in general is specified in ISO 18400-101.
This document is not applicable to aquatic nematodes because of differences in the sample matrix (e.g. water column). Methods for some other soil organism groups such as earthworms, collembolans enchytraeids or macro-invertebrates are covered in ISO 23611-1, ISO 23611-2, ISO 23611-3 and ISO 23611-5.
This document does not cover the pedological characterization of the site which is highly recommendable when sampling soil invertebrates. ISO 10390, ISO 10694, ISO 11272, ISO 11274, ISO 11277, ISO 11461 and ISO 11465 include suitable procedures for measuring pH, particle size distribution, C/N ratio, organic carbon content and water-holding capacity.
- Standard35 pagesEnglish languagesale 10% offe-Library read for1 day
This document specifies the crucial steps of a quantitative real-time polymerase chain reaction (qPCR) method to quantify the abundance of specific mRNA molecules extracted from Daphnia magna.
The method allows the identification of molecular responses to exposures for potentially toxic substances through the analysis of the abundance of specific mRNA molecules. In this document, the central genes involved in reproductive and toxic responses are included.
NOTE The selection of genes can be adapted to specific exposure conditions, for example, exposure to known toxic substances, by adding genes known to respond to a specific insult.
The present method allows for rapid, robust and sensitive detection of molecular responses and can be used to analyse the toxic effects of water leachates from soil and waste. The method gives information of the concentration of a substance or test-liquid at which toxic effects begin to occur prior to observations of reproductive or toxic effects at higher levels of organization, which reduces the need for the use of safety factors in toxicity assessment.
The method is useful in several types of risk assessment. In this document, the genes studied are appropriate for the assessment of the risks when recycling materials and for the classification of waste, but the method can be adapted to other types of risk assessment by including other genes.
- Technical specification23 pagesEnglish languagesale 10% offe-Library read for1 day
- Technical specification23 pagesEnglish languagesale 10% offe-Library read for1 day
ISO 19204:2017 describes in a general way the application of the soil quality TRIAD approach for the site-specific ecological risk assessment of contaminated soils. In detail, it presents in a transparent way three lines of evidence (chemistry, ecotoxicology and ecology) which together allow an efficient, ecologically robust but also practical risk assessment of contaminated soils. This procedure can also be applicable to other stress factors, such as acidification, soil compaction, salinization, loss of soil organic substance, and erosion. However, so far, no experience has been gained with these other applications. Therefore, this document focuses on soils contaminated by chemicals.
NOTE 1 This document focuses on ecological risk assessment. Thus, it does not cover human health end points.
In view of the nature of this document, the investigation procedure is described on a general level. It does not contain details of technical procedures for the actual assessment. However, this document includes references relating to technical standards (e.g. ISO 15799, ISO 17616) which are useful for the actual performance of the three lines of evidence.
In ecological risk assessment, the effects of soil contamination on the ecosystem are related to the intended land use and the requirements that this use sets for properly functioning soil. This document describes the basic steps relating to a coherent tool for a site-specific risk assessment with opportunities to work out site-specific details.
ISO 19204:2017 can also be used for the evaluation of clean-up operations, remediation processes or management measures (i.e. for the evaluation of the environmental quality after having performed such actions).
NOTE 2 This document starts when it has already been decided that an ecological risk assessment at a given site needs to be performed. In other words, the practical performance of the soil quality TRIAD and the evaluation of the individual test results will be described. Thus, nothing will be said about decisions whether (and if yes, how) the results of the assessment are included in soil management measures or not.
NOTE 3 The TRIAD approach can be used for different parts of the environment, but this document focuses mostly on the soil compartment. Comparable documents for other environmental compartments are intended to be prepared in addition (e.g. the terrestrial aboveground compartment) in order to perform a complete site assessment, based on the same principles and processes.
- Standard35 pagesEnglish languagesale 10% offe-Library read for1 day
This European Standard specifies a method for quantitative determination of 16 polycyclic aromatic hydrocarbons (PAH) (see Table ) in soil, sludge, sediment, treated biowaste, and waste, using GC-MS and HPLC-UV-DAD/FLD covering a wide range of PAH contamination levels (see Table 2).
When using fluorescence detection, acenaphthylene cannot be measured.
Table —Target analytes of this European Standard
Target analyte CAS-RNa
Naphthalene 91–20–3
Acenaphthene 83–32–9
Acenaphthylene 208–96–8
Fluorene 86–73–7
Anthracene 120–12–7
Phenanthrene 85–01–8
Fluoranthene 206–44–0
Pyrene 129–00–0
Benz[a]anthracene 56–55–3
Chrysene 218–01–9
Benzo[b]fluoranthene 205–99–2
Benzo[k]fluoranthene 207–08–9
Benzo[a]pyrene 50–32–8
Indeno[1,2,3-cd]pyrene 193–39–5
Dibenz[a,h]anthracene 53–70–3
Benzo[ghi]perylene 191–24–2
a CAS-RN Chemical Abstracts Service Registry Number.
The limit of detection depends on the determinants, the equipment used, the quality of chemicals used for the extraction of the sample and the clean-up of the extract
Under the conditions specified in this European Standard, lower limit of application from 10 μg/kg (expressed as dry matter) for soils, sludge and biowaste to 100 μg/kg (expressed as dry matter) for solid waste can be achieved. For some specific samples (e.g. bitumen) the limit of 100 μg/kg cannot be reached.
Sludge, waste and treated biowaste may differ in properties as well as in the expected contamination levels of PAH and presence of interfering substances. These differences make it impossible to describe one general procedure. This European Standard contains decision tables based on the properties of the sample and the extraction and clean-up procedure to be used.
The method may be applied to the analysis of other PAH not specified in the scope, provided suitability is proven by proper in-house validation experiments.
- Standard53 pagesEnglish languagesale 10% offe-Library read for1 day
This document is one of the family of standards (ISO 15799, ISO 19204) providing guidance on the characterization of soils and soil materials in relation to their retention and habitat functions and uses. It is appropriate to use it in conjunction with the two other standards in this family. It provides guidance on the choice and evaluation of tests applied for ecotoxicological characterization of soils and soil materials. Recommendations for test strategies with respect to the protection of ground and surface waters and the maintenance of the habitat function of soil are included. The tests recommended represent a minimum test battery that can be complemented by additional tests, or even be replaced by others, according to the intended uses or protection goals envisaged. The effect values indicated in this document do not refer to regulation but represent the lowest level at which an adverse effect is considered likely to occur.
- Standard21 pagesEnglish languagesale 10% offe-Library read for1 day
This document is one of a family of International Standards providing guidance on soils and soil materials in relation to certain functions and uses including conservation of biodiversity. It applies in conjunction with these other standards. It provides guidance on the selection of experimental methods for the assessment of the ecotoxic potential of soils and soil materials (e.g. excavated and remediated soils, refills, embankments) with respect to their intended use and possible adverse effects on aquatic and soil dwelling organisms.
NOTE This is a reflection of the maintenance of the habitat and retention function of the soil. In fact, the methods listed in this document are suitable for usage in a TRIAD approach, i.e. for an ecological assessment of potentially contaminated soils (see ISO 19204).
This document does not cover tests for bioaccumulation.
The ecological assessment of uncontaminated soils with a view to natural, agricultural or horticultural use is not within the scope of this document. Such soils can be of interest if they can serve as a reference for the assessment of soils from contaminated sites.
The interpretation of results gained by applying the proposed methods is not in the scope of this document.
- Standard58 pagesEnglish languagesale 10% offe-Library read for1 day
This document specifies one of the methods for evaluating the habitat function of soils and determining the effects of soil contaminants and chemicals on the reproduction of Eisenia fetida/Eisenia andrei by dermal and alimentary uptake. This chronic test is applicable to soils and soil materials of unknown quality, e.g. from contaminated sites, amended soils, soils after remediation, agricultural or other sites concerned, and waste materials.
This method is designed mainly for determining the effects of soil contaminants and chemicals on the reproduction of Eisenia fetida/Eisenia andrei. Technical information is also provided on how to use Eisenia fetida/andrei for testing chemicals under tropical conditions (see Annex A). Finally, this method also includes technical information on how to use it with other environmentally relevant earthworm species: e.g. Dendrodrilus rubidus and Aporrectodea caliginosa (see Annexes B and C).
This method does not apply to substances for which the air/soil partition coefficient is greater than one, or to substances with vapour pressure exceeding 300 Pa, at 25 °C. This method does not take into account the persistence of the substance during the test.
- Standard44 pagesEnglish languagesale 10% offe-Library read for1 day
This document specifies one of the methods for evaluating the habitat function of soils and determining the effects of soil contaminants and chemicals on the reproduction of Eisenia fetida/Eisenia andrei by dermal and alimentary uptake. This chronic test is applicable to soils and soil materials of unknown quality, e.g. from contaminated sites, amended soils, soils after remediation, agricultural or other sites concerned, and waste materials. This method is designed mainly for determining the effects of soil contaminants and chemicals on the reproduction of Eisenia fetida/Eisenia andrei. Technical information is also provided on how to use Eisenia fetida/andrei for testing chemicals under tropical conditions (see Annex A). Finally, this method also includes technical information on how to use it with other environmentally relevant earthworm species: e.g. Dendrodrilus rubidus and Aporrectodea caliginosa (see Annexes B and C). This method does not apply to substances for which the air/soil partition coefficient is greater than one, or to substances with vapour pressure exceeding 300 Pa, at 25 °C. This method does not take into account the persistence of the substance during the test.
- Standard36 pagesEnglish languagesale 15% off
This European standard specifies a method for the differentiated determination of the organic carbon content (TOC400) which is released at temperatures up to 400 °C, the residual oxidizable carbon (ROC) (including e.g. lignite (brown coal), hard coal, charcoal, black carbon, soot) and the inorganic carbon (TIC900) which is released at temperatures up to 900 °C.
The basis is the dry combustion to CO2 in a in the presence of oxygen using using temperatures ranging from 150°C to 900 °C in dry solid samples of soil, soil with anthropogenic admixtures and solid waste (see Table 1) with carbon contents of more than 1 g per kg (0,1 % C) (per carbon type in the test portion).
- Standard31 pagesEnglish languagesale 10% offe-Library read for1 day
This document specifies the crucial steps of a quantitative real-time polymerase chain reaction (qPCR) method to quantify the abundance of specific mRNA molecules extracted from Daphnia magna.
The method allows the identification of molecular responses to exposures for potentially toxic substances through the analysis of the abundance of specific mRNA molecules. In this document, the central genes involved in reproductive and toxic responses are included.
NOTE The selection of genes can be adapted to specific exposure conditions, for example, exposure to known toxic substances, by adding genes known to respond to a specific insult.
The present method allows for rapid, robust and sensitive detection of molecular responses and can be used to analyse the toxic effects of water leachates from soil and waste. The method gives information of the concentration of a substance or test-liquid at which toxic effects begin to occur prior to observations of reproductive or toxic effects at higher levels of organization, which reduces the need for the use of safety factors in toxicity assessment.
The method is useful in several types of risk assessment. In this document, the genes studied are appropriate for the assessment of the risks when recycling materials and for the classification of waste, but the method can be adapted to other types of risk assessment by including other genes.
- Technical specification23 pagesEnglish languagesale 10% offe-Library read for1 day
- Technical specification23 pagesEnglish languagesale 10% offe-Library read for1 day
This document specifies the general requirements, based on ISO 11074 and ISO/IEC 17025, for all steps in the planning (desk study and area reconnaissance) of the sampling and the preparation of samples for testing. It includes the selection of the sampling strategy, the outline of the sampling plan, the presentation of general sampling methods and equipment, as well as the methodology of the pre-treatment of samples adapted to the measurements of the activity of radionuclides in soil including granular materials of mineral origin which contain NORM or artificial radionuclides, such as sludge, sediment, construction debris, solid waste of different type and materials from technologically enhanced naturally occurring radioactive materials (mining, coal combustion, phosphate fertilizer production etc.). For simplification, the term “soil” used in this document covers the set of elements mentioned above. This document is addressed to the people responsible for determining the radioactivity present in soil for the purpose of radiation protection. It is applicable to soil from gardens, farmland, urban, or industrial sites, as well as soil not affected by human activities. This document is applicable to all laboratories regardless of the number of personnel or the range of the testing performed. When a laboratory does not undertake one or more of the activities covered by this document, such as planning, sampling, test or calibration, the corresponding requirements do not apply. NOTE The term “laboratory” is applicable to all identified entities (individuals, organizations, etc.) performing planning, sampling, test and calibration.
- Standard28 pagesEnglish languagesale 15% off
- Standard31 pagesFrench languagesale 15% off
- Amendment7 pagesEnglish languagesale 10% offe-Library read for1 day
This document aims to assist in designing and organizing trials for validation of biotests. The validation activities during the different steps of the standardization process are described. This document comprises the overall data evaluation and subsequent validation study conclusion. This document is intended for the validation of biotests which can differ in their experimental design and endpoints. It is possible that some of the requirements of this document are not applicable to all test methods.
- Technical specification43 pagesEnglish languagesale 15% off
- Technical specification42 pagesFrench languagesale 15% off
- Technical specification42 pagesFrench languagesale 15% off
This document specifies a test procedure for the evaluation of the habitat function of soils by determining effects of soil contaminants and substances on organic matter decomposition. This test is applicable to natural soils and soil materials of unknown quality (e.g. contaminated sites, amended soils, soils after remediation, agricultural or other sites under concern). This document also specifies how to use this method for testing substances under temperate conditions. This document is not applicable to substances for which the air/soil partition coefficient is greater than 1. It is not applicable to substances with vapour pressure exceeding 300 Pa at 25 °C. NOTE The stability of the test substance cannot be ensured over the test period. No provision is made in the test method for monitoring the persistence of the substance under test.
- Standard17 pagesEnglish languagesale 15% off
- Standard20 pagesFrench languagesale 15% off
ISO 19204:2017 describes in a general way the application of the soil quality TRIAD approach for the site-specific ecological risk assessment of contaminated soils. In detail, it presents in a transparent way three lines of evidence (chemistry, ecotoxicology and ecology) which together allow an efficient, ecologically robust but also practical risk assessment of contaminated soils. This procedure can also be applicable to other stress factors, such as acidification, soil compaction, salinization, loss of soil organic substance, and erosion. However, so far, no experience has been gained with these other applications. Therefore, this document focuses on soils contaminated by chemicals.
NOTE 1 This document focuses on ecological risk assessment. Thus, it does not cover human health end points.
In view of the nature of this document, the investigation procedure is described on a general level. It does not contain details of technical procedures for the actual assessment. However, this document includes references relating to technical standards (e.g. ISO 15799, ISO 17616) which are useful for the actual performance of the three lines of evidence.
In ecological risk assessment, the effects of soil contamination on the ecosystem are related to the intended land use and the requirements that this use sets for properly functioning soil. This document describes the basic steps relating to a coherent tool for a site-specific risk assessment with opportunities to work out site-specific details.
ISO 19204:2017 can also be used for the evaluation of clean-up operations, remediation processes or management measures (i.e. for the evaluation of the environmental quality after having performed such actions).
NOTE 2 This document starts when it has already been decided that an ecological risk assessment at a given site needs to be performed. In other words, the practical performance of the soil quality TRIAD and the evaluation of the individual test results will be described. Thus, nothing will be said about decisions whether (and if yes, how) the results of the assessment are included in soil management measures or not.
NOTE 3 The TRIAD approach can be used for different parts of the environment, but this document focuses mostly on the soil compartment. Comparable documents for other environmental compartments are intended to be prepared in addition (e.g. the terrestrial aboveground compartment) in order to perform a complete site assessment, based on the same principles and processes.
- Standard35 pagesEnglish languagesale 10% offe-Library read for1 day
This document is one of a family of International Standards providing guidance on soils and soil materials in relation to certain functions and uses including conservation of biodiversity. It applies in conjunction with these other standards. It provides guidance on the selection of experimental methods for the assessment of the ecotoxic potential of soils and soil materials (e.g. excavated and remediated soils, refills, embankments) with respect to their intended use and possible adverse effects on aquatic and soil dwelling organisms.
NOTE This is a reflection of the maintenance of the habitat and retention function of the soil. In fact, the methods listed in this document are suitable for usage in a TRIAD approach, i.e. for an ecological assessment of potentially contaminated soils (see ISO 19204).
This document does not cover tests for bioaccumulation.
The ecological assessment of uncontaminated soils with a view to natural, agricultural or horticultural use is not within the scope of this document. Such soils can be of interest if they can serve as a reference for the assessment of soils from contaminated sites.
The interpretation of results gained by applying the proposed methods is not in the scope of this document.
- Standard58 pagesEnglish languagesale 10% offe-Library read for1 day
This document is one of the family of standards (ISO 15799, ISO 19204) providing guidance on the characterization of soils and soil materials in relation to their retention and habitat functions and uses. It is appropriate to use it in conjunction with the two other standards in this family. It provides guidance on the choice and evaluation of tests applied for ecotoxicological characterization of soils and soil materials. Recommendations for test strategies with respect to the protection of ground and surface waters and the maintenance of the habitat function of soil are included. The tests recommended represent a minimum test battery that can be complemented by additional tests, or even be replaced by others, according to the intended uses or protection goals envisaged. The effect values indicated in this document do not refer to regulation but represent the lowest level at which an adverse effect is considered likely to occur.
- Standard21 pagesEnglish languagesale 10% offe-Library read for1 day
- Amendment8 pagesEnglish languagesale 10% offe-Library read for1 day
This document specifies an instrumental method for the routine determination of pH within the range pH 2 to pH 12 using a glass electrode in a 1:5 (volume fraction) suspension of soil, sludge and treated biowaste in either water (pH in H2O), in 1 mol/l potassium chloride solution (pH in KCl) or in 0,01 mol/l calcium chloride solution (pH in CaCl2).
This document is applicable to all types of air-dried soil and treated biowaste samples.
NOTE For example, pretreated in accordance with ISO 11464 or EN 16179 or EN 15002.
- Standard15 pagesEnglish languagesale 10% offe-Library read for1 day
This document specifies a method for sampling and handling free-living nematodes from terrestrial field soils as a prerequisite for using them as bio-indicators (e.g. to assess the quality of a soil as a habitat for organisms).
This document applies to all terrestrial biotopes in which nematodes occur. The sampling design of field studies in general is specified in ISO 18400-101.
This document is not applicable to aquatic nematodes because of differences in the sample matrix (e.g. water column). Methods for some other soil organism groups such as earthworms, collembolans enchytraeids or macro-invertebrates are covered in ISO 23611-1, ISO 23611-2, ISO 23611-3 and ISO 23611-5.
This document does not cover the pedological characterization of the site which is highly recommendable when sampling soil invertebrates. ISO 10390, ISO 10694, ISO 11272, ISO 11274, ISO 11277, ISO 11461 and ISO 11465 include suitable procedures for measuring pH, particle size distribution, C/N ratio, organic carbon content and water-holding capacity.
- Standard35 pagesEnglish languagesale 10% offe-Library read for1 day
This document specifies two methods for the determination of total organic carbon (TOC) in sludge, treated biowaste, soil and waste samples containing more than 0,1 % carbon in relation to the dry mass (dm).
NOTE This method can also be applied to other environmental solid matrices, provided the user has verified the applicability.
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